Abstract: 1. An improved method for producing fine nickel powder having a substantially spherical form and size ranging from about 3 microns to about 7 microns, containing sulphur within a critical range of about 0.02% to about 0.

Abstract: A gelled concentrate composition contains 70 to 30 weight percent gelled liquid and 30 to 70 weight percent solids component. The solids component comprises a fine powder of an ammonium compound and a vinyl polymer gelling agent. The gelling agent is present in the amount of 0.5 to 8.0 weight percent of the total composition. The resulting gelled concentrate, stable up to 18 months in storage, is useful in extinguishing fires.

Abstract: There is proposed for the final storage of radioactive wastes a container made of an uranium alloy which compared to known containers made of uranium is less susceptible to corrosion and does not show any anisotropic thermal expansion at high temperatures. For this purpose, there is alloyed with uranium, which is preferably depleted, 5 to 15 wt. % molybdenum, 2 to 15 wt. % copper, 1 to 5 wt. % zirconium, 0.5 to 5 wt. % chromium, 0.5 to 2 wt. % nickel, 0.5 to 1.5 wt. % niobium, and 0 to 5 wt. % iron with the proviso that the total content of the alloying metals is 10 to 16% and the total of chromium, nickel, and niobium is at least 1.5%.

Abstract: A method is disclosed for producing fluoronitrobenzene compounds by reacting chloronitrobenzene compounds with a fluoride salt in the presence of a tetramethylammonium salt phase-transfer catalyst. This catalyst allows the use of elevated reaction temperatures with substantial freedom from catalyst inactivation, resulting in yields and reaction rates which are improved over those of previously known methods using higher molecular weight quaternary ammonium salt phase transfer catalysts having more total carbon atoms in their ammonium cations.

Abstract: This invention comprises a process for separating 2,4-dinitrotoluene from a feed mixture comprising 2,4-dinitrotoluene and at least one isomer thereof, which process comprises contacting the mixture at adsorption conditions with an adsorbent comprising an X or Y type zeolite cation exchanged with a cation in the group K, Na, Ca, Ba, Li or Mg, thereby selectively adsorbing the 2,4-dinitrotoluene. The remainder of the feed mixture is removed from the adsorbent and the 2,4-dinitrotoluene is recovered by desorption at desorption conditions with a desorbent material comprising a C.sub.3 to C.sub.5 alcohol, a ketone, toluene, an ester or a nitrocompound.

Abstract: A PTC ceramic composition comprising a fundamental component represented by the formula:(V.sub.1-x A.sub.x).sub.2 O.sub.3wherein x is a value within the range of 0.ltoreq.x.ltoreq.0.02 and A is at least one of Cr and Al, and tin in an amount of 1 to 25 % by weight based on the total weight of the composition, has a small electric resistance in the low resistance state, good PTC properties, and a high density.

Abstract: An improved process is disclosed for preparing fluoronitrobenzene compounds wherein chloronitrobenzene compounds are reacted with potassium fluoride in a solvent dispersion thereof prepared from a mixture including the solvent, the fluoride, methanol and an aromatic compound.

Abstract: Starting from a homogeneous molten bath composed of zinc, mercury and possibly other elements, an alloy powder with substantially homogeneous particles is prepared and that alloy powder is made to react with metallic mercury or with a mercury compound, thereby producing an alloy powder enriched with mercury.

Abstract: An oxide dispersion strengthened cobalt-chromium superalloy produced by mechanical alloying containing a refractory oxide, preferably yttrium oxide, and characterized by excellent corrosion resistance, high fatigue strength and high temperature stability; and prostheses formed from said superalloy.

Abstract: There is provided a composition which comprises (1) a predominantly C.sub.6 -C.sub.12 high-boiling mixture of ketones, ethers, alcohols, esters, and aldehydes and (2) a fatty acid ester, such as sorbitan monooleate. Optionally, it can contain also a polyglycol having an average molecular weight of 3,800 or higher.There is provided also a method for defoaming an aqueous fluid system and preventing the formation of foam in said system, which method comprises adding to said system an effective defoaming and antifoaming amount of the aforesaid composition.

Abstract: Aromatic compounds are nitrated in the vapor phase via a process comprising contacting the aromatic compounds with a nitrating agent in the presence of a nitration promoting catalyst composition represented by the empirical formula:(M.sup.1.sub.a M.sup.2.sub.b O.sub.c).sub.x (NO.sub.2).sub.ywherein M.sup.1 is at least one element selected from Group 4b of the Periodic Table of the Elements, M.sup.2 is at least one element selected from Group 3b of the Periodic Table of the Elements, a is 1, b is 0 to 20, c is a number taken to satisfy the average valences of M.sup.1 and M.sup.2 in the oxidation states in which they exist in the composition, x is 1, and y is 0 to c.

Abstract: This invention relates to the fabrication of an improved electrode for an electrostatic atomizing device. The electrode consists of metal oxide-metal composite fragments dispersed and bonded in a metallic matrix. The composite fragments contain submicron metallic fibers uniformally arrayed in a nonconducting (insulating) matrix. The electrostatic atomizing device includes a cell having a chamber disposed therein, a discharge spray means in communication with the cell, at least two electrodes disposed in the chamber and being in liquid contact with the liquid in the chamber, the liquid in the chamber being transported to the discharge spray means and atomized into droplets, and a mechanism for generating by means of the electrodes, a charge through the liquid within the chamber, wherein the charge enamating from the improved electrode is sufficient to generate free excess charge in the liquid within the chamber, and the liquid is atomized into droplets.

Abstract: A synergistic, aqueous, free flowing defoaming composition comprising as the primary component an aqueous hydrophobic dispersion of an alcohol of 14-28 carbon atoms, a fatty acid of 14-28 carbon atoms, a soap of a fatty acid of 14-28 carbon atoms and a nonionic or anionic surfactant, and as a secondary component a dispersion of a hydrophobic solid in a water insoluble liquid.

Abstract: A composition of matter having a Rockwell A hardness of at least 85 is formed from a precursor mixture comprising between 3 and 10 weight percent boron carbide and the remainder a metal mixture comprising from 70 to 90 percent tungsten or molybdenum, with the remainder of the metal mixture comprising nickel and iron or a mixture thereof. The composition has a relatively low density of between 7 to 14 g/cc. The precursor is preferably hot pressed to yield a composition having greater than 100% of theoretical density.

Abstract: Novel demulsifier compositions, their method of preparation and use as demulsifiers are described. The novel demulsifiers comprise the partially condensed reaction product of a blend of at least two oxyalkylated materials with a vinyl monomer. The demulsifiers are useful in the resolution of water-in-oil emulsions.

Abstract: The invention concerns the manufacture of nitromethane by nitration of mene in a homogeneous gaseous phase, the nitrating agent being nitric acid, nitrogen peroxide or mixtures thereof. According to the disclosed process, the molar ratio methane/nitrating agent is between 0.1 and 5; the reaction contact time between 0.1 and 120 seconds; the reaction pressure between 1 and 35 bars; the temperature between 270.degree. and 600.degree. C. The nitration is carried out in the presence of an active agent of the halogen or derivative type introduced in a molar ratio at the most equal to 3. An installation is disclosed for industrially manufacturing nitromethane.

Abstract: A process for the manufacture of 2,2', 4,4', 6,6-hexanitrostilbene (HNS) from dipicrylethane (DPE) or trinitrotoluene (TNT) which consists of oxidizing DPE or TNE substrate in the presence of an aprotic solvent and a basic salt of a carboxylic acid. The acid preferably consists of an ammonium or an alkali metal salt of a monocarboxylic or a dicarboxylic acid. The reaction step consists of heating the substrate and salt dissolved in the solvent to between 15.degree. and 50.degree. C., and contacting the reaction mixture with dry air or oxygen for up to 2 hours. The HNS product is precipitated out by quenching the reaction mixture in acidified water, and is optionally purified by washing first in methanol and then in acetone.

Abstract: A new high density composition of matter, 1,1'-dinitro-3,3'-azo-1,2,4-triazole, has been synthesized using inexpensive, commonly available compounds. This compound has been found to be an explosive, and its use as a propellant is anticipated.

Abstract: The present invention aims to provide a sliding member: to be operated under a high load and high sliding speed; having high impact resistance and high break-in property; to be highly resistant and stable under boundary lubricating conditions, and; to be engaged with the swash plate made of iron or aluminum in a swash plate type compressor. The sliding member of the present invention comprises:a base comprising an iron-based alloy; anda bearing layer, consolidated with the base by fusion and formed by applying on said base a powder coating having a thickness of not more than 0.5 mm, and then baking said coating, said powder consisting of an iron family element and an additive component which includes from 3 to 30% by weight of boron.

Abstract: A novel composite target material that is composed of a rare earth metal and a transition metal (iron-group metal) and which is used in the formation of a thin magnetooptical recording film by sputtering is disclosed. Also disclosed is a process for producing such composite target material.The process comprises the steps of providing a rare earth metal and an iron-group transition metal as separate entities, mixing these metals without alloying, and hot-forming the mixture at a temperature lower than the eutectic point of the system of metallic components in the mixture, thereby forming an intermetallic compound at the interface between the rare earth metal and the transition metal while causing said metals to be bonded together.The target material produced by this process contains 30-50 wt % of the rare earth metal, with the balance being made of the iron-group transition metal and incidental impurities.