Abstract: A technique for the quantitative monitoring of a nonionic surfactant, such as nonylphenolpolyglycolether, in an acid tinning bath for the production of shiny, pore-free coatings on components. A measured amount of bath fluid (a bath specimen) is diluted with distilled water and mixed with sulfuric acid, and this mixture is then immediately titrated with a tannic acid solution until opalescence occurs.