Patents Examined by Smita Patel
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Patent number: 10337117Abstract: A method of Czochralski growth of a silicon ingot includes melting a mixture of silicon material and an n-type dopant material in a crucible. The silicon ingot is extracted from the molten silicon during an extraction time period. The silicon ingot is doped with additional n-type dopant material during at least one sub-period of the extraction time period.Type: GrantFiled: November 7, 2014Date of Patent: July 2, 2019Assignee: Infineon Technologies AGInventors: Nico Caspary, Hans-Joachim Schulze
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Patent number: 9938154Abstract: A precipitated silica production process that includes a precipitation reaction between a silicate and an acid is described, in which the acid used in at least one of the steps of the process is a concentrated acid.Type: GrantFiled: July 25, 2011Date of Patent: April 10, 2018Assignee: Rhodia OperationsInventors: Malika Clouin, Sylvaine Neveu, Joël Racinoux
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Patent number: 9925529Abstract: The invention relates to the purification and disinfection of air and water. A photocatalytic element consists of sintered glass beads with a pore volume fraction from 20% to 40% and a pore size from 0.1 to 0.5 mm, the surface of which is coated with a titanium dioxide powder, having a specific surface area of 150-400 m2/g, at the rate of 0.5-2% relative to the total mass of the photocatalytic element. The surface of the glass beads has a relief shape with a relief depression of 0.5-10 ?m. The method for producing the photocatalytic element comprises sintering the glass beads at a temperature that is 5-20° C. higher than the glass softening temperature, modifying the bead surface with chemical etching agents, and coating the bead surface with the titanium dioxide powder from a water suspension at a pH of 2.9±0.1.Type: GrantFiled: December 20, 2012Date of Patent: March 27, 2018Assignees: OOO “Krasnoe Pole”, Ipkhf Ran, Ntschian, OOO “Tiokraft”Inventors: Igor Lvovich Balikhin, Victor Ivanovich Berestenko, Igor Anatolevich Domashnev, Evgeny Nikolaevich Kabachnikov, Evgeny Nikolaevich Kurkin, Vladimir Nikolaevich Troitsky
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Patent number: 9895643Abstract: A wet scrubber (1) useful for cleaning a process gas comprises at least a first spray level system (20) and a second spray level system (26) arranged vertically above the first spray level system (20) in a wet scrubber tower (2). The first spray level system (20) comprises at least one gas-liquid contacting plate (38) which is operative for deflecting absorption liquid, that has been atomized by means of the second spray level system (26) and flowing downward in the wet scrubber tower (2), so deflected absorption liquid (AL) may contact process gas (F) contacted by absorption liquid atomized by the first spray level system (20).Type: GrantFiled: June 10, 2015Date of Patent: February 20, 2018Assignee: General Electric Technology GmbHInventor: Rikard Håkansson
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Patent number: 9890047Abstract: A process comprising: A) contacting one or more of sources of silicon oxide, selected from water soluble.silica sources arid alkali metal silicates, with an aqueous reaction medium, comprising one or more nonionic surfactants and thereby forming mesoporous structures comprising crosslinked silicon oxide units, wherein said crosslinked silicon oxide units have pores of about 1 to about 100 nanometers and wherein the aqueous reaction medium exhibits a pH of about 0 to about 4.0; B) exposing the aqueous reaction medium containing the mesoporous structures to elevated temperatures for a time sufficient to achieve the desired structure and pore size. Preferred water soluble silica sources comprise silicic acid, or polysilicic acids, The aqueous reaction, medium is prepared by combining one or more nonionic surfactants and water, theteby forming an aqueous, reaction medium, comprising micelles. Preferably, the aqueous reaction medium further comprises, a.Type: GrantFiled: November 19, 2012Date of Patent: February 13, 2018Assignee: Dow Global Technologies LLCInventors: Beata A Kilos, Cathy L Tway, Scott T Matteucci, Christopher J Tucker, Anne M Kelly-Rowley
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Patent number: 9868110Abstract: Provided are a method for producing a composite oxide and the composite oxide, which finds use as an easy-to-handle catalyst material having a high reforming rate of hydrocarbon to hydrogen even when oxidized. The method includes the steps of: (a) preparing a Ce aqueous solution not less than 80 mol % of which Ce ions are tetravalent, and a Zr aqueous solution containing Zr ions; (b1) mixing the Zr aqueous solution and a portion of the Ce aqueous solution to prepare a mixed aqueous solution (X1); (c1) hydrothermally processing solution (X1); (b2) adding the remainder of the Ce aqueous solution prepared in step (a) to a colloidal solution (Y1) of a composite salt obtained from step (c1) to prepare a colloidal solution (Y2) of a composite salt; (c2) hydrothermally processing solution (Y2) obtained from step (b2); (d) mixing a colloidal solution (Y3) of a composite salt obtained from step (c2) with an alkaline solution and a surfactant to prepare a precipitate; and (e) calcining the precipitate.Type: GrantFiled: October 1, 2013Date of Patent: January 16, 2018Assignee: SANTOKU CORPORATIONInventors: Shinya Matsuo, Tadatoshi Murota
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Patent number: 9862616Abstract: TiO2 based scrubbing granules, and methods of making and using such TiO2 based scrubbing granules are described. TiO2-based scrubbing granules include granulated TiO2 and about 0.5% to about 20% dry weight inorganic salt binder. Other TiO2 based scrubbing granules include unsintered granulated TiO2 and about 0.5% to about 20% dry weight inorganic salt binder. Inorganic salt binder include sodium aluminate. Methods of making TiO2 based scrubbing granules include i) combining TiO2 particles with inorganic salt binder to form TiO2-binder mixture comprising from about 0.5% to about 20% dry weight binder; ii) granulating the TiO2-binder mixture; and drying the granulated TiO2-binder mixture to form TiO2-based scrubbing granules.Type: GrantFiled: March 6, 2015Date of Patent: January 9, 2018Assignee: Cristal USA Inc.Inventors: Venkata Ramana Reddy Sama, Kit Stacey Eremchuk, Mark D. Pomponi, Gabor Feher, Alexandre Jean Fines
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Patent number: 9861966Abstract: A catalytic cracking catalyst is provided which has high cracking activity and with which the production of FCC gasoline having a high octane number can efficiently proceed without lowering a gasoline yield. Also provided are a process for producing the catalyst and a method of the catalytic cracking of a hydrocarbon oil with the catalyst. The catalyst for catalytic cracking of a hydrocarbon oil comprises a crystalline aluminosilicate, a binder, and a clay mineral in a certain proportion, wherein the content of sodium and potassium therein is 0.5% by mass or lower in terms of oxide (Na2O and K2O) amount, the content of at least one rare earth metal therein is 3.0% by mass or lower in terms of oxide (RE2O3, wherein RE is a rare earth element) amount, the [RE2O3+Na2O+K2O]/[crystalline aluminosilicate] ratio by mass is 0.1 or lower, and the catalyst has a xenon adsorption amount, as measured at an adsorption temperature of 25° C. and a partial xenon pressure of 650 torr, of 2.Type: GrantFiled: March 2, 2007Date of Patent: January 9, 2018Assignees: COSMO OIL CO., LTD., PETROLEUM ENERGY CENTERInventor: Katsuya Watanabe
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Patent number: 9862612Abstract: The method for producing silicon metal and porous carbon from rice hulls is provided. The method comprises a first step S1 of producing a rice hull charcoal M2 containing SiO2 and C by heat treatment of rice hulls M1; a second step S4 of exposing the rice hull charcoal M4 to at least any one of heated first inert gas G2 or reducing gas to produce SiC; a third step S5 of exposing SiC to a heating atmosphere containing Cl2 gas to produce SiCl4 and porous carbon P1; a fourth step S7 of reacting SiCl4 and Zn to produce silicon metal P2 and ZnCl2; and a fifth step S9 of electrolyzing ZnCl2 to produce Zn and Cl2 gas. The Cl2 gas in the fifth step S9 is used in the third step S5, and Zn in the fifth step S9 is used in the fourth step S7.Type: GrantFiled: May 22, 2013Date of Patent: January 9, 2018Assignee: SUMITOMO ELECTRIC INDUSTRIES, LTD.Inventors: Shinji Ishikawa, Toru Adachi, Taiichiro Yamashita
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Patent number: 9834663Abstract: A composition for forming a transparent coating film including hollow silica microparticles and a binder is provided. The hollow silica microparticles have an average particle diameter of 5 to 300 nm when measured by the dynamic light scattering method, a specific surface area of 50 to 1500 m2/g, and an outer shell in which cavities are formed. The microparticles lose weight by 1.0 W % or more at a temperature in the range of from 200° C. to 500° C. when measured by the thermogravimetry (TG). A surface charge (QA) of the hollow silica microparticles contained in the compositions for forming a transparent coating film is in the range from 5 to 20 ?eq/g.Type: GrantFiled: April 28, 2015Date of Patent: December 5, 2017Assignee: JGC Catalysts and Chemicals Ltd.Inventors: Ryota Sueyoshi, Ryo Muraguchi, Masayuki Matsuda, Mitsuaki Kumazawa, Toshiharu Hirai
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Patent number: 9821299Abstract: In a process for producing a phosphorus-modified zeolite catalyst, an aqueous reaction mixture comprising a source of silica and a source of an organic directing agent effective to direct the synthesis of a desired zeolite is heated at a temperature and for a time sufficient to produce crystals of the desired zeolite. Wet zeolite crystals can then be separated from the reaction mixture and, without removing all the water from the wet zeolite crystals, the zeolite can be converted into the ammonium form by ion exchange, and the crystals can be treated with a phosphorus compound. The phosphorus-treated, ammonium-exchanged zeolite can then be formed into a catalyst to be heated in one or more stages to remove the water and organic directing agent from the zeolite crystals and to convert the zeolite to the hydrogen form.Type: GrantFiled: October 16, 2012Date of Patent: November 21, 2017Assignee: EXXONMOBIL RESEARCH AND ENGINEERING COMPANYInventors: Wenyih Frank Lai, Merci A. Hamilton, Stephen J. McCarthy
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Patent number: 9782749Abstract: The aluminum silicate of the invention has: an element ratio of Si and Al, represented by Si/Al, of from 0.3 to 1.0 by molar ratio; a peak at approximately 3 ppm in a 27Al-NMR spectrum; peak A at approximately ?78 ppm and peak B at approximately ?85 ppm in a 29Si-NMR spectrum; and a peak at approximately 2?=26.9° and a peak at approximately 2?=40.3° in a powder X-ray diffraction spectrum. The aluminum silicate has an area ratio of peak B with respect to peak A of from 2.0 to 9.0, or does not include a tubular substance having a length of 50 nm or more as observed in a transmission electron microscope (TEM) photograph of the aluminum silicate taken at a magnification of 100,000.Type: GrantFiled: December 7, 2011Date of Patent: October 10, 2017Assignee: HITACHI CHEMICAL COMPANY, LTD.Inventors: Hiroki Mikuni, Kiyoshi Kawai
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Patent number: 9776181Abstract: In a process for forming a bulk hydroprocessing catalyst by sulfiding a catalyst precursor made in a co-precipitation reaction, up to 60% of the metal precursor feeds do not react to form catalyst precursor and end up in the supernatant as metal residuals. In the present disclosure, the metals can be recovered in a chemical precipitation step, wherein the supernatant is mixed with at least one of an acid, a sulfide-containing compound, a base, and combinations thereof to precipitate at least 50% of metal ions in at least one of the metal residuals, wherein the precipitation is carried out at a pre-select pH. The precipitate is isolated and recovered, yielding an effluent stream. The precipitate and/or the effluent stream can be further treated to form at least a metal precursor feed which can be used in the co-precipitation reaction. The process generates an effluent to waste treatment containing less than 50 ppm metals.Type: GrantFiled: March 20, 2015Date of Patent: October 3, 2017Assignee: Chevron U.S.A. Inc.Inventors: Alexander Kuperman, Theodorus Ludovicus Michael Maesen, Dennis Dykstra
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Patent number: 9725319Abstract: The present invention provides a catalyst for production of nitric oxide from ammonia and oxygen. The catalyst has the composition A3-xBxO9-y, wherein A and B are selected from the group Mn, Co, Cr, Fe and Al, x is between 0 and 3 and y is between 0 and 6. The catalyst has a high selectivity towards nitric oxide and a low ignition temperature in the reactor. Further the present invention relates to a method for the production of gas comprising nitric oxide by the catalyst of the present invention. The produced gas has a low content of nitrous oxide.Type: GrantFiled: August 22, 2008Date of Patent: August 8, 2017Assignee: YARA INTERNATIONAL ASAInventor: David Waller
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Patent number: 9718024Abstract: To provide a method for predicting a deactivation phenomenon in a flue-gas desulfurization unit to prevent the occurrence of the deactivation phenomenon before it happens. There is provided a method for preventing the occurrence of a deactivation phenomenon in a flue-gas desulfurization unit that treats flue gas of a coal-fired boiler, the method includes calculating a deactivation potential as an index of the deactivation phenomenon based on alkaline components such as Na, Ca, Mg, and K contained in ash in the flue gas, and performing an operation management, such as adjustment of set value of a pH control system, on the flue-gas desulfurization unit depending on change of the deactivation potential.Type: GrantFiled: August 22, 2012Date of Patent: August 1, 2017Assignee: Chiyoda CorporationInventors: Noboru Takei, Chisa Nishizaki
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Patent number: 9687820Abstract: An exhaust gas cleaning catalyst for an internal combustion engine includes a cerium-containing oxide, palladium supported on the cerium-containing oxide, zinc supported on the cerium-containing oxide, and barium supported on the cerium-containing oxide.Type: GrantFiled: January 30, 2013Date of Patent: June 27, 2017Assignee: HONDA MOTOR CO., LTD.Inventors: Yoshiyuki Nakanishi, Masanori Hashimoto, Hiroshi Koyama, Syouji Inose
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Patent number: 9647198Abstract: Piezoelectric oriented ceramics containing a Pb(Ti, Zr)O3-based compound having a high degree of orientation not lower than 0.64, which was calculated with the Lotgering method based on an X-ray diffraction pattern in a prescribed cross-section thereof, and having a sintered density not lower than 85% of a theoretical density.Type: GrantFiled: May 30, 2014Date of Patent: May 9, 2017Assignees: MURATA MANUFACTURING CO., LTD., NATIONAL INSTITUTE FOR MATERIALS SCIENCEInventors: Yasunari Miwa, Shinichiro Kawada, Masahiko Kimura, Tohru Suzuki, Tetsuo Uchikoshi, Yoshio Sakka
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Patent number: 9637394Abstract: The present invention discloses a method preparing a TiO2 nanostructure comprising: mixing an organic acid and an aminoalcohol to form an ionic liquid; heating the ionic liquid with titanium ions and lithium ions to form a layered structure; and annealing the mixture to form the TiO2 nanostructure. There is also provided uses of the prepared nanostructure.Type: GrantFiled: September 25, 2012Date of Patent: May 2, 2017Assignee: NANYANG TECHNOLOGICAL UNIVERSITYInventors: Jiehua Liu, Xue-Wei Liu, Xiangfeng Wei
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Patent number: 9616413Abstract: The present invention provides a catalyst for production of nitric oxide from ammonia and oxygen. The catalyst has the composition A((n+1)?x)BxC(n(1?y))DnyO(3n+1)+d, wherein A is a lanthanide (La, Gd, Nd, Sm) or yttrium, B is an alkaline-earth cation (Ca, Sr or Ba), C is Fe and D is Cr, Mn, Ni, Ce, Ti, Co or Mg, wherein A, B, C and D are selected independent of each other. The catalyst has a high selectivity towards nitric oxide and a low ignition temperature in the reactor. Further the present invention relates to a method for the production of gas comprising nitric oxide by the catalyst of the present invention. The produced gas has a very low content of nitrous oxide.Type: GrantFiled: October 23, 2008Date of Patent: April 11, 2017Assignee: YARA INTERNATIONAL ASAInventor: David Waller
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Patent number: 9597668Abstract: A selective nickel-based hydrogenation catalyst and the preparation thereof, characterized in that: provided that the catalyst is weighed 100%, it comprises nickel oxide 14-20% as active component, lanthanum oxide and/or cerium oxide 2-8%, and VIB element oxide 1-8% as aids, 2-8% silica, 1-8% alkaline earth metal oxides, and alumina as the balance. The catalyst specific surface area is 60-150 m2/g, and the pore volume is 0.4-0.6 ml/g. The catalyst has good hydrogenation performance, especially impurity and colloid resistance and hydrogenation stability. The catalyst can be applied to the diolefin selective hydrogenation of medium or low-distillate oil, especially of the full-distillates pyrolysis gasoline.Type: GrantFiled: August 11, 2014Date of Patent: March 21, 2017Assignee: PETROCHINA COMPANY LIMITEDInventors: Shunqin Liang, Ying Qian, Longgang Lv, Limin Sun, Yundi Zheng, Tinghai Wang, Jie Wu, Fengxia Cao