Abstract: A method is disclosed for recovering cobalt, which comprises adding ammonia to a cobalt chloride solution to a pH of from about 8.8 to about 9.6 with oxidation, to form hexammine cobalt (III) chloride, adding to the resulting solution of hexammine cobalt (III) chloride, sodium chloride in an amount sufficient to result in the precipitation of at least about 98% by weight of the cobalt as cobalt hexammine (III) chloride at a temperature of no greater than about 40.degree. C., separating the precipitate of cobalt hexammine (III) chloride from the resulting mother liquor which contains the balance of the cobalt, adding to the mother liquor, aluminum powder in an amount sufficient to result in the precipitation of the balance of the cobalt as cobalt metal, and separating the cobalt metal from the resulting spent liquor.

Abstract: A thermopulse apparatus for deburring parts has a hollow body (1) housing a working chamber (2) in such a manner as to define a space (7) between the outer walls (6) thereof and inner walls (4) of the body (1) for liquid (8) partly filling the space. The chamber (2) has spark plugs (9), an inlet valve (20), an exhaust valve (12) mounted in the bottom part of the chamber (2) along the longitudinal axis (16) thereof under the layer of liquid (8), and a covermember (13) for accommodation of the parts (14) being treated, the convermember being reciprocatable within the chamber (2). Ports (23 and 32) respectively are provided in the side walls (22) of the valve (12) and in the covermember (13) on the side of the valve (12).

Abstract: The disclosed particulate composition of simple or mixed oxalate of ferromagnetic metals is characterized in that it is provided in the form of needle-shaped particles having a length comprised between 0.05 and 0.5 micrometer, with a proportion higher than 60% of particles having a length equal to the average length .+-.0.1 .mu.m. and an acicular ratio higher than 3, said average length being comprised between 0.15 and 0.35 .mu.m; its preparation and its application are also disclosed.

Abstract: Alloys of a first group of metals containing at least one iron group metal and one or more easily oxidizable metals can be formed by forming an aqueous solution of the first group of metals, forming solids containing the metals from the solution, reducing the solids to a metallic powder, converting the metallic powder to metallic alloy spherical powders, agglomeration the spherical powder with one or more easily oxidizable metals in a non-oxidizing atmosphere, thereafter the agglomerates are subjected to a sufficient temperatures under non-oxidizing conditions to form an alloy. Alternatively, the easily oxidizable metals can be agglomerated with the solids containing the iron group metal prior to converting the agglomerates to a spherical alloy powder.

Abstract: A method for working high-purity, mechanically strong targets containing brittle phases in the equilibrium state. First a porous body is manufactured from part of the component with a higher melting point and thereafter the porous body is impregnated with an impregnating composition corresponding to the remainder of the components required to form the ultimate composition of the target. The composition of the impregnation material must be selected in such a manner that the reaction between the impregnation material and the porous body shall produce no phases of low melting points.

Abstract: A method is disclosed for producing fine cobalt metal powder which comprises adding to a solution of cobaltous chloride, sodium hydroxide in an amount equal to at least the stoichiometric amount required to form a precipitate of the major portion of the cobalt as cobaltous hydroxide and a mother liquor containing the balance of the starting cobalt, separating the precipitate from the mother liquor, water washing the precipitate to remove essentially all of the sodium therefrom, and reducing the precipitate to fine cobalt metal powder having an FSSS of from about 0.5 to about 2.0. Drying of the precipitate before reduction results in the fine cobalt metal powder having essentially no tailings.

Abstract: An apparatus has a cylindrical working chamber (2) with a bottom member (7) provided with admission and discharge valves (3,5) and a spark plug (4). The bottom member (7) is made as a hollow cylinder having end plates and openings (8), the height and outside diameter of which are approximately equal to the height and inside diameter of the working chamber (2). Sealing rings (11, 12) are interposed between the chamber (2) and the hollow cylinder.

Abstract: An apparatus for thermal deburring of parts has a working chamber (6) with a bottom member (3), an inlet valve (8), a spark plug (9) and an outlet valve. The latter is made in the form of a rod (10) having a through passage (11), one end of the passage communicating with the interior of the chamber (6) and the other end being disposed in a vessel (1) containing a liquid (2) and surrounded by an annular cooling chamber (13).

Abstract: Process for increasing the room-temperature ductility of a workpiece composed of oxide-dispersion-hardened nickel-base superalloy and existing as coarse, longitudinally oriented columnar crystallites by subjecting the previously zone-annealed workpiece to a solution anneal in the temperature range between 1,160.degree. and 1,280.degree. C. under argon atmosphere for 1/2 h to 5 h and then to a purposefully chosen cooling down at a rate of 0.1.degree. C./min to 5.degree. C./min to a temperature of 500.degree. to 700.degree. C. Thereafter the workpiece is cooled down to room temperature in air. Preferred purposefully chosen cooling down rate: approx. 0.5.degree. C./min.

Abstract: An apparatus and method for forming metal powders in which a stream of atomized molten metal is expelled substantially horizontally within a sealed chamber containing a non-reactive gas under pressure, and permitted to free-fall in an arcuate path through the chamber. Atomization is accomplished by use of a nozzle device in which a forced stream of molten metal is cut into droplets by a spiraling jet of the non-reactive gas.

Abstract: A process for producing powder particles comprises forming an aqueous solution of the metal values of iron, cobalt, nickel and molybdenum, said metals being present in a predetermined ratio, forming from the solution a reducible solid material selected from the group consisting of salts of said metals, oxides of said metals, hydroxides of said metals and mixtures thereof, and reducing said material to form irregular shaped metallic powder particles.

Abstract: A method for torch cutting metal walls by burning powdered metals admixed with a gas oxidizer to establish a pre-heat flame at a cutting zone and followed by continuously adding a gas cutting agent for intensifying said flame cutting through the metal wall by burning and melting, and an apparatus to implement this method and which locates a body to the wall to be cut and carries and advances a torch over said wall with the discharge of said powdered metals and gases for preheat and followed by the continuous addition of said cutting agent for continuous cutting of the wall, and all of which is adapted to remote underwater operation within steel casings and over steel plate, as well as through other metals and materials.

Abstract: System and method for producing metal or alloy powder are described which mprises a housing defining a cylindrical chamber having an inlet and an outlet and a plurality of passageways in the form of fluid nozzles defined through the housing wall along axes oriented at preselected angle to the chamber wall, the passageways being operatively connected to a pressurized source of fluid so that fluid is injected into the chamber as fluid jets of preselected flow rate and is swirled in controllable helical fashion generally toward the chamber outlet, and a molten source of metal or alloy operatively connected through a molten metal nozzle and atomization die to the inlet of the chamber for directing molten particles into contact with the fluid jets for solidification and cooling along downward helical paths within the chamber. A plurality of concentric annular bins may be disposed near the outlet of the chamber for collecting powder formed within the chamber.

Abstract: A process for forming maraging steel alloys comprise forming an aqueous solution containing the metal values of iron, cobalt, nickel and molybdenum in a predetermined ratio, forming the reducible solid material from the solution, reducing the solid material to form metallic powder particles. These particles are entrained in a carrier gas and fed into a high temperature zone to form droplets. The droplets are cooled to form essentially spherical particles which are agglomerated with a predetermined amount of at least one readily oxidizable metal selected from the group consisting of aluminum, titanium and vanadium. The agglomerates are entrained in a carrier gas and fed into a high temperature zone to form droplets which are thereafter cooled to form essentially spherical shaped particles of a maraging steel alloy containing at least one readily oxidizable metal.

Abstract: A powder material and a process for producing the material are disclosed. The powder material consists essentially of iron group based and chromium based spherical particles. The material is essentially free of elliptical shaped material and elongated particles having rounded ends. The material has a particle size of less than about 20 micrometers in diameter and has an oxygen content of less than about 0.8% by weight. The process for making the spherical particles involves reducing the size of a starting material to produce a finer powder essentially all of which has a particle size of less than about 20 micrometers in diameter. This is done by fluid energy milling. The finer powder is entrained in a carrier gas and passed through a high temperature zone at a temperature above the melting point of the powder, the temperature being from about 5500.degree. C. to about 17,000.degree. C.

Abstract: A powder material and a process for producing the material are disclosed. The powder material consists essentially of spherical particles selected from the group consisting of metals, metal alloys, ceramic glasses, crystalline ceramic materials, and combinations thereof. The material is essentially free of elliptical shaped material and elongated particles having rounded ends. The material has a particle size of less than about 20 micrometers in diameter and has an oxygen content of less than about 0.8% by weight. The process for making the spherical particles involves reducing the size of a starting material to produce a finer powder essentially all of which has a particle size of less than about 20 micrometers in diameter. This is done by fluid energy milling. The finer powder is entrained in a carrier gas and passed through a high temperature zone at a temperature above the melting point of the powder, the temperature being from about 5500.degree. C. to about 17,000.degree. C.

Abstract: A method is provided for rapidly solidifying rare earth-transition metal containing alloy. It entails introducing the alloy into the flame of a plasma torch and directing the torch flame onto the inside surface of a rotating quench cylinder. A non-oxidizing gas is also directed onto the quench surface so that the alloy solidifies at a rate such that a powder having a substantially amorphous to finely crystalline microstructure is obtained and such that the solidified alloy does not adhere to the quench surface and can be easily collected.

Abstract: A method for increasing the yield of fine and ultrafine powder from a metal or metal alloy, including such high surface tension metals and alloys as copper, Fe-based alloys, Cu-Al-Fe alloys and Ni-Cr-Fe-B-Si alloys. A pressurized stream of molten metal is atomized by a cone of impinging gas streams, the apex of the gas cone being less than 50 mm from the melt outlet and 11-24 mm from the gas orifices. The gas velocity is greater than 100 m/sec, and the mass flow ratio of melt to gas is less than 0.10. The melt stream is pressurized by introducing pressurizing gas to an overpressure zone above the melt, e.g. in a sealed crucible.

Abstract: A wheeled holder is designed to hold and carry a welding torch stably along a chosen welding line. The holder includes adjusting means for varying the mounting position of the torch relative to the wheels. The circumferential edge of each wheel is designed as a knife edge to improve the holder's ability to be steered along a curved line.

Abstract: A plasma arc hole cutting device is disclosed for removing selected portions of metal workpieces, such as stainless steel, for testing or marking purposes. A plasma torch is connected at one end to a rotatable cam element and spaced a distance from the center of the cam element such that rotation of the cam element by a drive motor causes the plasma torch to rotate in an orbit about a longitudinal axis defined by the cam element. Suitably supported, the plasma torch burns a circular hole through the workpiece, thereby creating a slug which may be removed and analyzed, leaving a circular hole in the workpiece.