Abstract: A method of forming a polycrystalline diamond cutting element includes assembling a diamond material, a substrate, and a source of catalyst material or infiltrant material distinct from the substrate, the source of catalyst material or infiltrant material being adjacent to the diamond material to form an assembly. The substrate includes an attachment material including a refractory metal. The assembly is subjected to a first high-pressure/high temperature condition to cause the catalyst material or infiltrant material to melt and infiltrate into the diamond material and subjected to a second high-pressure/high temperature condition to cause the attachment material to melt and infiltrate a portion of the infiltrated diamond material to bond the infiltrated diamond material to the substrate.
Type:
Grant
Filed:
November 20, 2015
Date of Patent:
July 23, 2019
Assignee:
SMITH INTERNATIONAL, INC.
Inventors:
Yahua Bao, Fulong Wang, J. Daniel Belnap, Ronald K. Eyre, Yi Fang
Abstract: The present invention relates to a suspension of cerium oxide particles in a liquid phase, in which said particles comprise secondary particles comprising primary particles, and a process for preparing said liquid suspension in which the cerium IV/total cerium molar ratio before precipitation is comprised between 1/10000 and 1/500000 and that the thermal treatment is being carried out under an inert atmosphere.
Abstract: An agglomerate abrasive grain includes a mixture of individual abrasive grains and hollow bodies, wherein the abrasive grains and the hollow bodies are held together via a binding matrix of aluminosilicate and alkali silicate, and the agglomerate abrasive grain has an open porosity and a closed porosity in each case ranging from 5% by volume to 40% by volume, wherein the total porosity of the agglomerate abrasive grain is less than 50% by volume.
Abstract: In an embodiment, a method of fabricating a polycrystalline diamond compact (“PDC”) includes forming a polycrystalline diamond (“PCD”) table in the presence of a metal-solvent catalyst in a first high-pressure/high-temperature (“HPHT”) process. The PCD table includes bonded diamond grains defining interstitial regions, with the metal-solvent catalyst disposed therein. The method includes at least partially leaching the PCD table to remove at least a portion of the metal-solvent catalyst therefrom. The method includes subjecting the at least partially leached PCD table and a substrate to a second HPHT process under diamond-stable temperature-pressure conditions to partially infiltrate the at least partially leached PCD table with an infiltrant. A maximum temperature (T), a total process time (t), and a maximum pressure (P) of the second HPHT process are chosen so that ? is about 2° Celsius·hours/gigapascals (“° C.·h/GPa”) to about 325° C.·h/GPa, with ? represented as ?=T·t/P.
Type:
Grant
Filed:
December 7, 2010
Date of Patent:
June 4, 2019
Assignee:
US SYNTHETIC CORPORATION
Inventors:
Debkumar Mukhopadhyay, Kenneth E. Bertagnolli, Jair J. Gonzalez
Abstract: In an embodiment, a polycrystalline diamond compact includes a substrate, and a polycrystalline diamond (“PCD”) table bonded to the substrate and including an exterior working surface, at least one lateral surface, and a chamfer extending between the exterior working surface and the at least one lateral surface. The PCD table includes bonded diamond grains defining interstitial regions. The PCD table includes a first region adjacent to the substrate and a second leached region adjacent to the first region and extending inwardly from the exterior working surface to a selected depth. At least a portion of the interstitial regions of the first region include an infiltrant disposed therein. The interstitial regions of the second leached region are substantially free of metal-solvent catalyst. The second region is defined by the exterior working surface, the lateral surface, the chamfer, and a generally horizontal boundary located below the chamfer.
Type:
Grant
Filed:
February 11, 2014
Date of Patent:
May 28, 2019
Assignee:
US SYNTHETIC CORPORATION
Inventors:
Debkumar Mukhopadhyay, Kenneth E. Bertagnolli, Jair J. Gonzalez
Abstract: Disclosed is an ultrafine abrasive biopolymer soft polishing film having a base material, the base material including a high polymer base material formed by crosslinking, solidifying and drying a uniform mixture that include from 0.1-10 wt % of an ultrafine abrasive that is chemically coated with a coupling agent to provide a surface-modified ultrafine abrasive; from 5-15 wt % of a chemical additive for controlling dryness; and from 1-10 wt % of a biopolymer sol, wherein the coupling agent improves dispersion and holding of the surface-modified ultrafine abrasive in the high polymer base material, and a method of making the same.
Type:
Grant
Filed:
May 19, 2015
Date of Patent:
May 14, 2019
Assignee:
HUAQIAO UNIVERSITY
Inventors:
Jing Lu, Xipeng Xu, Hui Huang, Yunyun Song
Abstract: The present invention relates to a method for preparing pearlescent pigment through metal oxide coating based on a sheet-like substrate, and the obtained pearlescent pigment. The present invention further relates to a method for preparing pearlescent pigment through coating a sheet-like substrate by hydrolyzing metal salt under an acid condition, wherein a pH value is adjusted by using inorganics such as MgO, MgOH or CaCO3 that does not dissolve in water but can dissolve through reacting with an acid. According to the method, no free metal oxide is generated when the metal salt is hydrolyzed, so that the production cost is reduced, product quality is improved, problems possibly generated in an application process of the product are avoided, and a production process is more environment-friendly.
Type:
Grant
Filed:
February 4, 2015
Date of Patent:
May 14, 2019
Assignee:
Fujian Kuncai Material Technology Co., Ltd.
Abstract: A method of forming a shaped abrasive particle includes forming a first mixture and a second mixture in a single forming process into an integral precursor shaped abrasive particle, wherein the first mixture has a different composition than a composition of the second mixture.
Abstract: Embodiments relate to polycrystalline diamond compacts and methods of manufacturing such compacts in which an at least partially leached polycrystalline diamond (“PCD”) table is infiltrated with first and second infiltrants. The first infiltrant includes a low viscosity cobalt-based and/or nickel-based alloy infiltrant. The second infiltrant (e.g., copper) is specifically selected to be more easily infiltrated and/or removed (e.g., leached) than a pure cobalt infiltrant. In an embodiment, a method includes forming a PCD table in the presence of a metal-solvent catalyst in a first high-pressure/high-temperature (“HPHT”) process. The PCD table may be at least partially leached to remove at least a portion of the metal-solvent catalyst therefrom. The leached PCD table and a substrate are subjected to a second HPHT process effective to bond the substrate to the leached PCD table while at least partially infiltrating the PCD table with at least the first and second infiltrants.
Type:
Grant
Filed:
June 24, 2014
Date of Patent:
May 7, 2019
Assignee:
US SYNTHETIC CORPORATION
Inventors:
Debkumar Mukhopadhyay, Brandon Paul Linford, Jed Clarke
Abstract: The present invention relates to a process for the preparation of a surface-reacted precipitated calcium carbonate (PCC) pigment having an insoluble, at least partially crystalline calcium salt on its surface. In the process of the present invention, a PCC containing pigment is contacted with H3O+ ions and a solubilized anion in an aqueous medium in the presence of excess solubilized calcium ions to form the surface-reacted PCC having an insoluble, at least partially crystalline calcium salt of the anion formed on its surface.
Type:
Grant
Filed:
December 2, 2008
Date of Patent:
May 7, 2019
Assignee:
Omya International AG
Inventors:
Daniel E. Gerard, Patrick A. C. Gane, Joachim Schölkopf, Hans-Joachim Weitzel
Abstract: A polycrystalline compact includes a plurality of diamond grains of micron size, submicron size, or both, and a plurality of diamond nanoparticles disposed in interstitial spaces between the plurality of diamond grains. A method of forming a polycrystalline compact includes combining a plurality of micron and/or submicron-sized diamond grains and a plurality of diamond nanoparticles to form a mixture and sintering the mixture in a presence of a carburized binder to form a polycrystalline hard material having a plurality of inter-bonded diamond grains and diamond nanoparticles. Cutting elements including a polycrystalline compact and earth-boring tools bearing such compacts are also disclosed.
Type:
Grant
Filed:
March 15, 2013
Date of Patent:
May 7, 2019
Assignees:
Baker Hughes Incorporated, Element Six Limited
Inventors:
Anthony A. DiGiovanni, Roger William Nigel Nilen
Abstract: To perform polishing while reducing an LPD and preventing contamination with metals, particularly nickel and copper, in final polishing of a silicon wafer. A polishing composition contains abrasives, a water-soluble polymer, a basic compound, a chelating agent, and water, in which, when the particle diameter equivalent to a particle diameter at a cumulative volume of 10% from a smaller particle diameter side is defined as D10, the particle diameter equivalent to a particle diameter at a cumulative volume of 50% from the smaller particle diameter side is defined as D50, and the particle diameter equivalent to a particle diameter at a cumulative volume of 90% from the smaller particle diameter side is defined as D90 in a particle size distribution of particles present in the polishing composition, a value of a coarse particle frequency parameter A defined by (Expression 1) illustrated below is less than 1.
Abstract: Polycrystalline compacts include an interface between first and second volumes of a body of inter-bonded grains of hard material. The first volume is at least substantially free of interstitial material, and the second volume includes interstitial material in interstitial spaces between surfaces of the inter-bonded grains of hard material. The interface between the first and second volumes is configured, located and oriented such that cracks originating in the compact during use of the compacts and propagating along the interface generally toward a central axis of the compacts will propagate generally toward a back surface and away from a front cutting face of the compacts at an acute angle or angles. Methods of forming polycrystalline compacts involve the formation of such an interface within the compacts.
Abstract: A surface-coated cutting tool includes a base material and a coating formed on a surface of the base material. The coating includes a first hard coating layer including crystal grains having a sodium chloride-type crystal structure. The crystal grain has a layered structure in which a first layer composed of nitride or carbonitride of AlxTi1-x and a second layer composed of nitride or carbonitride of AlyTi1-y are stacked alternately into one or more layers. The first layer each has an atomic ratio x of Al varying in a range of 0.6 or more to less than 1. The second layer each has an atomic ratio y of Al varying in a range of 0.45 or more to less than 0.6. The largest value of difference between the atomic ratio x and the atomic ratio y is 0.05?x?y?0.5.
Type:
Grant
Filed:
June 7, 2016
Date of Patent:
April 9, 2019
Assignee:
SUMITOMO ELECTRIC HARDMETAL CORP.
Inventors:
Anongsack Paseuth, Hideaki Kanaoka, Shinya Imamura, Satoshi Ono
Abstract: Provided are abrasive articles in which the make layer, abrasive particle layer, and size layer are coated onto a backing according to a pre-determined coating pattern. All three components are generally in registration with each other, thereby providing a pervasive uncoated area extending across the backing. Advantageously, this configuration provides a coated abrasive that displays superior curl-resistance compared with previously disclosed abrasive articles. Moreover, this configuration resists loading, resists de-lamination, has enhanced flexibility, and decreases the quantity of raw materials required to achieve the same level of performance as conventional abrasive articles.
Type:
Grant
Filed:
July 1, 2011
Date of Patent:
April 2, 2019
Assignee:
3M Innovative Properties Company
Inventors:
Deborah J. Eilers, Jeffrey R. Janssen, Charles R. Wald, Christopher J. Lee, Schoen A. Schuknecht
Abstract: The present disclosure relates to an industrial device, such as a drill bit including a thermally stable polycrystalline diamond (TSP) table coupled to a substrate via an attachment joint, with at least one attachment material located in the attachment joint. At least one of the attachment materials includes a metal or metal alloy and an additive material having a hardness higher than the metal or metal alloy or a coefficient of thermal expansion lower than that of the metal or metal alloy.
Type:
Grant
Filed:
December 23, 2013
Date of Patent:
March 26, 2019
Assignee:
Halliburton Energy Services, Inc.
Inventors:
Seth Garrett Anderle, Cody William Knuteson
Abstract: The method for fabricating a hybrid dual phase filler for elastomers includes: impregnation of carbon black with ethanol suspension of magnetite in a ball mill; drying of the dual phase mixture till constant weight; grinding of the dried product in a ball mill; thermal activation under vacuum in a specifically designed reactor followed by a grinding of the final product in a ball mill. The hybrid dual phase filler includes carbon black impregnated with ethanol suspension of magnetite, contains 5 to 50 mass % of magnetite and 95 to 50 mass % of carbon black. Magnetite is a powder and includes up to 5% of SiO2, particle size up to 50? and density of 4.8-5.2 g/cm3 with a specific surface area (BET/) 400-900 m2/g; iodine number—370-750 mg/g; oil number 200-450 ml/100 g; total volume pore 0.5-1.5 cm3(STP)/g; micropore surface area 50-90 m2/g; external specific surface area 400-900 m2/g.
Type:
Grant
Filed:
July 6, 2016
Date of Patent:
March 26, 2019
Assignee:
KING ABDULAZIZ UNIVERSITY
Inventors:
Ahmed A. Al-Ghamdi, Omar A. Al-Hartomy, Falleh R. Al-Solamy, Nikolay Todorov Dishovsky, Petrunka Atanasova Malinova, Mihail Tsetskov Mihaylov
Abstract: Provided is a polishing composition with which surface defects can be efficiently reduced. This invention provides a polishing composition comprising a water-soluble polymer MC-end. The main chain of the water-soluble polymer MC-end is formed with a non-cationic region as its main structural part and a cationic region located at least at one end of the main chain. The cationic region has at least one cationic group.
Abstract: A polycrystalline super hard construction has a body of PCD material and a plurality of interstitial regions between inter-bonded diamond grains forming the PCD material. The body also has a first region substantially free of a solvent/catalyzing material which extends a depth from a working surface into the body of PCD material. A second region remote from the working surface includes solvent/catalyzing material in a plurality of the interstitial regions. A chamfer extends between the working surface and a peripheral side surface of the body of PCD material. The chamfer has a height which is the length along a plane perpendicular to the plane along which the working surface extends between the point of intersection of the chamfer with the working surface and the point of intersection of the chamfer and the peripheral side surface of the body of PCD material. The depth of the first region is greater than the height of the chamfer.
Type:
Grant
Filed:
November 5, 2013
Date of Patent:
March 5, 2019
Assignee:
Element Six Limited
Inventors:
Nedret Can, Habib Saridikmen, Roger William Nigel Nilen, Michael L. Doster, Anthony A. DiGiovanni, Matthew R. Isbell, Nicholas J. Lyons, Derek L. Nelms, Danny E. Scott