Abstract: A method of producing a monolithic ceramic body from a porous matrix includes providing a porous matrix having interstitial spaces, providing an infiltrating medium comprising a solvent and at least one reactive species, and infiltrating at least a portion of the interstitial space of the porous matrix with the infiltrating medium. The solvent is an inert medium that is not chemically reactive with the porous matrix, and is in a liquid phase when in the portion of the interstitial space of the porous matrix. The infiltrating medium is mechanically convected through the porous matrix. The at least one reactive species, when in a portion of the interstitial space of the porous matrix, reacts with a portion of the porous matrix to form a product, and the product fills at least a portion of the interstitial space.
Type:
Grant
Filed:
September 30, 2013
Date of Patent:
February 23, 2016
Assignee:
RUTGERS, THE STATE UNIVERSITY OF NEW JERSEY
Inventors:
Richard E. Riman, Vahit Atakan, John P. Kuppler, Kenneth M. Smith
Abstract: A method and apparatus to treat a dried unfired article comprising a ceramic precursor composition substantially held together by a binder, to be resistant to binder soluble solvent based processing. The method includes depositing a fluid on the article surface, and polymerizing the deposited fluid to form a polymer thin layer on the surface. The fluid may be an aerosol, a vapor, a fog, a mist, a smoke, or combinations thereof. An apparatus to perform the method and an article resistant to binder soluble solvent based processing are also provided. The article can be an unfired honeycomb body that includes a dried composition of ceramic precursor substantially held together by a binder and a layer disposed on a surface of the unfired honeycomb body. The surface to be exposed in the green state to a binder soluble solvent and the layer protects the binder from solubilization by the solvent.
Type:
Grant
Filed:
March 15, 2013
Date of Patent:
February 9, 2016
Assignee:
Corning Incorporated
Inventors:
Kenneth Joseph Drury, Paul John Shustack, Todd Parrish St. Clair
Abstract: A method of painting a five-sided container, which includes applying a water-based paint to the interior surfaces and the exterior surfaces of the container, and forcing heated air into the open side of the container to at least partially dry the paint on the interior surfaces and the exterior surfaces of the container.
Abstract: A process for producing a repair coating on at least one metallic surface that is coated with at least one corrosion protecting coating A applied with at least one composition selected from the group of pretreatment compositions, of organic compositions and of silicon compound(s) containing compositions, whereby the at least one corrosion protecting coating A has been at least partially removed in the area Z, whereby a thin corrosion protecting coating B containing at least one silicon compound is applied with a solution or dispersion containing a silane, a silanol, a siloxane, or a polysiloxane on at least a part of the area Z. A further corrosion protecting coating C may be applied.
Abstract: The present invention makes it possible to print embossed structures 111, 121 et seq. such as particularly arrays of optical lenses which may be contiguous. It consists of printing a first surface (S1) which may also equally well be the structures 111, 121 et seq. as the assembly 2 of separation surfaces between these structures, using an ink (M1) and of lowering the surface tension of this ink M1 so that it becomes lower than that of the printing medium, before printing the next layer which is then strongly repelled by the surface S1. This method makes it possible using very inexpensive known printing techniques to produce embossed structures forming substantial protuberances relative to the basis thereof, this being a major advantage in particular for lens arrays.
Abstract: A cost-effective process for treating a concrete structure includes the following steps. A surface of the concrete structure is coated with an organo-silicon compound and the organo-silicon coated surface is covered so as to reduce atmospheric exposure of the organo-silicon compound while the organo-silicon compound migrates into the concrete structure.
Abstract: A copper substrate for use as a contact having Sn plating, nickel plating and Au plating overlying the substrate. A combination of Sn plating is applied over a copper substrate; nickel plating is applied over the Sn plating; and Au plating is applied over the nickel plating to form a stack. The stack is then processed by a vapor phase Sn reflow step that results in the formation of intermetallics and eliminates stannous oxide layers that may otherwise form on the tin layer. The intermetallic layers provide excellent corrosion resistance, and serve as diffusion barriers to prevent the further migration of either Ni atoms or Cu atoms into the Sn, and Sn atoms outwardly into either the Ni or the Cu. Regardless of the thickness, the interfaces are substantially free of oxides, in particular tin oxide, and not prone to delamination.
Abstract: According to one embodiment, an imprinting apparatus includes an ejecting unit, a stage, a moving unit, and an observation unit. The ejecting unit ejects and drips a hardening resin material onto a substrate to be processed. The substrate to be processed is placed onto the stage. The moving unit relatively moves the ejecting unit and the stage. The observation unit observes the dripped hardening resin material and the pattern with the state in which the dripped hardening resin material and the pattern are overlaid on a plane, before the template is brought into contact with the hardening resin material.
Abstract: A method is provided for measuring the interaction of a disinfecting composition with a floor wax. The method include coating a surface with floor wax, allowing the coating to dry, applying a selected amount of disinfecting composition to the coated surface, and measuring, after a pre-determined amount of time, the tack of the surface, by using a controlled force measurement inverted probe machine. A detectable amount of tack indicates that the disinfecting composition has interacted with the floor wax. Alternatively, any tacky residue on the dried product surface may be sampled and analyzed by Fourier transform spectroscopy. Absorption at a wavelength associated with the floor wax indicates that the product has interacted with the floor wax. A foamable disinfecting composition having reduced interaction with floor wax is also provided.
Type:
Grant
Filed:
March 15, 2013
Date of Patent:
December 15, 2015
Assignee:
GOJO INDUSTRIES, INC.
Inventors:
Amanda Jo Copeland, Jeffrey Ross Davidson
Abstract: Systems and methods in accordance with embodiments of the invention implement layers of metallic glass-based materials. In one embodiment, a method of fabricating a layer of metallic glass includes: applying a coating layer of liquid phase metallic glass to an object, the coating layer being applied in a sufficient quantity such that the surface tension of the liquid phase metallic glass causes the coating layer to have a smooth surface; where the metallic glass has a critical cooling rate less than 1000 K/s; and cooling the coating layer of liquid phase metallic glass to form a layer of solid phase metallic glass.
Abstract: Method for promoting nucleate boiling on an interior surface of a vessel for boiling fluid in an industrial process, the method comprising the steps of: providing the vessel having the interior surface; controllably depositing a scale layer having a non-zero thickness onto the interior surface; monitoring an average thickness, x, of the deposit of the layer; and maintaining the average thickness, x, of the layer below a predetermined value or within a predetermined range of values during the operational life of the vessel, wherein x<k/h, wherein k is the effective thermal conductivity of the interior surface of the vessel and h is the heat transfer coefficient at the interior surface of the vessel in contact with the boiling fluid.
Type:
Grant
Filed:
August 22, 2013
Date of Patent:
December 8, 2015
Assignee:
Massachusetts Institute of Technology
Inventors:
Kripa K. Varanasi, Christopher Jameson Love
Abstract: A relief print master is created with a printhead that jets droplets of a polymerizable liquid on a cylindrical sleeve. The droplets follow a spiral path on the cylindrical sleeve. In a multiple printhead unit, there are different spiral paths associated with the constituting printheads in the multiple printhead unit. The distance between the spiral paths is not even. Preferred embodiments of the current invention provide a method and a system so that the distance between these spiral paths becomes even. The system can also be used for the creation of other types of print masters, such as offset print plates.
Abstract: Disclosed is a paint film which has excellent heat-radiating properties which comprises an undercoat paint film layer which contains from 1 to 20 mass % with respect to the total solid fraction of the paint film of carbon black and a top-coat paint film layer which contains 1 to 40 mass % with respect to the total solid fraction of the paint film of a pearl pigment and which does not contain aluminum powder and the paint film thickness of the top-coat paint film layer is from 11 to 50 ?m.
Abstract: A more efficient process of sealing an anodized aluminum article, which can facilitate higher production rates than conventional sealing techniques, includes steps of providing an article comprised of aluminum or an aluminum alloy that has been anodized, treating the oxide layer with a solution containing an anion capable of combining with a cation to form a water-insoluble precipitate, and contacting the treated oxide layer with a second solution containing a cation which combines with the anion to form a water-insoluble precipitate. In certain embodiments, the oxide layer can be treated with a dye to provide a sealed anodized aluminum article exhibiting enhanced dye retention.
Abstract: A method of synthesizing multilayer heterostructures including an inorganic oxide layer residing on a solid substrate is described. Exemplary embodiments include producing an inorganic oxide layer on a solid substrate by a liquid coating process under relatively mild conditions. The relatively mild conditions include temperatures below 225° C. and pressures above 9.4 mb. In an exemplary embodiment, a solution of diethyl aluminum ethoxide in anhydrous diglyme is applied to a flexible solid substrate by slot-die coating at ambient atmospheric pressure, and the diglyme removed by evaporation. An AlOx layer is formed by subjecting material remaining on the solid substrate to a relatively mild oven temperature of approximately 150° C. The resulting AlOx layer exhibits relatively high light transmittance and relatively low vapor transmission rates for water. An exemplary embodiment of a flexible solid substrate is polyethylene napthalate (PEN). The PEN is not substantially adversely affected by exposure to 150° C.
Type:
Grant
Filed:
March 15, 2011
Date of Patent:
November 3, 2015
Assignee:
Alliance for Sustainable Energy, LLC
Inventors:
Scott R. Hammond, Matthew Reese, Benjamin Rupert, Alexander Miedaner, Calvin Curtis, Dana Olson, David S. Ginley
Abstract: Corrosion inhibitor compositions are provided that can include a mixture of one or more transition metals, one or more organic phosphates, one or more inorganic phosphates, optionally a dispersant, and hydroxyphosphono acetic acid and/or salts thereof. Methods of mitigating or inhibiting corrosion of housing or conduits containing aqueous mediums are also disclosed. The methods can include the steps of pretreating the metal conduit with a mixture of one or more transition metals, one or more organic phosphates, one or more inorganic phosphates, and hydroxyphosphono acetic acid, introducing an aqueous medium into the metal conduit, and injecting a mixture of one or more transition metals, one or more organic phosphates, one or more inorganic phosphates, and hydroxyphosphono acetic acid and/or salts thereof into the aqueous medium.
Type:
Grant
Filed:
March 15, 2013
Date of Patent:
November 3, 2015
Assignee:
Ecolab USA Inc.
Inventors:
Jasbir S. Gill, Danilo Zim, Matheus Paschoalino
Abstract: A process for the production of a dark-color multi-layer coating, comprising the successive steps: (1) applying an NIR-opaque coating layer A? from a solventborne coating composition A to a substrate, (2) applying a coating layer B? from a solventborne coating composition B onto the substrate provided with coating layer A?, (3) subjecting the coated substrate obtained in step (2) to a drying step, (4) applying a clear coat layer, and (5) curing the coating layers simultaneously; wherein both coating compositions A and B comprise binders and crosslinkers comprising melamine-formaldehyde resin crosslinker, wherein both coating compositions A and B comprise certain proportions of cellulose ester binder and NAD binder and/or sheet silicate and/or fumed silica and/or urea SCA and/or polyolefine wax, wherein the pigment content of coating composition A comprises <90 wt.
Abstract: A facility suitable for coating the inside of a pipe element with a mortar that comprises a transport device (32) for feeding dry matter of the mortar that includes a transport chamber (48) and a transport member (54) for transporting the dry matter arranged in the transport chamber, the transport chamber being provided with a dry matter inlet (50) and a dry matter outlet (52); a mixing and projection device (34) for mixing the dry matter with liquid matter to obtain the mortar having a mixing member (82) and a mixing chamber (74) wherein the mixing chamber has a dry matter inlet (76) fed by the dry matter outlet (52), a liquid matter inlet (78) and a mortar outlet (80).
Type:
Grant
Filed:
April 1, 2011
Date of Patent:
October 27, 2015
Assignee:
Saint-Gobain Pam
Inventors:
Victoria Lages, Yann Monnin, José De Sousa, Jean Garrant
Abstract: Methods of treating the surface of a metal-containing hardmask used in the manufacture of semiconductors by contacting the hardmask surface with a composition capable of adjusting the water contact angle so as to substantially match that of subsequently applied organic coatings are provided.
Type:
Grant
Filed:
January 19, 2013
Date of Patent:
October 27, 2015
Assignee:
Rohm and Haas Electronic Materials LLC
Inventors:
Deyan Wang, Peter Trefonas, III, Jieqian Zhang, Peng-Wei Chuang
Abstract: The method for forming a coating film includes: supplying a first liquid from a nozzle to a cylindrical substrate to thereby form the coating film of the first liquid, wherein the method includes, pressing a member including a second liquid, to form a liquid film of the second liquid on the peripheral surface, and forming the coating film of the first liquid includes: supplying the first liquid onto the liquid film of the second liquid formed on the peripheral surface of the substrate to form a bead of the first liquid between the liquid-supplying unit and the liquid film of the second liquid, and extending the bead in a circumferential direction of the substrate.