Abstract: [Object] An object of the present invention is to provide a high-aspect-ratio plate-like alumina particle having low aggregability and high dispersibility and a method for producing the particle. [Solving Means] The above problem is solved by providing a plate-like alumina particle including a step of firing an aluminum compound in the presence of a shape-controlling agent and a molybdenum compound serving as a fluxing agent. The above problem is solved also by providing a method for producing a plate-like alumina particle, the method including a step in which the aluminum compound and the molybdenum compound react with each other to form aluminum molybdate and a step in which the aluminum molybdate is decomposed to obtain the plate-like alumina particle.
Abstract: A method of producing new hydrophobic aluminas by i) providing a slurry comprising an alumina compound, the slurry having a pH of above 5.5; ii) mixing an organic composition comprising carboxylic acids with long hydrocarbon chains with the slurry to form an acid modified slurry; iii) hydrothermally conditioning the acid modified slurry to form a hydrothermally aged slurry; and iv) drying the hydrothermally aged slurry. The new hydrophobic aluminas have surface modified structures distinguished by a low humidity content and very small nanoparticles. These new hydrophobic aluminas can be uniformly dispersed in a substrate, for example polymers.
Abstract: A preprocessing method comprises a sintering step of heating a solid material container filled with a solid material using a temperature which is lower than either the melting point or sublimation of the solid material, whichever is lower, and crystallizing at least part of the solid material, and an impurity removal step of heating the solid material container filled with the solid material using a temperature which is lower than either the melting point or sublimation of the solid material, whichever is lower, and removing at least part of the impurities included in the solid material.
Type:
Grant
Filed:
December 6, 2018
Date of Patent:
November 7, 2023
Assignees:
L'Air Liquide, Societe Anonyme Pour L'Etude Et L'Exploitation des Procedes Georges Claude, American Air Liquide, Inc.
Inventors:
Kohei Tarutani, Jean-Marc Girard, Nicolas Blasco, Stefan Wiese, Guillaume Husson
Abstract: A packed bed catalyst in a pressurized vessel/reactor during contact with a dioxide species precursor enhances catalytic conversion of the precursor to the dioxide species, compared with the same catalytic conversion performed in a non-pressurized vessel/reactor.
Type:
Grant
Filed:
October 5, 2021
Date of Patent:
October 31, 2023
Assignee:
DRIPPING WET WATER, INC.
Inventors:
Richard Sampson, Allison Sampson, James Andrew Mialkowski, Mauricio Mata Nieto
Abstract: Methods for modifying a catalyst system component are disclosed in which a feed mixture containing a fluid and from 1 to 15 wt. % of a catalyst system component is introduced into an inlet of a hydrocyclone, an overflow stream containing from 0.1 to 5 wt. % solids and an underflow stream containing from 10 to 40 wt. % solids are discharged from the hydrocyclone, and the underflow stream is spray dried to form a modified catalyst component. Often, from 4 to 20 wt. % of the catalyst system component in the feed mixture has a particle size of less than or equal to 20 ?m, or less than or equal to 10 ?m.
Type:
Grant
Filed:
September 12, 2022
Date of Patent:
October 31, 2023
Assignee:
Chevron Phillips Chemical Company LP
Inventors:
Mark Scott, Evan Merk, Carlos A. Cruz, Mitchell D. Refvik, Max P. McDaniel
Abstract: A method of making NiO nanoparticles is described, as well as a method of using NiO nanoparticles as an electrocatalyst component to a porous carbon electrode. The carbon electrode may be made of carbonized filter paper. Together, this carbon-supported NiO electrode may be used for water electrolysis. Using a pamoic acid salt in the NiO nanoparticle synthesis leads to smaller and monodisperse nanoparticles, which support higher current densities.
Type:
Grant
Filed:
February 23, 2018
Date of Patent:
October 24, 2023
Assignee:
King Fahd University of Petroleum and Minerals
Inventors:
Md. Abdul Aziz, Mohammed Ameeh Ahmed Qasem
Abstract: A ceramic and a method of forming a ceramic including milling steel slag exhibiting a diameter of 5 mm of less to form powder, sieving the powder to retain the powder having a particle size in the range of 20 to 400 removing free iron from the powder with a magnet, heat treating the powder at a temperature in the range of 700° C. to 1200° C. for a time period in the range of 1 hour to 10 hours and oxidizing retained iron in the powder, compacting the powder at a compression pressure in the range of 20 MPa to 300 MPA, and sintering the powder at a temperature in the range of 700° C. to 1400° C. for a time period in the range of 0.5 hours to 4 hours to provide a ceramic.
Type:
Grant
Filed:
February 22, 2018
Date of Patent:
October 17, 2023
Assignee:
KHALIFA UNIVERSITY OF SCIENCE AND TECHNOLOGY
Inventors:
Nicolas Jean-Michel Calvet, Uver Dario Villalobos Cardozo, Khaloud Mohammed Al Na'Imi, Jean Francois Hoffmann
Abstract: A method for producing an aerogel composite includes drying a wet gel generated from a sol comprising a silica particles, and at least one selected from the group consisting of a silicon compound having a hydrolyzable functional group in a molecule, and a hydrolysis product of the silicon compound.
Abstract: The present invention relates to catalyst compositions containing a mixed oxide catalyst of formula (I) or formula (II) as described herein, their preparation, and their use in a process for ammoxidation of various organic compounds to their corresponding nitriles and to the selective catalytic oxidation of excess NH3 present in effluent gas streams to N2 and/or NOx.
Inventors:
Yawu T. Chi, Scott G. Moffatt, Mikhail Khramov, Ranjeeth Reddy Kalluri, Bruce F. Monzyk, Soundar Ramchandran, Marty Alan Lail, Maruthi Sreekanth Pavani
Abstract: A compound includes indium element (In), gallium element (Ga), aluminum element (Al) and oxygen element (O), the compound having a triclinic crystal system with lattice constants being a=10.07±0.15 ?, b=10.45±0.15 ?, c=11.01±0.15 ?, ?=111.70±0.50°, ?=107.70±0.50° and ?=90.00±0.50°.
Abstract: A multilayer supported oxidative coupling of methane (OCM) catalyst composition (alpha-Al2O3 support, first single oxide layer, one or more mixed oxide layers, optional second single oxide layer) characterized by formula AaZbEcDdOx/alpha-Al2O3; A is alkaline earth metal; Z is first rare earth element; E is second rare earth element; D is redox agent/third rare earth element; the first, second, third rare earth element are not the same; a=1.0; b=0.1-10.0; c=0.1-10.0; d=0-10.0; x balances oxidation states; first single oxide layer (Zb1Ox1, b1=0.1-10.0; x1 balances oxidation states) contacts alpha-Al2O3 support and one or more mixed oxide layers; one or more mixed oxide layers (Aa2Zb2Ec2Dd2Ox2, a2=1.0; b2=0.1-10.0; c2=0.1-10.0; d2=0-10.
Type:
Grant
Filed:
September 21, 2020
Date of Patent:
September 12, 2023
Assignee:
SABIC Global Technologies B.V.
Inventors:
Wugeng Liang, Azim Ali, Hector Perez, Jae Hyung Kim, Pankaj Gautam, David West
Abstract: A Si-containing film forming composition comprising a catalyst and/or a polysilane and a N—H free, C-free, and Si-rich perhydropolysilazane having a molecular weight ranging from approximately 332 dalton to approximately 100,000 dalton and comprising N—H free repeating units having the formula [—N(SiH3)x(SiH2-)y], wherein x=0, 1, or 2 and y=0, 1, or 2 with x+y=2; and x=0, 1 or 2 and y=1, 2, or 3 with x+y=3. Also disclosed are synthesis methods and applications for using the same.
Type:
Grant
Filed:
February 21, 2019
Date of Patent:
August 29, 2023
Assignees:
L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude, American Air Liquide, Inc.
Inventors:
Antonio Sanchez, Gennadiy Itov, Manish Khandelwal, Cole Ritter, Peng Zhang, Jean-Marc Girard, Zhiwen Wan, Glenn Kuchenbeiser, David Orban, Sean Kerrigan, Reno Pesaresi, Matthew Damien Stephens, Yang Wang, Guillaume Husson, Grigory Nikiforov
Abstract: A metal chloride generator is provided. The metal chloride generator is a metal chloride centrifugal reactor that can be operated under conditions sufficient to cause metal particles and chlorine in the generator to be brought into contact with one another and react using centrifugal force to form metal chloride. A process for manufacturing titanium dioxide that utilizes the metal chloride generator is also provided.
Abstract: Lanthanide oxides and mixed lanthanide oxides can be produced using furnace or microwave assisted solid-state synthesis. The use of Ln-tri(methylsilyl)amide-based precursors yields spherical nanoparticles. The formation of spherical shaped nanoparticles is likely due to the preferential single-step decomposition of the Ln-TMS as well as the low activation energy to overcome decomposition. Reaction temperature, initial metal ion ratio, and reaction dwell time can be used to control the final nanoparticle size. The method enables solvent-free, high-yield synthesis of morphology-controlled lanthanide oxides.
Type:
Grant
Filed:
July 28, 2021
Date of Patent:
August 8, 2023
Assignee:
National Technology & Engineering Solutions of Sandia, LLC
Inventors:
LaRico Juan Treadwell, Avi Gabriel Bregman, Marissa Ringgold
Abstract: A method of synthesizing copper oxide nanoparticles includes preparing a liquid extract of Rumex vesicarius, dissolving copper salt in the liquid extract to provide a solution with copper nanoparticles, adding a base to the solution with copper nanoparticles to form a precipitate including copper oxide nanoparticles. Copper oxide nanoparticles prepared according to the method are effective photocatalysts for degrading organic dyes and antibacterial agents and exhibit anticancer activities.
Type:
Grant
Filed:
March 23, 2021
Date of Patent:
August 8, 2023
Assignee:
KING SAUD UNIVERSITY
Inventors:
Ali Aldalbahi, Raneem Aldawish, Manal Ahmed Gasmelseed Awad, Noura Saleem Aldosari, Reem Hamad Alshathri, Leen Abdullah Aldwihi, Raghad Alammari, Khloud Ibrahim Bin Shoqiran
Abstract: In one embodiment, a composition of matter includes a crystalline porous structure having a density in a range from about 30 to about 50 mg/cm3. In another embodiment, a kit includes an amorphous, porous material, an inert pressure medium, a heating source, and a sample chamber configured to withstand an applied pressure of at least about 20 GPa. Other aspects and embodiments of the present invention will become apparent from the following detailed description, which, when taken in conjunction with the drawings, illustrate by way of example the principles of the invention.
Type:
Grant
Filed:
October 15, 2019
Date of Patent:
August 8, 2023
Assignee:
Lawrence Livermore National Security, LLC
Inventors:
Peter J. Pauzauskie, Jonathan C. Crowhurst, Marcus A. Worsley, Joe H. Satcher, Jr.
Abstract: A field of thermal treatment of ceramic materials is provided, and relates to a method for thermal treatment of a solid ceramic part in a microwave cavity, the direction of the electrical field E being substantially uniform in an empty cavity, comprising the steps that consist of placing, in the cavity, at least one ceramic part surrounded by at least one first susceptor with dimensions, material and arrangement configured to emit infrared radiation, each first susceptor including at least one first main surface, each first main surface being an adjusted surface in which the cone distances are parallel to the electrical field E, and of emitting the microwaves into the cavity.
Type:
Grant
Filed:
October 20, 2017
Date of Patent:
August 1, 2023
Assignees:
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE, UNIVERSITE DE CAEN NORMANDIE, ECOLE NATIONALE SUPERIEURE D'INGENIEURS CAEN, UNIVERSITE POLYTECHNIQUE HAUTS-DE-FRANCE, ASSOCIATION POUR LA RECHERCHE ET LE DEVELOPPEMENT DE METHODES ET PROCESSUS INDUSTRIELS-ARMINES
Abstract: Disclosed herein is a fungicide, including a porous carbon material and a silver member adhered to the porous carbon material, wherein a value of a specific surface area based on a nitrogen BET, namely Brunauer, Emmett, and Teller method is equal to or larger than 10 m2/g, and a volume of a fine pore based on a BJH, namely Barrett, Joyner, and Halenda method and an MP, namely Micro Pore method is equal to or larger than 0.1 cm3/g.
Abstract: A process for producing a particulate TiO2 includes supplementing metatitanic acid with an alkali compound in a quantity of 1200 ppm to 2400 ppm of alkali, with a phosphorus compound in a quantity of 0.1 wt.-% to 0.3 wt.-% by weight of P, expressed as phosphorus, and with an aluminum compound in a quantity of 1 ppm to 1000 ppm of Al, expressed as Al, to obtain a mixture. The quantity of the alkali compound, of the phosphorus compound, and of the aluminum compound are with respect to the TiO2 content. The mixture is calcined at a constant temperature of 940° C. to 1020° C. until a numerical fraction X50 of TiO2 has a primary crystallite size of at least 200 nm, to obtain a calcined mixture. The calcined mixture is cooled to obtain a cooled calcined mixture. The cooled calcined mixture is grinded to obtain the particulate TiO2.