Abstract: A method and apparatus for enrichment of heavy oxygen isotopes is provided wherein an oxygen starting material which contains heavy oxygen isotopes is enriched in at least one of oxygen molecule 16O17O, 16O18O, 17O17O, 17O18O and 18O18O, by means of cryogenic distillation of the oxygen starting material containing heavy oxygen isotopes. In addition, a method and apparatus are provided for further increasing the concentration of at least one of the heavy isotope oxygen molecules by means of conducting isotope scrambling on the above-mentioned plurality of oxygen molecules enriched by means of the above mentioned cryogenic distillation.
Abstract: The invention is a process to recover a high pressure hydrogen-rich gas stream from a purge gas stream taken from a hydrotreater. This purge gas stream is admixed with synthesis gas that was the original source of the hydrogen to form a gaseous mixture. This mixed gas comprising purge gas and synthesis gas is advantageously treated to remove acid gases and possibly other impurities. The mixed gas is then treated to extract a hydrogen-rich gas and a hydrogen-depleted gas using, for example, a membrane. At least a portion of the hydrogen-rich gas is then heated and compressed as necessary and is recycled to the hydrotreater.
Abstract: A method is provided for performing array microcrystallizations to determine suitable crystallization conditions for a molecule. The method comprises forming an array of microcrystallizations, each microcrystallization comprising a drop containing a molecule to be crystallized, the drop having a volume of less than 1 &mgr;L; storing the array of microcrystallizations under conditions suitable for molecule crystals to form in the drops in the array; and detecting molecule crystal formation in the drops.
Type:
Grant
Filed:
June 18, 1999
Date of Patent:
October 2, 2001
Assignee:
The Regents of the University of California
Inventors:
Bernard D. Santarsiero, Raymond C. Stevens, Peter G. Shultz, Joseph M. Jaklevic, Derek T. Yegian, Earl Cornell, Robert A. Nordmeyer, Jian Jin, William F. Kolbe, Arthur L. Jones, Donald C. Uber
Abstract: A metal hydride getter purifier operated at less than 350° C. to remove impurities such as carbon dioxide, carbon monoxide, nitrogen, oxygen and water to levels of the order of one ppb or less from hydrogen without creating greater than 10 ppb methane. A cryogenic stage after the getter stage may be used to ensure removal of methane from hydrogen.