Abstract: A process for the efficient and cost-effective preparation of graphene from a natural source of carbon, resulting from the combination of mild, natural acids, including citric and acetic acids, with sonic frequency, as well as the use of magnets, to exfoliate graphene nanoplatelets from the natural carbon source. The natural carbon source, referred to as Biochar, can be any organic matter based and converted via pyrolytic and/or gasification means. The process includes tuning the frequency of sound energy to maximize the rate of exfoliation to a resonant frequency with the feed material itself, with a range anywhere between 1 Hz-1 THz. The use of magnets, including ferrous magnets, applies electromagnetic pressure on the as yet exfoliated Biochar fragments, which moves the fragments into the field of sound energy. The resonant exfoliation process that takes place within the bath itself, results in the hexagonal structure needed to produce graphene.

Abstract: A device for converting a carbon pill into graphene is provided including a space between at least two electrically conductive surfaces, wherein the electrically conductive surfaces are configured to support a carbon pill in the space. The device also includes at least two electrodes electrically coupled to the at least two electrically conductive surfaces. The device also includes a power supply connected to the electrodes for passing a current through the electrodes to convert the carbon pill into graphene. A carbon pill for graphene conversion is also provided including a first carbon material for synthesizing to graphene by joule heating. The first carbon material is compressed from a powder form into a pill form. The carbon pill includes a second material for at least one of binding the first carbon material from a powder form into a pill form and improving conductivity of the first carbon material.

Abstract: Carbon nanotube foams are provided which comprise tubes substantially aligned longitudinally in a first direction, wherein: each tube defines an outer wall and an inner wall, and each tube comprises an entangled bundle of carbon nanotubes substantially aligned longitudinally in the first direction; and tubes in at least a subset of the tubes are positioned with respect to each other to form one or more first hexagonal units, wherein each first hexagonal unit comprises first-hexagonal-unit tubes, wherein the first-hexagonal-unit tubes comprise six peripheral first-hexagonal-unit tubes and a central first-hexagonal-unit tube, wherein the six peripheral first-hexagonal-unit tubes surround the central first-hexagonal-unit tube in a juxtaposed, hexagonal configuration. Articles of manufacture, e.g., helmets, comprising the foams are also provided which are configured to cover at least a portion of an object, e.g.

Abstract: A method for the solidification and packaging of waste is provided. The method includes providing a container and solidification materials, mixing the solidification materials, and inserting the solidification materials into the container at a first site location. The method also includes transporting the container having the solidification materials to a second site location, providing waste materials at the second site location, inserting waste materials into the container at the second location, and mixing the waste materials and the solidification materials in the container at the second site location. The first site location is not located on-site at a nuclear facility, and the second site location is located on-site at a nuclear facility.

Abstract: A polycrystalline composite comprising diamond particles and non-diamond carbon, wherein: the sum of the content Vd of the diamond particles and the content Vg of the non-diamond carbon is more than 99% by volume based on the total volume of the polycrystalline composite; the median diameter d50 of the diamond particles is 10 nm or more and 200 nm or less; the dislocation density of the diamond particles is 1.0×1013 m?2 or more and 1.0×1016 m?2 or less; and the content Vd of the diamond particles and the content Vg of the non-diamond carbon satisfy the relationship represented by the formula 1:0.01<Vg/(Vd+Vg)?0.5 Formula 1.

Abstract: The disclosure relates to modified multi-walled carbon nanotubes (MWCNTs) that include MWCNTs with carboxylate moieties (e.g., laurate moieties) covalently bonded thereto, and related methods.

Abstract: A porous carbon material which is a single porous carbon material having micropores, mesopores and macropores, wherein, with respect to a total pore volume, the volume percentage of the micropores is 13 to 74 volume %, the volume percentage of the mesopores is 13 to 75 volumes, and the volume percentage of the macropores is 5 to 74 volume %.

Abstract: A method for recovering hafnium and impurity metals from a hafnium-containing waste residue, comprises dissolving the waste residue in sulfuric acid and ammonium sulfate to obtain an acidic solution, adjusting acidity of the acidic solution, and adding a complexing agent to obtain a material solution; conducting extraction to obtain a hafnium-loaded organic phase and an impurity metal ions-containing aqueous phase; subjecting the hafnium-loaded organic phase to purification, stripping, precipitation, and filtration, and washing and burning to obtain hafnium oxide; precipitating the impurity metal ions-containing aqueous phase, washing a resulting precipitate to remove the complexing agent; dissolving a resulting precipitates of the impurity metal ions in sulfuric acid, and adjusting acidity of a resulting solution to obtain a solution of the impurity metal ions; extracting the solution of the impurity metal ions to obtain an impurity metal ions-loaded organic phase, purifying and stripping to obtain oxides of

Abstract: A reactor system can include a reactor, including: a first inlet for a first stream including a liquid sulfur including a dissolved hydrogen sulfide, a polysulfide, or a combination thereof. A second inlet can be for a second stream, wherein the second stream can be an oxygen-containing gas with no more than about 2%, by weight nitrogen. A packing can be in contact with a catalyst.

Abstract: A fullerene derivative has a structure of formula (1) or formula (2): wherein Ar is a substituted or unsubstituted aromatic ring, * is a carbon atom at the point of attachment to a fullerene core, X is O, S, Se, or Te, and R is an organic group.

Abstract: Compositions and methods directed to the synthesis and use of silicon carbide with, biomedical applications is provided. The method of synthesis includes providing a polydimethysiloxane (PDM'S) substrate, and irradiating at least a portion of the substrate with a laser under conditions sufficient to produce silicon carbide comprising 3C silicon carbide (3C-Si€). The composition can be used to modulate biological activity through electrical, chemical and heat stimuli.

Abstract: Spherical, low surface area precipitated silicas are useful as matting agents in powder coatings. Corresponding matte powder coating compositions and methods of preparing matte powder coatings containing the silicas are provided.

Abstract: A method for recycling a carbon fiber-reinforced resin including a carbon fiber and a matrix resin is provided, and the method includes: a first heating step of heating the carbon fiber-reinforced resin to decompose the matrix resin so as to obtain an intermediate in which the decomposition residue of the matrix resin is adhered to the carbon fiber; an unwinding step of unwinding an intermediate fiber from the intermediate; a second heating step of heating the unwound intermediate fiber to decompose the decomposition residue of the matrix resin adhered to the intermediate fiber so as to obtain a recycled carbon fiber; and a winding step of winding the recycled carbon fiber.

Abstract: A method for preparing carbon black according to the present invention comprises the steps of: pyrolyzing by heating waste tires; separating char in the pyrolyzed material from an iron-containing foreign substance; pulverizing the char into fine particles or fine powder to form carbon black; pelletizing the carbon black; cooling and drying the pelletized carbon black; and packaging the pelletized carbon black, wherein the pyrolyzing step comprises: a primary pyrolysis step of heating waste tires; and a secondary pyrolysis step of heating char and iron in the primary pyrolyzed material, and the heating temperature of the secondary pyrolysis step is higher than the heating temperature of the primary pyrolysis step.

Abstract: Disclosed herein is an apparatus and method for fabrication of large diameter single-walled carbon nanotube films. Advantageously, large diameter single-walled carbon nanotube films may be useful as transparent electrodes with high transparency and lower sheet resistance. In one embodiment, the method includes supplying carrier carbon monoxide and catalyst precursor through a first inlet at a temperature below the reaction temperature of the catalyst precursor; supplying heated carbon monoxide through a second inlet such that the heated carbon monoxide mixes with the carrier carbon monoxide and the catalyst an aerosol; reacting the aerosol in a reaction chamber to form a composite aerosol of single walled carbon nanotubes, metal nanoparticles, carbon monoxide, and carbon dioxide. In this embodiment, the heated carbon monoxide heats the catalyst precursor which reacts with the carbon monoxide to form carbon nanotubes.

Abstract: A method of manufacturing silicon nano-powders and a manufacturing equipment implementing such method. The method according to the invention utilizes a plurality of aluminum powders to react with a silicon tetrahalide into a plurality of silicon nano-powders and an aluminum trihalide to obtain the silicon nano-powders.

Abstract: A silver-doped, nano-porous hydroxyapatite material is provided that can be utilized to capture radioactive iodine, 129I. Methods of using the silver-doped, nano-porous hydroxyapatite material to remove radioactive iodine, and methods of manufacturing the material are also provided.

Abstract: Pitch compositions suitable for spinning may comprise: a pitch having a softening point (SP) below 400° C. and is capable of achieving a radial Hencky strain prior to break of about 0.7 to about 10, at spinning temperature (Ts) ranging from about SP?30° C. to about SP+80° C. Methods for producing a carbon fiber from a pitch composition at a temperature within a spinning temperature (Ts) range may comprise determining a temperature range wherein the maximum radial Hencky strain (?R) lies above a minimum process radial Hencky strain, and wherein the minimum process radial Hencky strain is within a range of about 0.7 to about 10. The spinning temperature (Ts) range may be determined by measuring a maximum radial Hencky strain (?R) prior to break at a series of different temperatures and strain rates. Carbon fiber composites may comprise of the said carbon fiber.

Abstract: A process for converting avocado peels into hard carbon-based anodes for sodium ion batteries and a hard carbon material formed according to that process. The avocado peels are simply washed and dried, and then carbonized using a high temperature conversion step. Electrochemical measurements confirmed the applicability of avocado-derived hard carbon as electrode active materials, with high reversible capacities of 320 mAh/g over 50 cycles at 50 mA/g, good rate performance of 86 mAh/g at 3500 mA/g, and Coulombic efficiencies above 99.9% after 500 cycles.

Abstract: Compositions, systems and methods for using zeolites to eliminate scents and odors are disclosed. The compositions and methods use a zeolite, preferably a dry flowable powder of zeolite, desiccant, and monocalcium phosphate to eliminate scent. Applications of using the compositions and systems are also disclosed, including eliminating human scents and other odors to enhance ability for a hunter, wildlife enthusiast, photographer and the like to access proximity to an animal that is otherwise deterred by scents. Other applications of use are also disclosed.