Patents Examined by Wilbur Bascomb
  • Patent number: 5417812
    Abstract: Ethyl benzene is difficult to separate from xylenes by conventional distillation or rectification because of the proximity of their boiling points. Ethyl benzene can be readily separated from xylenes by azeotropic distillation. Effective agents for separating ethyl benzene from p-xylene are methyl formate, n-butanol and cyclopentanol; from p-xylene and m-xylene, n-butanol.
    Type: Grant
    Filed: January 10, 1994
    Date of Patent: May 23, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5417814
    Abstract: 3-Methyl-2-butanol is difficult to separate from 2-pentanol by conventional distillation or rectification because of the proximity of their boiling points. 3-Methyl-2-butanol can be readily separated from 2-pentanol by extractive distillation. Effective agents are acetamide or 2,2,2-trichloroethanol.
    Type: Grant
    Filed: December 5, 1994
    Date of Patent: May 23, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5417813
    Abstract: 1-Butanol is difficult to semarate from 2-pentanol by conventional distillation or rectification because of the proximity of their boiling points. 1-Butanol can be readily separated from 2-pentanol by azeotropic distillation. Effective agents are 1-octene, hexane and methyl cyclohexane.
    Type: Grant
    Filed: July 11, 1994
    Date of Patent: May 23, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5415786
    Abstract: Process for treating, especially waters to be made drinkable, with ozone in a reactor (2), especially with a bubble column, in which ozone is generated (in 1) in a gas enriched in oxygen containing at least 70% of oxygen by volume, to produce an ozonised gas containing more than 2%, especially from 2% to 20%, of ozone by weight, in which the said ozonised gas is diluted by means of a secondary fluid and the treatment is carried out by means of the diluted ozonised gas.Another subject of the invention is a plant for the use of the process according to the invention, comprising an ozoniser (1) generating an ozonised gas, at least one reactor (2) for treatment with ozone, and a supply pipe (3) connecting the outlet of the ozoniser with the inlet of the reactor, in which means (4, 5; 15, 16), for injecting a secondary fluid into the said supply pipe (3), are additionally provided.
    Type: Grant
    Filed: June 28, 1993
    Date of Patent: May 16, 1995
    Assignee: Trailigaz-Compagnie Generale de l'Ozone
    Inventors: Nathalie Martin, Philippe Serpry
  • Patent number: 5415741
    Abstract: Ethanol is difficult to separate from isopropanol by conventional distillation or rectification because of the proximity of their boiling points. Ethanol can be readily separated from isopropanol by azeotropic distillation. Effective agents are acetonitrile and methylene chloride.
    Type: Grant
    Filed: October 18, 1994
    Date of Patent: May 16, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5409579
    Abstract: Disclosed is a method and apparatus for recovering acetic acid from an acetic acid/water waste stream which includes a dehydration column into which the stream is fed and a liquid-liquid extraction system for recovering acetic acid from the condensate of the overhead stream of the dehydration column. Optionally, low pressure and/or high pressure absorber systems are provided to process vapor and/or liquid streams associated with the recovery system and/or the plant in which the acetic acid is used to further the recovery of acetic acid and reduce atmospheric pollution.
    Type: Grant
    Filed: July 12, 1993
    Date of Patent: April 25, 1995
    Assignee: Glitsch, Inc.
    Inventors: Ronald G. Gualy, Wiston Lamshing, Joseph C. Gentry, Fernando Varela
  • Patent number: 5409576
    Abstract: A rotating evaporator device is disclosed for the distillation or concentration of liquids. The rotating evaporator device of the present invention utilizes a multiplicity of pairs of disks wherein each disk pair forms a cavity within which heating vapor condenses on the interior surfaces of the disk pair and evaporation occurs from a thin film of distilland deposited on the outside surfaces of the disk pair by means of flexible wipers pressing on the outside surfaces of the disk pair. The centrifugal force created by the rotation of the disks causes the distillate and distilland films to be very thin resulting in very high heat transfer coefficient. The pairs of disks are joined together at the inside peripheries and are rotated about a stationary hollow shaft wherein heating vapor is introduced into the cavities through ports in the shaft and stationary scoops are connected to the shaft to withdraw the condensate from the circumferential peripheries of the cavities.
    Type: Grant
    Filed: July 16, 1993
    Date of Patent: April 25, 1995
    Inventor: Badawi Tleimat
  • Patent number: 5407565
    Abstract: The solids collector collects solids that may be ejected by an HVE. The collector includes a deflector for efficiently filling the collector.
    Type: Grant
    Filed: February 12, 1993
    Date of Patent: April 18, 1995
    Assignee: A-Dec, Inc.
    Inventors: George K. Austin, Jr., David L. Curtis
  • Patent number: 5407542
    Abstract: 3-Methyl-2-butanol is difficult to separate from 1-butanol by conventional distillation or rectification because of the proximity of their boiling points. 3-Methyl-2-butanol can be readily separated from 1-butanol by azeotropic distillation. Effective agents are methyl acetoacetate and dioxane.
    Type: Grant
    Filed: September 13, 1994
    Date of Patent: April 18, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5407561
    Abstract: An apparatus for separating solids suspended in incoming pressurized liquid slurry is disclosed. The apparatus comprises a vessel having an elongated cylindrical vessel wall, a closed upper end and a bottom section for accumulation of solids. The vessel includes a stirrer mounted for rotation along an inside surface of the bottom section and a discharge spool mounted beneath the bottom section including at least one opening. An underflow pump is provided for discharging separated solids without loss of pressure in the apparatus. The apparatus further includes means for detecting solids level in the apparatus, which preferably operates without disturbing settling of the solids therein. Also, the apparatus includes a feedwell for receiving an incoming pressurized slurry stream, the feedwell having an opening a predetermined distance above a level in the apparatus defined by settled solids.
    Type: Grant
    Filed: May 7, 1993
    Date of Patent: April 18, 1995
    Assignee: Alcan International Limited
    Inventors: Fusanosuke Iida, Fitzgerald Stewart, Donald Puxley
  • Patent number: 5407541
    Abstract: 3-Methyl-2-butanol is difficult to separate from 2-pentanol by conventional distillation or rectification because of the proximity of their boiling points. 3-Methyl-2-butanol can be readily separated from 2-pentanol by azeotropic distillation. Effective agents are pentane, 2,2-dimethyl butane and dioxane.
    Type: Grant
    Filed: September 13, 1994
    Date of Patent: April 18, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5407540
    Abstract: 3-Methyl-2-butanol is difficult to separate from 1-butanol by conventional distillation or rectification because of the proximity of their boiling points. 3-Methyl-2-butanol can be readily separated from 1-butanol by extractive distillation. Effective agents are ethyl n-valerate, dimethylacetamide and dimethylsulfoxide.
    Type: Grant
    Filed: September 23, 1994
    Date of Patent: April 18, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5405505
    Abstract: Benzene is difficult to separate from cyclohexane or cyclohexene by conventional distillation or rectification because of the close proximity of their boiling points. Benzene can be readily separated from cyclohexane or cyclohexene by using azeotropic distillation. Effective agents are: for benzene from cyclohexane, dimethoxymethane; for benzene from cyclohexene, methanol.
    Type: Grant
    Filed: January 14, 1994
    Date of Patent: April 11, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5405504
    Abstract: 1-Decene is impossible to separate from 2-octanone by conventional distillation or rectification because the two compounds form a minimum boiling azeotrope. 1-Decene can be readily separated from 2-octanone by azeotropic distillation. Effective agents are 1-propanol, 2-ethoxyethanol, and methanol.
    Type: Grant
    Filed: January 31, 1994
    Date of Patent: April 11, 1995
    Assignee: Lloyd Berg
    Inventors: Lloyd Berg, Randy W. Wytcherley
  • Patent number: 5403448
    Abstract: 1-Decene is difficult to separate from 2-octanone by conventional distillation or rectification because of the proximity of their boiling points. 1-Decene can be readily separated from 2-octanone by azeotropic distillation. Effective agents are butyl propionate and 1-propanol.
    Type: Grant
    Filed: January 14, 1994
    Date of Patent: April 4, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5401366
    Abstract: 1-Butanol is difficult to separate from 2-pentanol by conventional distillation or rectification because of the proximity of their boiling points. 1-Butanol can be readily separated from 2-pentanol by extractive distillation. Effective agents are ethyl benzene, d-limonene and terpinolene.
    Type: Grant
    Filed: July 11, 1994
    Date of Patent: March 28, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5399244
    Abstract: Benzene and other aromatics are separated from a stream of mixed hydrocarbons containing both aromatics and non-aromatics by extractive distillation with a solvent system containing dimethyl sulfoxide and optionally a co-solvent, preferably water, followed by distillation stripping of the aromatics from the enriched solvent system, and recycle of the lean solvent system to the extractive distillation step.
    Type: Grant
    Filed: December 6, 1993
    Date of Patent: March 21, 1995
    Assignee: Glitsch, Inc.
    Inventors: Joseph C. Gentry, Lloyd Berg, John C. McIntyre, Randa W. Wytcherley
  • Patent number: 5397441
    Abstract: Ethyl benzene is difficult to separate from o-xylene by conventional distillation or rectification because of the closeness of their boiling points. Ethyl benzene can be readily separated from o-xylene by extractive distillation. Effective agents are phenol, cresols, nitrotoluenes and cyclododecanol.
    Type: Grant
    Filed: January 14, 1994
    Date of Patent: March 14, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg
  • Patent number: 5393385
    Abstract: Hexane is difficult to separate from vinyl acetate and/or methyl acrylate by conventional distillation or rectification because of the closeness of their boiling points. Hexane can be readily separated from vinyl acetate and/or methyl acrylate by extractive distillation. Effective agents are dimethylsulfoxide and dimethylformamide.
    Type: Grant
    Filed: March 14, 1994
    Date of Patent: February 28, 1995
    Assignee: Lloyd Berg
    Inventors: Lloyd Berg, Randi W. Wytcherley
  • Patent number: 5391264
    Abstract: alpha-Phellandrene is difficult to separate from d-limonene by conventional distillation or rectification because of the proximity of their boiling points. alpha-Phellandrene can be readily separated from d-limonene by azeotropic distillation. Effective agents are n-butyl acetate and sulfolane.
    Type: Grant
    Filed: March 14, 1994
    Date of Patent: February 21, 1995
    Assignee: Lloyd Berg
    Inventor: Lloyd Berg