Patents Examined by Lynne Edmondson
  • Patent number: 9607741
    Abstract: The present invention relates to ferrite particles for bonded magnet, having a volume-average particle diameter of 2.1 to 2.7 ?m and a particle diameter ×90 of 4.3 to 5.4 ?m wherein the ×90 represents a particle diameter at which a cumulative percentage of particles under sieve (undersize particles) based on a volume thereof is 90%, when determined from a particle size distribution thereof measured by using a laser diffraction type particle size distribution measuring apparatus.
    Type: Grant
    Filed: April 18, 2014
    Date of Patent: March 28, 2017
    Assignee: TODA KOGYO CORPORATION
    Inventors: Yasuhiko Fujii, Minoru Ohsugi, Yasushi Nishio, Yosuke Koyama, Shigeru Takaragi
  • Patent number: 9598636
    Abstract: A red phosphor in the form of a Mn-activated complex fluoride having the formula: A2MF6:Mn wherein M is one or more tetravalent elements selected from Si, Ti, Zr, Hf, Ge, and Sn, and A is one or more alkali metals selected from Li, Na, K, Rb, and Cs, and contains at least Na and/or K, is surface treated with a treating solution containing a surface treating agent selected from an organic amine, quaternary ammonium salt, alkyl betaine or fluorochemical surfactant, alkoxysilane, and fluorinated polymer.
    Type: Grant
    Filed: December 20, 2013
    Date of Patent: March 21, 2017
    Assignee: SHIN-ETSU CHEMICAL CO., LTD.
    Inventors: Masami Kaneyoshi, Masatoshi Ishii
  • Patent number: 9598635
    Abstract: A method for the photo-mediated phase transfer of inorganic nanocrystals, such as luminescent quantum dots, QDs, is provided. Irradiation, specifically UV excitation (?ex<400 nm), promotes the in-situ ligand exchange of hydrophobic quantum dots with hydrophilic ligands and their facile transfer to polar solvents and buffer media. The technique enables transfer of quantum dots and other nanocrystal materials from hydrophobic to polar and hydrophilic solutions.
    Type: Grant
    Filed: May 7, 2013
    Date of Patent: March 21, 2017
    Assignee: The Florida State University Research Foundation, Inc.
    Inventors: Hedi Mattoussi, Igor Alabugin, Goutam Palui, Tommaso Avellini
  • Patent number: 9592555
    Abstract: A continuous flow reactor for the efficient synthesis of nanoparticles with a high degree of crystallinity, uniform particle size, and homogenous stoichiometry throughout the crystal is described. Disclosed embodiments include a flow reactor with an energy source for rapid nucleation of the procurors following by a separate heating source for growing the nucleates. Segmented flow may be provided to facilitate mixing and uniform energy absorption of the precursors, and post production quality testing in communication with a control system allow automatic real-time adjustment of the production parameters. The nucleation energy source can be monomodal, multimodal, or multivariable frequency microwave energy and tuned to allow different precursors to nucleate at substantially the same time thereby resulting in a substantially homogenous nanoparticle. A shell application system may also be provided to allow one or more shell layers to be formed onto each nanoparticle.
    Type: Grant
    Filed: March 14, 2014
    Date of Patent: March 14, 2017
    Assignee: Shoei Electronic Materials, Inc.
    Inventors: David M. Schut, Thomas E. Novet, George M. Williams
  • Patent number: 9586867
    Abstract: CaF2 translucent ceramics includes at least two rare earth elements selected from a group consisting of La, Pr, Nd, Sm, Eu, Tb, Dy, Ho, Er, Tm, Yb, and Lu.
    Type: Grant
    Filed: May 5, 2014
    Date of Patent: March 7, 2017
    Assignee: NIKON CORPORATION
    Inventor: Hitoshi Ishizawa
  • Patent number: 9580648
    Abstract: A color stable Mn4+ doped phosphor of formula I, Ax[MFy]:Mn4+??I wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7; and wherein % intensity loss of the phosphor after exposure to light flux of at least 80 w/cm2 at a temperature of at least 50° C. for at least 21 hours is ?4%.
    Type: Grant
    Filed: May 23, 2014
    Date of Patent: February 28, 2017
    Assignee: General Electric Company
    Inventors: James Edward Murphy, Anant Achyut Setlur, Florencio Garcia, Robert Joseph Lyons, Ashfaqul Islam Chowdhury, Nagaveni Karkada, Prasanth Kumar Nammalwar
  • Patent number: 9583272
    Abstract: The present invention aims to provide an electrolyte solution for electrochemical devices, which has excellent thermal stability and high decomposition voltage and produces a small amount of evaporation at high temperatures. The present invention also aims to provide an aluminum electrolytic capacitor and an electric double layer capacitor, both of which include the electrolyte solution for electrochemical devices. The present invention relates to an electrolyte solution for electrochemical devices, the electrolyte solution including a solvent and an electrolyte, the solvent containing a sulfone compound represented by the formula (1): wherein R represents a C1-6 alkyl group.
    Type: Grant
    Filed: February 8, 2013
    Date of Patent: February 28, 2017
    Assignee: Sumitomo Seika Chemicals Co., Ltd.
    Inventors: Shunji Oyama, Noriko Yamamoto, Naoka Hirabayashi
  • Patent number: 9583129
    Abstract: An aspect of the present invention relates to a method of manufacturing hexagonal ferrite magnetic powder. The method of manufacturing hexagonal ferrite magnetic powder comprises wet processing hexagonal ferrite magnetic particles obtained following acid treatment in a water-based solvent to prepare an aqueous magnetic liquid satisfying relation (1) relative to an isoelectric point of the hexagonal ferrite magnetic particles: pH0?pH*?2.5, wherein, pH0 denotes the isoelectric point of the hexagonal ferrite magnetic particles and pH* denotes a pH of the aqueous magnetic liquid, which is a value of equal to or greater than 2.0, adding a surface-modifying agent comprising an alkyl group and a functional group that becomes an anionic group in the aqueous magnetic liquid to the aqueous magnetic liquid to subject the hexagonal ferrite magnetic particles to a surface-modifying treatment, and removing the water-based solvent following the surface-modifying treatment to obtain hexagonal ferrite magnetic particles.
    Type: Grant
    Filed: August 20, 2014
    Date of Patent: February 28, 2017
    Assignee: FUJIFILM Corporation
    Inventors: Masahiko Mori, Hiroyuki Suzuki
  • Patent number: 9567516
    Abstract: A process for synthesizing a manganese (Mn4+) doped phosphor includes milling particles of the a phosphor precursor of formula I, and contacting the milled particles with a fluorine-containing oxidizing agent at an elevated temperature Ax[MFy]:Mn4+??(I) wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7.
    Type: Grant
    Filed: June 12, 2014
    Date of Patent: February 14, 2017
    Assignee: General Electric Company
    Inventors: James Edward Murphy, Anant Achyut Setlur, Florencio Garcia, Srinivas Prasad Sista
  • Patent number: 9546317
    Abstract: An economic, direct synthetic method for producing water soluble ZnS QDs that are ready for bioconjugation is provided. The method can produce aqueous ZnS QDs with emission wavelengths varying from 400 nm to 700 nm. Highly luminescent metal sulfide (MS) QDs are produced via an aqueous synthesis route. MS QDs are capped with thiol-containing charged molecules in a single step. The resultant MS QDs exhibit the distinctive excitonic photoluminescence desired of QDs and can be fabricated to avoid undesirable broadband emissions at higher wavelengths. The aqueous ZnS QDs are stable in biological fluids over a long period of time. In addition, non-toxic ZnS QDs have been produced with good photoluminescence properties.
    Type: Grant
    Filed: June 18, 2013
    Date of Patent: January 17, 2017
    Assignee: Drexel University
    Inventors: Wei-Heng Shih, Wan Y. Shih, Hui Li
  • Patent number: 9546318
    Abstract: A process for preparing a Mn4+ doped phosphor of formula I Ax[MFy]:Mn+4??I includes contacting a mixture of a compound of formula Ax[MFy], a compound of formula AX, and a Mn+n source comprising a fluoromanganese compound, with a fluorine-containing oxidizing agent in gaseous form, at an elevated temperature, to form the Mn4+ doped phosphor; wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; X is F, Cl, Br, I, HF2, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7; and n is 2, 3, or 4.
    Type: Grant
    Filed: May 1, 2014
    Date of Patent: January 17, 2017
    Assignee: General Electric Company
    Inventors: James Edward Murphy, Robert Joseph Lyons, Anant Achyut Setlur, Jr.
  • Patent number: 9514776
    Abstract: The method of manufacturing hexagonal ferrite magnetic particles includes providing hexagonal ferrite magnetic particles by conducting calcination of particles comprising an iron salt and an alkaline earth metal salt to cause fertilization; and further includes preparing the particles comprising an iron salt and an alkaline earth metal salt by adhering a glass component, followed by the alkaline earth metal salt, to the iron salt; and conducting calcination of the particles prepared to form a calcined product in which hexagonal ferrite is detected as a principal component in X-ray diffraction analysis.
    Type: Grant
    Filed: December 2, 2013
    Date of Patent: December 6, 2016
    Assignee: FUJIFILM Corporation
    Inventors: Yasushi Hattori, Kazufumi Omura
  • Patent number: 9512357
    Abstract: A process for synthesizing a Mn4+ doped phosphor is presented. The process includes contacting a source of Mn4+ ions to a suspension comprising aqueous hydrofluoric acid and a complex fluoride compound of formula (II) in solid form, and then contacting a source of A+ ions to the suspension to form the Mn4+ doped phosphor, Ax[MFy]?? (II) Wherein, A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7.
    Type: Grant
    Filed: July 22, 2014
    Date of Patent: December 6, 2016
    Assignee: General Electric Company
    Inventor: James Edward Murphy
  • Patent number: 9512356
    Abstract: A process for preparing a Mn4+ doped phosphor of formula I Ax[MFy]:Mn+4?? I includes combining in an acidic solution, an A+ cation, an anion of formula MFy, and a Mnn+ source comprising a fluoromanganese compound, precipitating a Mnn+ containing phosphor precursor from the acidic solution, and contacting the Mnn+ containing phosphor precursor with a fluorine-containing oxidizing agent in gaseous form, at an elevated temperature, to form the Mn4+ doped phosphor; wherein A is Li, Na, K, Rb, Cs, or a combination thereof; M is Si, Ge, Sn, Ti, Zr, Al, Ga, In, Sc, Hf, Y, La, Nb, Ta, Bi, Gd, or a combination thereof; x is the absolute value of the charge of the [MFy] ion; y is 5, 6 or 7; and n is 2 or 3.
    Type: Grant
    Filed: May 1, 2014
    Date of Patent: December 6, 2016
    Assignee: General Electric Company
    Inventors: Robert Joseph Lyons, James Edward Murphy, Anant Achyut Setlur, Jr.
  • Patent number: 9512359
    Abstract: The present invention provides a phosphor comprising a europium-activated sialon crystal having a basic composition represented by a formula: (Sr1-x, Eux)?Si?Al?O?N? (1) (wherein x is 0<x<1, ? is 0<??4 and ?, ?, ? and ? are numbers such that converted numerical values when ? is 3 satisfy 9<??15, 1???5, 0.5???3 and 10???30), wherein the phosphor is composed of particles having a sphericity of 0.65 or more and emits green light by being excited by ultraviolet light, violet light or blue light.
    Type: Grant
    Filed: March 15, 2013
    Date of Patent: December 6, 2016
    Assignees: Kabushiki Kaisha Toshiba, Toshiba Materials Co., Ltd.
    Inventors: Daichi Usui, Yasuhiro Shirakawa, Hirofumi Takemura, Tsutomu Ishii
  • Patent number: 9507032
    Abstract: In one embodiment, a material comprises a crystal comprising strontium iodide providing at least 50,000 photons per MeV, where the strontium iodide material is characterized by a volume not less than 1 cm3. In another embodiment, a scintillator optic includes europium-doped strontium iodide providing at least 50,000 photons per MeV, where the europium in the crystal is primarily Eu2+, and the europium is present in an amount greater than about 1.6%. A scintillator radiation detector in yet another embodiment includes a scintillator optic comprising SrI2 and BaI2, where a ratio of SrI2 to BaI2 is in a range of between 0:1 and 1.0, the scintillator optic is a crystal that provides at least 50,000 scintillation photons per MeV and energy resolution of less than about 5% at 662 keV, and the crystal has a volume of 1 cm3 or more; the scintillator optic contains more than about 2% europium.
    Type: Grant
    Filed: October 7, 2013
    Date of Patent: November 29, 2016
    Assignee: Lawrence Livermore National Security, LLC
    Inventors: Stephen A. Payne, Nerine J. Cherepy, Giulia E. Hull, Alexander D. Drobshoff, Arnold Burger
  • Patent number: 9487411
    Abstract: The method of manufacturing magnetic particles, wherein the magnetic particles are magnetic particles for magnetic recording, and includes subjecting starting material magnetic particles to glass component-adhering treatment to be adhered with a glass component, and subjecting the magnetic particles after the glass component-adhering treatment to coercive force-reducing treatment with heating, to provide magnetic particles having lower coercive force than the starting material magnetic particles.
    Type: Grant
    Filed: April 22, 2014
    Date of Patent: November 8, 2016
    Assignee: FUJIFILM Corporation
    Inventor: Yasushi Hattori
  • Patent number: 9478331
    Abstract: An aspect of the present invention relates to a method of manufacturing hexagonal strontium ferrite magnetic powder, which comprises melting a starting material mixture which has a composition, as a composition converted into an oxide, lying within a region enclosed by the following four points: (a) SrO=48.0 mol %, Fe2O3=17.2 mol %, B2O3=34.8 mol %; (b) SrO=55.9 mol %, Fe2O3=17.7 mol %, B2O3=26.4 mol %; (c) SrO=41.7 mol %, Fe2O3=40.9 mol %, B2O3=17.4 mol %; (d) SrO=36.7 mol %, Fe2O3=40.1 mol %, B2O3=23.2 mol %; in a ternary diagram with SrO, Fe2O3, which may include an Fe substitution element, and B2O3 as apexes, to provide a melt, and quenching the melt to obtain a solidified product; and heat treating the solidified product to precipitate hexagonal strontium ferrite magnetic particles within the solidified product.
    Type: Grant
    Filed: March 15, 2013
    Date of Patent: October 25, 2016
    Assignee: FUJIFILM Corporation
    Inventors: Nobuo Yamazaki, Hiroyuki Suzuki
  • Patent number: 9468134
    Abstract: In order to provide a noise suppression sheet whose imaginary part magnetic permeability ??, representing a magnetic loss component, is large at a GHz-band frequency, thus having an excellent noise suppression effect, the noise suppression sheet comprises a flat magnetic powder having a saturation magnetostriction of 12.0×10?6 or more and 38.0×10?6 or less and an organic binder.
    Type: Grant
    Filed: February 20, 2013
    Date of Patent: October 11, 2016
    Assignee: NEC TOKIN CORPORATION
    Inventor: Toshiyuki Igarashi
  • Patent number: 9460850
    Abstract: To provide ferrite magnetic powders for bond magnet capable of surely suppressing residual hexavalent chrome, being an environmental load substance, having no adverse influence on the magnetic characteristics, which is an obstacle in use, and without damaging productivity and at a low cost. The method includes the steps of obtaining sintered powders by sintering raw material powders; wet-pulverizing the sintered powders; wet-cleaning the sintered powders; and annealing the cleaned sintered powders, wherein in the step of the wet-pulverization and in the step of wet-cleaning, generation of the hexavalent chrome, being an environmental load substance, is suppressed by performing the pulverization and cleaning while maintaining pH of a dispersion solvent at 8.5 or less, at the time of pulverization and cleaning.
    Type: Grant
    Filed: April 17, 2014
    Date of Patent: October 4, 2016
    Assignees: DOWA F-TEC CO., LTD., DOWA ELECTRONICS MATERIALS CO., LTD.
    Inventors: Shuichi Kohayashi, Hiroya Ikeda, Hideki Katayama, Keisuke Ayabe