Patents Examined by Edward A. Miller
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Patent number: 6136113Abstract: An improved thermally stable, storage stable gas generating composition characterized by both an increased burning rate and a decreased pressure exponent for producing a clean, nontoxic, substantially ash- and solids-free gas for inflating inflatable structures such as vehicle airbags is provided. Optimum combustion efficiencies and operating pressures are achieved in the improved gas generating composition by adding an effective amount of a copper or copper compound catalyst to a gas generating composition that is preferably a eutectic mixture or solid solution of ammonium nitrate, at least one highly oxygenated fuel, potassium or cesium perchlorate or nitrate and an optional binder.Type: GrantFiled: August 7, 1998Date of Patent: October 24, 2000Assignee: Atlantic Research CorporationInventors: Brian K. Wheatley, James D. Martin, Robert D. Lynch
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Patent number: 6136115Abstract: A process is disclosed for producing prills comprised of ammonium dinitramide The prills can include, if desired, one or more thermal stabilizers, and processing aid(s). Solid particulate ADN is introduced into the top of a melting column, allowed to melt to form pre-prills while passing through a hot-zone ("heated zone") in the prilling column. The pre-prills are allowed to spheridize in the presence of an upwardly blown inert medium which is counter current to the path of the ADN in the prilling column. The flow is designed not to blow the ADN out of the prilling column. The rate of spheridization (prill formation) can, if desired, be accelerated by providing additional cooling, such as refrigeration, to the cooling zone in the prilling column. The ADN prills are suitable for use in propellants.Type: GrantFiled: July 1, 1998Date of Patent: October 24, 2000Assignee: Cordant Technologies Inc.Inventors: Thomas K. Highsmith, Corey S. McLeod, Robert B. Wardle, Roger Hendrickson
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Patent number: 6132536Abstract: An automated propellant blending apparatus and method uses closely metered addition of countersolvent to a binder solution with propellant particles dispersed therein to precisely control binder precipitation and particle aggregation. A profile of binder precipitation versus countersolvent-solvent ratio is established empirically and used in a computer algorithm to establish countersolvent addition parameters near the cloud point for controlling the transition of properties of the binder during agglomeration and finishing of the propellant composition particles. The system is remotely operated by computer for safety, reliability and improved product properties, and also increases product output.Type: GrantFiled: October 7, 1998Date of Patent: October 17, 2000Assignee: The United States of America as represented by the Administrator of the National Aeronautics and Space AdministrationInventors: Carl W. Hohmann, Douglas W. Harrington, Maureen L. Dutton, Billy Charles Tipton, Jr., James W. Bacak, Frank Salazar
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Patent number: 6123359Abstract: The present invention relates to an inflator for a vehicle airbag employing non-azide gas generants. The invention also relates to a new filter system for airbag inflators. The filter is a metal ribbon coiled within the inflator house. The metal ribbon comprises at least one segment of apertures and a segment of expanded metal.Type: GrantFiled: July 25, 1998Date of Patent: September 26, 2000Assignee: Breed Automotive Technology, Inc.Inventors: Raul Cabrera, Cezary Grzelczyk
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Patent number: 6123789Abstract: Compositions are provided which, when burned, produce significant levels of infrared radiation, but only limited levels of visible radiation. The basic components of the compositions include a binder, an oxidizer, and a fuel, where the binder also acts the fuel. Preferred oxidizers include those compounds which produce large quantities of infrared radiation when the flare composition is burned. Such oxidizers include potassium nitrate, cesium nitrate, rubidium nitrate, and combinations of these compounds. Selection of the binder is important in order to provide the composition with the desirable characteristics identified above. The binder of the present invention does not produce significant soot. At the same time, the binder serves to form a composition which is processible, avoids chunking, and is compatible with the oxidizers used. It has been found that polymer binders which include relatively short carbon chains (1-6 continuous carbon atoms) are preferred.Type: GrantFiled: February 10, 1995Date of Patent: September 26, 2000Assignee: Cordant Technologies Inc.Inventor: Daniel B. Nielson
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Patent number: 6120058Abstract: An apparatus (10) for inflating an air bag includes a container (12) having a chamber (16) for holding an inert gas and an oxidizer gas under pressure. A body (20) of a combustible material is disposed in the container (12). The body (20) of combustible material comprises a non-metallic nitrogen containing compound, a thermoplastic polymer, and an oxidizer material. The oxidizer material is selected from the group consisting of an alkali metal nitrate, alkali-earth metal nitrate, ammonium perchlorate, alkali metal perchlorate, alkali-earth metal perchlorate, organo-ammonium nitrate, or ammonium dinitramide. An igniter (32) ignites the body (20) of combustible material to generate combustion products that mix with, and heat, the inert gas and the oxidizer gas. The body (20) of combustible material undergoes further combustion upon exposure to the oxidizer gas to yield an inflation fluid comprising the combustion products, the inert gas, and any unreacted oxidizer gas.Type: GrantFiled: August 23, 1996Date of Patent: September 19, 2000Assignee: TRW Vehicle Safety Systems Inc.Inventors: Michael G. Mangum, Jerome W. Emery, David D. Ryder
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Patent number: 6113715Abstract: The invention relates to methods for forming an emulsion explosive composition and to methods for sensitizing an emulsion explosive composition. The methods involve the in-situ expansion of organic microspheres during the formation of the emulsion explosive composition.Type: GrantFiled: July 9, 1998Date of Patent: September 5, 2000Assignee: Dyno Nobel Inc.Inventors: John B. Halander, Kerry S. Atkinson
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Patent number: 6093269Abstract: A pyrotechnic gas generant composition including a high oxygen balance compound or fuel which is the resulting reaction product of aminoguanidine nitrate and nitric acid. Specifically, the resulting reaction product is a yellow precipitate that can be used alone, with or without oxidizers or other additives, for very rapid self-deflagration or in combination with oxidizers and additives. In each instance, the gas generant composition provides both high gas output and low production of solid combustion products. Further, the precipitant is relatively non-hygroscopic and has a high burn rate. Specifically, the gas generating composition is useful as a gas generator for an air bag of an occupant restraint system for an automobile, gun propellants, inflation and expulsion devices, flotation devices, pyrotechnics, fire suppression devices and smokeless, reduced smoke and smokey rocket propellants.Type: GrantFiled: December 18, 1997Date of Patent: July 25, 2000Assignee: Atlantic Research CorporationInventors: Norman H. Lundstrom, Aaron J. Greso, Robert S. Scheffee
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Patent number: 6087267Abstract: A process for selectively plasma etching polycrystalline silicon or polysilicon in preference to silicon dioxide which minimizes the detrimental effect of carbon. It has been discovered that carbon from the plasma etch chemicals or from photoresist present interferes disadvantageously with the selective plasma etch of polysilicon as opposed to silicon dioxide. By heat treating and deep ultraviolet light treating the photoresist prior to the plasma etch step and by using non-carbon etch chemicals, this detrimental carbon effect can be reduced.Type: GrantFiled: March 4, 1986Date of Patent: July 11, 2000Assignee: Motorola, Inc.Inventors: Jasper W. Dockrey, Patrick K. Thomas, Dennis C. Hartman
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Patent number: 6073438Abstract: A eutectic solution of ammonium nitrate and either aminoguanidiine nitrate (AGN) or guanidine nitrate (AN) in the form of a present pellet is used to generate a particulate-free, non-toxic, odorless and colorless gas that is useful wherever an immediate source of such gas is required, such as the inflation of an occupant restraint air bag. The use of the material in the form of a eutectic totally eliminates pellet cracking. Moreover, the addition of a minor amount of potassium nitrate to the eutectic solution eliminates the ammonium nitrate phase change due to temperature cycling without adversely affecting the pressed pellets' freedom from cracking due to said temperature cycling.Type: GrantFiled: February 10, 1998Date of Patent: June 13, 2000Assignee: Atlantic Research CorporationInventors: Robert S. Scheffee, Brian K. Wheatley
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Patent number: 6071364Abstract: Gas generating compositions are formed from a fuel, one or more oxidizers and mica. The gas generant composition of this invention yields solid combustion products and inflating gases having a reduced content of undesirable gases such as NO.sub.x and CO.Type: GrantFiled: February 19, 1997Date of Patent: June 6, 2000Assignee: Breed Automotive Technology, Inc.Inventors: J B Canterberry, Samuel Steven Schlueter, John Herman Adams, Robert Keith Walsh
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Patent number: 6066214Abstract: A solid propellant composition includes an oxidizer, a fuel and a binder, the oxidizer containing a significant amount of bismuth oxide (Bi.sub.2 O.sub.Type: GrantFiled: October 30, 1998Date of Patent: May 23, 2000Assignee: Alliant Techsystems Inc.Inventor: Theodore F. Comfort
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Patent number: 6059906Abstract: The present invention is directed to an age-stabilized and/or strengthened ammonium nitrate propellant composition wherein the strengthening agent is selected from the group consisting of azodicarbonamide, dicyandiamide, oxamide and mixtures thereof and wherein the age-stabilizing agent is a molecular sieve having a pore size of 13 angstroms or less.Type: GrantFiled: December 19, 1997Date of Patent: May 9, 2000Assignee: Universal Propulsion Company, Inc.Inventors: Wayne C. Fleming, Hugh J. McSpadden, Donald E. Olander
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Patent number: 6051087Abstract: A formulation is provided which is capable of performing as a liner layer between a rocket motor casing and the propellant grain disposed within the interior of the rocket motor casing. The composition produces relatively little smoke during the operation of the rocket motor and is capable of securely bonding a wide range of conventional propellants to a wide range of conventional casings. In one preferred formulation, the liner consists of from from about 50% to about 75% oxygen containing polymer; from about 3% to about 15% curing agent; from about 5% to about 50% filler and from about 0.01% to about 0.5% cure catalyst.Type: GrantFiled: December 16, 1992Date of Patent: April 18, 2000Assignee: Cordant Technologies Inc.Inventors: Dale E. Hutchens, Norman Cohen
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Patent number: 6042664Abstract: The present invention relates to a pyrotechnical, aerosol-forming composition for the purpose of extinguishing fires in confined spaces, containing potassium nitrate in a quantity of 67-72% by mass, phenolformaldehyde resin in a quantity of 8-12% by mass and dicyandiamide as the balance, wherein the particles of the potassium nitrate comprise a maximum average diameter of 25 .mu.m, the particles of the phenolformaldehyde resin comprise a maximum average diameter of 100 .mu.m and the particles of the dicyandiamide comprise a maximum average diameter of 15 .mu.m.A further object of the invention is a method for the preparation of the composition, which can be manufactured in conventional installations, by preparing a phenolformaldehyde solution using a mixture of ethyl alcohol with acetone in a ratio of 30-50:70-50 and by mixing and subsequently granulating during the drying process at 20-70.degree. C. The drying process is preferably performed at 40.degree. C. by means of circulating air.Type: GrantFiled: July 21, 1998Date of Patent: March 28, 2000Assignee: R-Amtech International, Inc.Inventors: Valeriy Nikolaevitch Kozyrev, Valeriy Nilovitch Yemelyanov, Alexey Ivanovitch Sidorov, Vladimir Andreevitch Andreev
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Patent number: 6039819Abstract: A solid propellant composition comprising an organic polymer fuel binder, an inorganic perchlorate oxidizer salt, ferrocenyl phosphine or phosphine oxide derivatives and in particular, triferrocenyl phosphine oxide, which function as stable solid combustion modifiers.Type: GrantFiled: March 4, 1982Date of Patent: March 21, 2000Assignee: Atlantic Research CorporationInventors: Charles E. Harrod, William D. Stephens
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Patent number: 6036894Abstract: This invention relates to the manufacture of composite propellants containing rubbery binders and particulate non-binder ingredients. The process consists of curing a mixture of a functionally-terminated hydro-carbon prepolymer and a cross-linking agent to form a viscoelastic first binder composition, mixing the binder with non-binder ingredients to form a plastic propellant, and rubberising at least a part of the plastic propellant by adding to it a further quantity of the cross-linking agent, provided the propellant is formed into a propellant charge while still in a plastic state. The further quantity of the cross-linking agent may be mixed in with the plastic propellant prior to forming, or applied to the surface of the plastic propellant after having been formed into a charge.In a preferred embodiment of the invention, the prepolymer consists of an hydroxy-terminated polybutadiene having a molecular weight of about 3000 and a functionally of about 2.Type: GrantFiled: May 27, 1983Date of Patent: March 14, 2000Assignee: The Secretary of State for Defence in her Brittanic Majesty's Government of the United Kingdom of Great Britain and Northern Ireland.Inventors: Robert James Brown, Ernest Melville Guthrie Cooke, Graham James Spickernell, Arthur Ronald Treadgold, Bernard George Tucker
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Patent number: 6033500Abstract: The present invention is directed to an airbag explosive composition comprising a fuel ingredient, an oxidizing agent and a binder for binding them, said binder being hydrotalcite group expressed by the following general formula (1), and a producing method therefor:[M.sup.2+.sub.1-x M.sup.3+.sub.x (OH).sub.2 ].sup.x+ [A.sup.n-.sub.x/n. mH.sub.2 O].sup.x- (1)whereM.sup.2+ represents a bivalent metal such as Mg.sup.2+, Mn.sup.2+, Fe.sup.2+, Co.sup.2+, Ni.sup.2+, Cu.sup.2+ and Zn.sup.2+ ;M.sup.3+ represents a trivalent metal such as Al.sup.3+, Fe.sup.3+, Cr.sup.3+, Co.sup.3+ and In.sup.3+ ;A.sup.n- represents an n-valence anion such as OH.sup.-, F.sup.-, Cl.sup.-, NO.sub.3.sup.-, C0.sub.3.sup.2-, SO.sub.4.sup.2-, Fe(CN).sub.6.sup.3-, CH.sub.3 COO.sup.-, oxalate ion and salicylate ion; and0<x.ltoreq.0.33.Type: GrantFiled: January 27, 1998Date of Patent: March 7, 2000Assignees: Sensor Technology Co., Ltd., Nippon Kayaku Kabushiki-KaishaInventors: Yuji Ito, Eishi Sato, Akihiko Tanaka, Makoto Iwasaki, Kenjiro Ikeda, Eri Oishi, Ryo Minoguchi, Eiichiro Yoshikawa, Akihiko Kuroiwa
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Patent number: 6032410Abstract: A sod comprising a root support matrix that itself comprises a mixture of soil and/or sand, and shredded carpet fragments, wherein the shredded carpet fragments are from about one-tenth percent (0.1%) to about five percent (5.0%) by weight of the matrix; and a plurality of plants growing in said root support matrix, said plants having roots entangled with said shredded carpet fragments. The shredded carpet fragments comprise a mass of entangled face yarns some of which yarns have bits of carpet backing material attached thereto, wherein at least about ninety percent (90%), and more preferably at least about ninety-five percent (95%), of the bits of carpet backing material have no one dimension greater than about one-quarter (0.25) inch.Type: GrantFiled: January 28, 1997Date of Patent: March 7, 2000Assignee: E. I. du Pont de Nemours and CompanyInventor: Vijayendra Kumar
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Patent number: 6026749Abstract: A combustion inhibiting composition for use in conjunction with a solid, gas-generating charge, the composition comprising an organic polymeric material containing an oxygen-containing organic filler compatible with said polymeric material, the oxygen to carbon atom ratio of the composition being at least 1:3.Type: GrantFiled: February 3, 1978Date of Patent: February 22, 2000Assignee: Imperial Metal Industries (KYNOCH) LimitedInventors: Stuart Gordon, Geoffrey Ian Evans