Abstract: The invention provides a process for depositing a coating onto particles being pneumatically transported in a tube. The process comprising the steps of providing a tube having an inlet opening and an outlet opening; feeding a carrier gas entraining particles into the tube at or near the inlet opening of the tube to create a particle flow through the tube; and injecting a first self-terminating reactant into the tube via at least one injection point downstream from the inlet opening of the tube for reaction with the particles in the particle flow. The process is suitable for atomic layer deposition and molecular layer deposition. An apparatus for carrying out the process is also disclosed.

Abstract: A method for improving the insulating character/and or penetration resistance of a surface comprising lining a surface of a lime kiln, a cement kiln, a roasting kiln, a thermal oxidizer, or a fluidized bed reactor that is subject to wear by an alkali environment and/or an alkaline environment with a refractory composition comprising a refractory aggregate consisting essentially of a calcium hexa aluminate clinker having the formula CA6, wherein C is equal to calcium oxide, wherein A is equal to aluminum oxide, and wherein the hexa aluminate clinker has from zero to less than about fifty weight percent C12A7, and wherein greater than 98 weight percent of the calcium hexa aluminate clinker having a particle size ranging from ?20 microns to +3 millimeters, for forming a liner of the surface.

Abstract: A method of manufacturing polycrystalline abrasive elements consisting of micron, sub-micron or nano-sized ultrahard abrasives dispersed in micron, sub-micron or nano-sized matrix materials. A plurality of ultrahard abrasive particles having vitreophilic surfaces are coated with a matrix precursor material in a refined colloidal process and then treated to render them suitable for sintering. The matrix precursor material can be converted to an oxide, nitride, carbide, oxynitride, oxycarbide, or carbonitride, or an elemental form thereof. The coated ultrahard abrasive particles are consolidated and sintered at a pressure and temperature at which they are crystallographically or thermodynamically stable.

Abstract: A method for improving the heat resistance of a resistive element embedded in an alumina deposit covering a surface of a substrate, in which the alumina deposit includes a surface portion and a deep portion which is sandwiched between the surface portion and the surface of the substrate and in which the resistive element is located, is provided. The method includes a densification of the surface portion of the alumina deposit.

Abstract: Fire resistant glazings comprise a fire resistant interlayer based upon a silicate waterglass are characterized by the incorporation of aluminum ions. The aluminate is incorporated as a solution which has been partially neutralized using hydroxycarboxylic acid which is preferably citric acid. The incorporation of aluminum provides glazings have improved fire resistance and impact properties.

Abstract: The present invention relates to a method for preparing a carbon-based particle/copper composite material in which carbon-based particles such as graphite and copper are mixed, the method including mixing a solution of a polymer organic compound having a main chain of carbon and a copper precursor in a solvent, with a dispersion solution of carbon-based particles in a first dispersion medium to produce a mixture, adding a first reducing agent to the mixture to form composite particles in which copper (I) oxide particles are attached to the surface of the carbon-based particles, and sintering the composite particles under a non-oxidizing atmosphere. According to the preparing method, a composition material is obtained, in which carbon-based particles and copper are well mixed.

Abstract: A method is provided for coating a substrate, in particular a fiber reinforced plastic component, a protective layer being applied, with preference by means of thermal spraying, to a non-cured resin film applied to a release film, and subsequently, after removal of the release film, the resin film being applied to the substrate and cured.

Abstract: A coating for spark plugs and engine parts is resistant to fouling. The coating may be applied to the spark plug or engine part by dipping the part in a sol gel solution, ensuring it wets the part, and extracting it at a slow, controlled rate. As the part is allowed to dry, the sol gel reacts with moisture in the air to form a thin oxide film. Unlike conventional sol gel applications, which apply the oxide directly to the part, the present invention may form an oxide coating, in situ, while drying in place on the part.

Abstract: A method of polymerizing monomer to form polymer at the surface of particulate material, said method comprising: providing a dispersion of said particulate material in a continuous liquid phase, said dispersion comprising a RAFT agent as a stabilizer for said particulate material, and said continuous liquid phase comprising one or more ethylenically unsaturated monomers; and polymerizing said one or more ethylenically unsaturated monomers under the control of said RAFT agent to thereby form polymer at the surface of said particulate material.

Abstract: This invention relates to a method for preparing an organic film at the surface of a solid support, with a step of contacting said surface with a liquid solution including (i) at least one solvent, (ii) at least one adhesion primer, under non-electrochemical conditions, and allowing the formation of radical entities based on the adhesion primer. The liquid solution can also include (iii) at least one monomer different from the adhesion primer and radically polymerizable. This invention also relates to a non-electrically-conductive solid support on which an organic film according to said method is grafted, and a kit for preparing an essentially polymeric organic film at the surface of a solid support.

Abstract: In one aspect of the invention, a method of synthesizing a lithium metal phosphate composite usable for a lithium secondary battery includes the steps of forming a nanometer-size precursor comprising lithium source and metal phosphate nanoparticles having each nanoparticle at least partially coated a layer of carbon precursor, spray drying the nanometer-size precursor at a first desired temperature to form micron-size particles packed with the lithium metal phosphate precursor nanoparticles, and sintering the micron-size particles at a second desired temperature under an inert and/or reduction atmosphere to form a micron-size lithium metal phosphate composite.

Abstract: Highly luminescent nanostructures, particularly highly luminescent quantum dots, are provided. The nanostructures have high photoluminescence quantum yields and in certain embodiments emit light at particular wavelengths and have a narrow size distribution. The nanostructures can comprise ligands, including C5-C8 carboxylic acid ligands employed during shell formation and/or dicarboxylic or polycarboxylic acid ligands provided after synthesis. Processes for producing such highly luminescent nanostructures are also provided, including methods for enriching nanostructure cores with indium and techniques for shell synthesis.

Abstract: The present invention is directed to a method for forming a crystalline cobalt silicide film, comprising the steps of: applying to a surface made of silicon a composition obtained by mixing a compound represented by the following formula (1A) or (1B): SinX2n+2??(1A) SimX2m??(1B) wherein each X in the formulas (1A) and (1B) is a hydrogen atom or a halogen atom, n is an integer of 1 to 10, and m is an integer of 3 to 10, or a polymer thereof with a zero-valent cobalt complex to form a coating film; heating the coated film at 550 to 900° C. so as to form a two-layer film which is composed of a first layer made of a crystalline cobalt silicide on the surface made of silicon and a second layer containing silicon atoms, oxygen atoms, carbon atoms and cobalt atoms on the first layer; and removing the second layer of the two-layer film.

Abstract: Exemplary embodiments of the invention provide barrier coated substrates and methods of coating a substrate with a barrier coating derived from sol gels. An example includes a barrier coated aerospace component that is subject to hot salt corrosion during use. The barrier coating is derived from oxidation of a coating composition that includes at least one sol gel. The barrier coating resists hot salt corrosion for an incubation period of such duration that an uncoated superalloy substrate under the same conditions would suffer corrosion to a depth of about 2.0 mils. Methods of applying the barrier coating include the steps of selecting a first liquid sol gel and wetting surfaces of the superalloy substrate with the selected first liquid sol gel. The wetted surfaces of the superalloy substrate are subjected to heat treatment. The heat treatment includes sintering of sol gel to oxide to produce a barrier coating.

Abstract: A process for applying an oxidation resistant coating to an article includes the steps of mixing at least about 10% by volume to up to about 99% by volume of a slurry at least one silica based material having a viscosity of about 1×102 poise to about 1×107 poise at a temperature of about 1,292° F. (700° C.) to about 3,272° F. (1,800° C.) at least about 1% by volume to up to about 90% by volume of the slurry at least one oxygen scavenger, and a liquid medium to form the slurry; coating an article with the slurry to form a slurry coated article; and heat treating under an inert atmosphere the slurry coated article to form an article having at least one oxidation resistant coating layer containing the at least one oxygen scavenger.

Abstract: A method of manufacturing a multiscale (hierarchical) superhydrophobic surface is provided. The method includes texturing a polymer surface at three size scales, in a fractal-like or pseudo-fractal-like manner, the lowest scale being nanoscale and the highest microscale. The hydrophobic polymer surface may be converted to hydrophobic metal surface by subsequent deposition of a metal layer onto the polymer surface.

Abstract: A method of manufacturing encapsulated superhard material includes the steps of providing a source of superhard material, providing a mixture comprising an appropriate binder, a solvent or fluid medium and the intended coating or encapsulating layer, combining the superhard material and the mixture in a shovel rotor, the shovel rotor having a vessel including a rotor, the vessel adapted to receive a stream of gas. The rotor is rotated at an appropriate velocity such that the superhard material is encapsulated by the mixture.

Abstract: A process for the formation of pellets containing an ultra hard (superhard) core coated with an encapsulating material includes utilizing a shovel rotor in combination with a rotating pan and/or a fluidized bed apparatus in sequence. The process includes providing a source of superhard material, providing a mixture comprising a binder, a solvent or fluid medium and the intended coating or encapsulating layer, and combining the superhard material and the mixture in a shovel rotor. The rotor of the shovel rotor is rotated at a velocity such that the superhard material is encapsulated by the mixture to form pellets. The pellets are introduced into a rotating vessel or fluidized bed granulating apparatus, and the pellets are contacted with encapsulating material to form pellets of greater mass than the pellets introduced into the vessel.

Abstract: A method of coating with an aqueous coating composition having a pH <5 of silica nanoparticles having a, average particle diameter of ?40 nm, silica nanoparticles having an average particle diameter of ?50 nm, and a tetraalkoxysilane. The resulting coatings are substantially uniform in thickness, durably adheres to the substrate, and provides antireflection and or hydrophilic surface properties to the substrate.

Abstract: A method for making a nano-scale film includes the steps of: (a) providing a suspension including an organic solvent and a number of nano-scale particles dispersed therein; (b) dropping/releasing the suspension into a liquid having a specific gravity greater than that of the nano-scale particles; and (c) forming a uniform film of nano-scale particles on the surface of the liquid.