Abstract: A dispersion of capsules in critical or supercritical carbon dioxide is provided. The capsules include an aqueous solution encapsulated by zeolite-templated carbon particles. Also provided is a method of making a dispersion of aqueous solution capsules. The method includes providing a medium of critical or supercritical carbon dioxide, introducing the aqueous solution into the critical or supercritical carbon dioxide medium, and introducing a zeolite-templated carbon particle into the critical or supercritical carbon dioxide medium. Associated methods of using the disclosed dispersions in hydrocarbon-bearing formations are also provided.
Abstract: A nanocarbon separation device includes a separation tank which is configured to accommodate a dispersion liquid including a nanocarbon, a first electrode that is provided at an upper part in the separation tank, a second electrode that is provided at a lower part in the separation tank, and a partition member that is provided between the first electrode and the second electrode in the separation tank, and the partition member partitions the separation tank into a plurality of regions.
Abstract: High quality flake graphite is produced by methods that include mixing a carbon-containing feedstock with a catalyst to form a feedstock/catalyst mixture, or coating a catalyst with a carbon-containing feedstock, and subjecting the mixture or feedstock-coated catalyst to irradiation with a laser to convert the feedstock into flake graphite in the presence of the catalyst. In some instances, the feedstock is converted to a char by pyrolysis and the char is instead subjected to laser irradiation. The feedstock can be a biomass or a carbonaceous material. The catalyst can be an elemental metal, an alloy, or a combination thereof. In some instances, methods described herein have been found to produce high quality flake graphite in the form of potato shaped agglomerates.
Type:
Grant
Filed:
March 2, 2018
Date of Patent:
July 5, 2022
Assignee:
The George Washington University
Inventors:
Michael J. Wagner, Nathan A. Banek, Dustin T. Abele, Kevin R. McKenzie, Jr.
Abstract: The invention relates to a process for the preparation of a citrate-coated amorphous calcium phosphate nanoparticle which comprises the following steps: 1) providing a first solution of a salt of calcium and a citrate salt wherein the molar ratio of citrate ion to calcium ion is in the range from 1 to 2 thus obtaining a clear first solution; 2) providing a second solution of a salt capable to give phosphate anion and a carbonate salt; 3) mixing together the first and the second solution at a pH in the range from 8 to 11; 4) precipitating the nanoparticle; and 5) drying the nanoparticle obtained from step 4). Preferably and advantageously the invention provides for the addition of a fluoride compound in step 2) for obtaining a fluorine-doped citrate-coated calcium phosphate nanoparticle or a nanoparticle agglomerate. The nanoparticle/nanoparticle agglomerate of the invention has a peculiar superficial area and a diameter that allow to use it as a biomaterial for dentistry application.
Abstract: A method for manufacturing a metallic component including the steps of providing a capsule, which defines at least a portion of the shape of the metallic component, arranging metallic material in the capsule, sealing the capsule, subjecting the capsule to Hot Isostatic Pressing for a predetermined time, at a predetermined pressure and at a predetermined temperature, and optionally, removing the capsule. The metallic material is at least one pre-manufactured coherent body, which pre-manufactured coherent body being made of metallic powder, wherein at least a portion of the metallic powder is consolidated such that the metallic powder is held together into a pre-manufactured coherent body. At least one portion of the pre-manufactured coherent body is manufactured by Additive Manufacturing by subsequently arranging superimposed layers of metallic powder.
Type:
Grant
Filed:
May 28, 2020
Date of Patent:
June 28, 2022
Assignee:
MTC Powder Solutions AB
Inventors:
Tomas Berglund, Rickard Sandberg, Martin Ostlund, Johan Sundstrom
Abstract: Provided herein are graphene nanoribbons with high structural uniformity and low levels of impurities and methods of synthesis thereof. Also provided herein are graphene nanoplatelets of superior structural uniformity and low levels of impurities and methods of synthesis thereof. Further provided herein are mixtures of graphene nanoribbons and graphene nanoplatelets of good structural uniformity and low levels of impurities and methods of synthesis thereof. The method includes, for example, the steps of depositing catalyst on a constantly moving substrate, forming carbon nanotubes on the substrate, separating carbon nanotubes from the substrate, collecting the carbon nanotubes from the surface where the substrate moves continuously and sequentially through the depositing, forming, separating and collecting steps. Further processing steps convert the synthesized carbon nanotubes to graphene nanoribbons, graphene nanoplatelets and mixtures thereof.
Abstract: A facile and scalable method to prepare graphene-based amphiphilic Janus nanosheets with high efficiency utilizing the formation of hydrogen bonding to immobilize graphene oxide (GO) on the surfaces of starch microspheres. After selective functionalization of the exposed surface using alkylamine, amphiphilic Janus nanosheets (AJN) were obtained by releasing the nanosheets from the starch microspheres.
Abstract: The present disclosure is directed to multifunctional conductive wire and methods of making multifunctional conductive wire. According to some aspects, the multifunctional conductive wire disclosed herein can function as a current carrier and as a battery, either for providing or storing power. The multifunctional conductive wires disclosed herein can eliminate the need for heavy metal conductors in various devices while improving power efficiency.
Abstract: A CNT dispersion includes a dispersion medium, and a nanocarbon material containing carbon nanotubes dispersed in the dispersion medium. 98% or more of the nanocarbon material has a length of 1 ?m or more and 105 ?m or less and the nanocarbon material has an average aspect ratio of 100 or more and 20000 or less.
Abstract: Provided is a method of producing isolated graphene sheets, comprising: (a) providing a reacting slurry containing a mixture of particles of a graphite or carbon material and an intercalant and/or an oxidizing agent; (b) providing one or a plurality of flow channels to accommodate the reacting slurry, wherein at least one of the flow channels has an internal wall surface and a volume and an internal wall-to-volume ratio of from 10 to 4,000; (c) moving the reacting slurry continuously or intermittently through at least one or a plurality of flow channels, enabling reactions between the graphite or carbon particles and the intercalant and/or oxidant to occur substantially inside the flow channels to form a graphite intercalation compound (GIC) or oxidized graphite (e.g. graphite oxide) or oxidized carbon material as a precursor material; and (d) converting the precursor material to isolated graphene sheets.
Abstract: The present disclosure provides an apparatus capable of continuously producing carbon nanotubes having high crystallinity, a low residual catalyst content and a high aspect ratio. The apparatus for producing carbon nanotubes includes: a reaction unit configured to synthesize carbon nanotubes (CNTs), a supply unit configured to supply a carbon source to the reaction unit through a supply pipe; and a collection unit configured to collect carbon nanotubes discharged from the reaction unit, wherein the reaction unit may include a chemical vapor deposition reactor.
Type:
Grant
Filed:
July 8, 2020
Date of Patent:
May 17, 2022
Assignee:
KOREA INSTITUTE OF SCIENCE AND TECHNOLOGY
Inventors:
Seung Min Kim, Sung Hyun Lee, Jun Beom Park, Ji Hong Park, Dong Myeong Lee, Sook Young Moon, Hyeon Su Jeong
Abstract: A method for making a solid carbon material comprises: delivering a liquid comprising at least one liquid organic compound into a reaction region of a reactor; delivering a gas comprising at least one gaseous organic compound into the reaction region of the reactor; and inducing a chemical reaction between the at least one liquid organic compound and the at least one gaseous organic compound, wherein: the chemical reaction occurs in the reaction region of the reactor; the solid carbon material is made via the reaction; the solid carbon material is made during the reaction in the form of a dispersion comprising the solid carbon material dispersed in the liquid; and the chemical reaction is a homogeneous reaction comprising homogeneous nucleation of the solid carbon material in the reaction region of the reactor.
Abstract: A method of making a carbon nanotube composite yarn, the method including growing floating carbon nanotubes in a reactor, forming a mat of carbon nanotubes from the floating carbon nanotubes, a deposition step including depositing secondary particles on at least a portion of the mat of carbon nanotubes to provide a carbon nanotube composite mat, and a densification step including densifying the carbon nanotube composite mat to provide a carbon nanotube composite yarn.
Abstract: A method of making an array of aligned hafnium oxide nanotubes is provided. The method includes generating a first reactant gas from a first solution comprising a first hafnium precursor dissolved in a first solvent. Directing the flow of the first reactant gas over a substrate to form a seed layer that comprises particles of hafnium oxide. The method further includes generating a second reactant gas from a second solution comprising a second hafnium precursor dissolved in a second solvent. Directing the flow of the second reactant gas over the seed layer to form the array of aligned hafnium oxide nanotubes substantially perpendicular on a surface of the substrate. A method of using the array of aligned hafnium oxide tubes for detection of toxic gases in a gas sample is also provided.
Type:
Grant
Filed:
August 3, 2021
Date of Patent:
May 3, 2022
Assignee:
King Abdulaziz University
Inventors:
Waleed Elsayed Mahmoud Elsayed, Ahmed Abdullah Salem Al-Ghamdi, Yusuf Abdulaziz Al-Turki
Abstract: A graphite composition is provided. A graphite composition according to one embodiment of the present invention comprises: a graphite composite in which nanoparticles having a catecholamine layer on the surface thereof are fixed on graphite; and graphite of at least one of graphite flakes, spherical graphite, and expanded graphite. According to this, since the graphite composition has a high dispersibility in a substrate of a different material, a composite material thus realized exhibits a uniform heat dissipation performance and can prevent mechanical strength from deteriorating at a specific position. In addition, since the compatibility with the substrate of a different material is excellent and thus the interface property with the substrate is excellent, the realized composite material can exhibit a further improved heat dissipation performance and mechanical strength.
Abstract: Provided is a material that has excellent handleability and processability, and that when used as a support for a different material, enables support of the different material up to an inner part thereof. A carbon sheet contains one or more carbon nanotubes and has a porosity of not less than 5% and not more than 90%. The carbon sheet preferably includes: a porous substrate made from carbon; and the carbon nanotubes, attached to the porous substrate. The carbon nanotubes contained in the carbon sheet are preferably single-walled carbon nanotubes. Moreover, the carbon nanotubes contained in the carbon sheet preferably have a nitrogen adsorption specific surface area of 600 m2/g or more.
Abstract: A graphene nanoribbon precursor having a structural formula represented by a following chemical formula (1), wherein in the following chemical formula (1): n is an integer greater than or equal to 0; X is bromine, iodine or chlorine; and Y is hydrogen or fluorine.
Abstract: Applicability to a composite material with high purity and high strength, and a material requiring high conductivity or high thermal conductivity is enhanced. The present invention relates to a multi-walled carbon nanotube having two or more tubes of a graphene sheet where carbon atoms are arranged in a hexagonal honeycomb form, coaxially, wherein a diameter of an outermost wall based on observation of an image by a transmission electron microscope is 3 nm or more and 15 nm or less, and a length based on observation of an image of a scanning electron microscope is 1.0 mm or more, an aggregate of multi-walled carbon nanotubes and a method for preparing the multi-walled carbon nanotube.
Type:
Grant
Filed:
April 16, 2020
Date of Patent:
April 19, 2022
Assignee:
TPR CO., LTD.
Inventors:
Toshiaki Shimizu, Shinpei Teshima, Yasuhiko Okamura, Yusuke Kawaguchi, Kazuki Otomo, Yuta Koguchi, Katsuhito Suzuki, Yoshio Bando
Abstract: The present invention relates to a system for the production of carbon nanotubes from carbonaceous matter, preferably, plastic waste and solar energy; Method of production.
Type:
Grant
Filed:
June 26, 2018
Date of Patent:
April 12, 2022
Assignee:
UNIVERSIDAD DE CHILE
Inventors:
Francisco Gracia Caroca, Mauricio Morel Escobar, Vania Jocelyn Rojas Fuentes, Gerardo Cabrera Papamija, Nicolas Carvajal
Abstract: A method for making carbon fiber in which the tensile strength of carbon fiber is increased without dehumidifying the ambient air that enters every oxidation oven in a multiple oxidation oven system. A positive effect on tensile strength is provided when ambient air entering only the first oven in a series of oxidation ovens is dehumidified. In addition, the ambient air entering the last oven is not dehumidified when one or more of the preceding oxidation ovens is operated with dehumidified air.
Type:
Grant
Filed:
August 21, 2019
Date of Patent:
April 12, 2022
Assignee:
HEXCEL CORPORATION
Inventors:
Peter Andrew Ferrin, Devon Cadwaladar Todd Thomas