Patents Examined by Xiaowei Su
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Feedstock and heterogeneous structure for tough rare earth permanent magnets and production therefor
Patent number: 12205762Abstract: New types of particle feedstocks and heterogeneous grain structures are provided for rare earth permanent magnets (REPMs) and their production in a manner to significantly enhance toughness of the magnet with little or no sacrifice in the hard magnetic properties. The novel tough REPMs made from the feedstock have heterogeneous grain structures, such as bi-modal, tri-modal, multi-modal, laminated, gridded, gradient fine/coarse grain structures, or other microstructural heterogeneity and configurations, without changing the chemical compositions of magnets.Type: GrantFiled: October 15, 2018Date of Patent: January 21, 2025Assignee: Iowa State University Research Foundation, Inc.Inventors: Jun Cui, Baozhi Cui -
Patent number: 12194573Abstract: A solder paste contains a flux and a metal powder, wherein the flux contains: 0.5% by mass to 20.0% by mass of a (carboxyalkyl)isocyanurate adduct; 5.0% by mass to 45.0% by mass of a rosin; and a solvent. The (carboxyalkyl)isocyanurate adduct is at least one selected from the group consisting of mono(carboxyalkyl)isocyanurate adducts, bis(carboxyalkyl)isocyanurate adducts and tris(carboxyalkyl)isocyanurate adducts.Type: GrantFiled: March 27, 2020Date of Patent: January 14, 2025Assignee: SENJU METAL INDUSTRY CO., LTD.Inventors: Hiroyoshi Kawasaki, Masato Shiratori, Yuji Kawamata
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Patent number: 12198840Abstract: A rare earth permanent magnet material and a raw Material composition, a preparation method therefor and use thereof. The rare earth permanent magnet material comprises the following components in percentage by mass: 29.0-32.0 wt. % of R, where R comprises RH, and the content of RH is greater than 1 wt. %; 0.30-0.50 wt. % of Cu (not including 0.50 wt. %); 0.10-1.0 wt. % of Co; 0.05-0.20 wt. % of Ti; 0.92-0.98 wt. % of B; and the remainder being Fe and unavoidable impurities; wherein R is a rare-earth element and at least comprises Nd; and RH is a heavy rare-earth element and at least comprises Tb. The R-T-B system permanent magnet material exhibits excellent performance, wherein Br?14.30 kGs, and Hcj?24.1 kOe. The invention can synchronously improve Br and Hcj.Type: GrantFiled: July 22, 2020Date of Patent: January 14, 2025Assignee: FUJIAN GOLDEN DRAGON RARE-EARTH Co., Ltd.Inventors: Qin Lan, Jiaying Huang, Zhixing Xie, Weiguo Mou, Qingfang Huang
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Patent number: 12191060Abstract: Provided a soft magnetic alloy ribbon containing Fe and B. Convex portions having an average convex portion height of 7 nm to 130 nm are present on an alloy surface.Type: GrantFiled: August 23, 2022Date of Patent: January 7, 2025Assignee: TDK CORPORATIONInventors: Kyotaro Abe, Isao Nakahata, Takuya Tsukahara
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Patent number: 12180557Abstract: The present invention relates to a cold rolled steel sheet containing C: 0.15% or more and 0.40% or less, Si: 0.50% or more and 4.00% or less, Mn: 1.00% or more and 4.00% or less, and sol. Al: 0.001% or more and 2.000% or less, having a metallic structure consisting of 35 to 65 area % of ferrite phases, 35 to 65 area % of hard second phases, and 0 to 5 area % of remaining phases, wherein 60% or more of the ferrite phases are recrystallized ferrite phases, an average crystal grain size defined by 15° grain boundaries is 5.0 ?m or less, a maximum connecting rate of the hard second phases is 10% or more, and a two-dimensional isoperimetric constant of the hard second phases is 0.20 or less.Type: GrantFiled: March 31, 2020Date of Patent: December 31, 2024Assignee: NIPPON STEEL CORPORATIONInventors: Shohei Yabu, Koutarou Hayashi, Akihiro Uenishi
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Patent number: 12179291Abstract: A method for step-soldering includes applying a first solder alloy having a melting point in a temperature range from 160 to 210° C. to a jointed portion of a first electronic component and a substrate, and heating them in the temperature range from 160 to 210° C., and applying a second solder alloy having the melting point in a temperature range lower than 160° C. to a joint portion of a second electronic component and the substrate, and heating them in the temperature range lower than 160° C. The first solder alloy consists of 13-22 mass % of In, 0.5-2.8 mass % of Ag, 0.5-5.0 mass % of Bi, 0.002-0.05 mass % of Ni and a balance Sn.Type: GrantFiled: March 27, 2023Date of Patent: December 31, 2024Assignee: SENJU METAL INDUSTRY CO., LTD.Inventors: Takashi Saito, Shunsaku Yoshikawa, Naoko Izumita
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Patent number: 12129532Abstract: The present invention discloses an yttrium-added rare earth permanent magnet material and a preparation method therefor. The chemical formula of the material is expressed as (YxRe1-x)aFe100-a-b-cMbBc according to the mass percentage, wherein 0.05?x?0.5, 20?a?28, 0.5?b?2, 0.5?c?1.5, Re is Nd and/or Pr, and M is Al and/or Nb. According to the present invention, the relatively surplus and inexpensive rare earths yttrium and cerium are used to replace Nd and/or Pr in NdFeB. By controlling the ratio of the rare earth elements such as yttrium, cerium and neodymium, and adding an appropriate amount of Nb and/or Al element, the rare earth elements are used in a comprehensive and balanced manner while better magnetic properties are maintained.Type: GrantFiled: June 20, 2018Date of Patent: October 29, 2024Assignees: GRIREM ADVANCED MATERIALS CO., LTD., GUOKE RE ADVANCED MATERIALS CO., LTD.Inventors: Yang Luo, Dunbo Yu, Jiajun Xie, Caohuan Zhang, Ningtao Quan, Yuanfei Yang, Haijun Peng
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Patent number: 12116649Abstract: The high-strength hot-dip galvanized steel sheet has a specific chemical composition and the following steel microstructure. In a region extending from 300 to 400 ?m from a surface layer of the steel sheet in a thickness direction of the steel sheet, the total area fraction of martensite and bainite containing carbides is 60 to 100%, and the average grain size of prior austenite is 15 ?m or less. In the region extending from 300 to 400 ?m from the surface layer of the steel sheet in the thickness direction of the steel sheet, the ratio of the height of a peak of P in an Auger electron spectrum at a position 5 nm or more from a prior-austenite grain boundary to the height of a peak of P in an Auger electron spectrum at the prior-austenite grain boundary is 0.20 or more.Type: GrantFiled: August 23, 2019Date of Patent: October 15, 2024Assignee: JFE Steel CorporationInventors: Hiroshi Hasegawa, Tatsuya Nakagaito, Yuki Takeda
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Patent number: 12116648Abstract: An object is to provide a cold-rolled steel sheet having excellent phosphatability, even in the case where a phosphating solution has a low temperature, and a method for manufacturing the steel sheet, and a cold-rolled steel sheet for annealing. A cold-rolled steel sheet for annealing has a chemical composition containing C: 0.01 mass % to 0.30 mass %, Si: less than 0.10 mass % (including 0.0 mass %), Mn: 2.0 mass % to 3.5 mass %, P: 0.05 mass % or less, S: 0.01 mass % or less, and Al: 0.15 mass % or less, the balance being Fe and inevitable impurities, in which Si and/or Si oxide exists on a surface of the steel sheet with an average coating thickness of 1 nm to 20 nm.Type: GrantFiled: March 20, 2019Date of Patent: October 15, 2024Assignee: JFE Steel CorporationInventors: Hiroyuki Masuoka, Shinichi Furuya, Akira Matsuzaki, Hayato Takeyama
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Patent number: 12104217Abstract: Provided is a grain-oriented electrical steel sheet having a film that is effective for the magnetic properties of the steel sheet and particularly effective for iron loss reduction and has favorable adhesion. In a grain-oriented electrical steel sheet, an insulating film partially enters into a steel substrate to form an anchor part, a depth of the anchor part from the surface of the steel substrate is 3.5 ?m or less, and a number of neck parts of 5 ?m2 or less in area is 0.06/?m2 or less and a number of neck parts of 10 ?m2 to 40 ?m2 in area is 0.005/?m2 or more and 0.011/?m2 or less, where each neck part is a remaining part of the insulating film on the surface of the steel substrate when peeling the insulating film from the steel substrate in a bend test for the grain-oriented electrical steel sheet.Type: GrantFiled: March 27, 2020Date of Patent: October 1, 2024Assignee: JFE STEEL CORPORATIONInventors: Makoto Watanabe, Masanori Takenaka, Takashi Terashima
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Patent number: 12104219Abstract: Grain-oriented electrical steel sheet excellent in magnetic properties and excellent in adhesion of a primary coating to the steel sheet is provided. The grain-oriented electrical steel sheet is provided with a base steel sheet having a chemical composition containing C: 0.005% or less, Si: 2.5 to 4.5%, Mn: 0.050 to 1.000%, a total of S and Se: 0.005% or less, sol. Al: 0.005% or less, and N: 0.005% or less and having a balance of Fe and impurities and a primary coating having Mg2 SiO4 as a main constituent formed on a surface of the base steel sheet. A peak position of Al emission intensity obtained when conducting elemental analysis by glow discharge spectrometry from a surface of the primary coating in a thickness direction is present in a range of 2.0 to 12.0 ?m from a surface of the primary coating to the thickness direction. A sum of perimeters of the Al oxides at the peak position of Al emission intensity is 0.20 to 1.00 ?m/?m2, and a number density of Al oxides is 0.02 to 0.20/?m2.Type: GrantFiled: January 12, 2023Date of Patent: October 1, 2024Assignee: NIPPON STEEL CORPORATIONInventors: Ichiro Tanaka, Ryutaro Yamagata, Nobusato Morishige, Takashi Kataoka, Masaru Takahashi
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Patent number: 12090533Abstract: Provided is a method for rolling a steel sheet and a method for manufacturing a steel sheet capable of preventing occurrence of defects in appearance of a steel sheet caused by oil spots of a coolant and preventing occurrence of defects in shape of a steel sheet by appropriately controlling thermal deformation of work rolls. The method for rolling a steel sheet according to the present invention is a method for rolling a steel sheet involving feeding of a coolant to rolls that form a rolling mill during the rolling. The method includes keeping a coolant feeding rate at or lower than a predetermined rate lower than an upper constant rate at a start of operation of the rolling mill, and increasing the coolant feeding rate to the upper constant rate in response to an amount of center buckles of the steel sheet reaching or exceeding an upper target value.Type: GrantFiled: December 26, 2019Date of Patent: September 17, 2024Assignee: JFE Steel CorporationInventors: Ken Kurisu, Kentaro Ishii, Kazuma Takeuchi
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Patent number: 12080478Abstract: A gradient Nd—Fe—B magnet includes an Nd—Fe—B magnet block extending along a magnetization direction and having a plurality of surfaces perpendicular to the magnetization direction. A first film, is disposed on one of the surfaces. A second film is disposed on another one of the surfaces, opposite of the one of the surfaces. The first film and the second film are diffused into the Nd—Fe—B magnet block dividing the Nd—Fe—B magnet block into an edge region, a transition region, and a central region along a plane perpendicular to the magnetization direction wherein the edge region has a coercivity that remains constant in a direction perpendicular to the magnetization direction, and the coercivity, along said magnetization direction, gradually decreases from the one of the surfaces and the another one of the surfaces towards a point located therebetween. A method of making the gradient Nd—Fe—B magnet is disclosed herein.Type: GrantFiled: July 1, 2019Date of Patent: September 3, 2024Assignee: YANTAI SHOUGANG MAGNETIC MATERIALS INC.Inventors: Kunkun Yang, Zhongjie Peng, Chuanshen Wang
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Patent number: 12074475Abstract: A rare earth permanent magnet has a first surface and satisfies A1<B1, A1?C1, and A1?D1 where A1 is a coercive force of a portion a1 including a center of gravity of the first surface, B1 is a coercive force of a portion b1, C1 is a coercive force of a portion c1, and D1 is a coercive force of a portion d1, and a heavy rare earth element is present on a top layer of the first surface.Type: GrantFiled: March 22, 2021Date of Patent: August 27, 2024Assignee: TDK CorporationInventor: Takuma Hayakawa
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Patent number: 12062472Abstract: The present disclosure provides neodymium-iron-boron magnetic body having gradient distribution, comprising an ease-to-demagnetize zone and a hard-to-demagnetize zone, wherein in a direction perpendicular to magnetization direction, remanence of the ease-to-demagnetize zone is less than remanence of the hard-to-demagnetize zone, and coercivity of the ease-to-demagnetize zone is greater than coercivity of the hard-to-demagnetize zone; and along the direction perpendicular to magnetization direction, the remanence and the coercivity of the ease-to-demagnetize zone are respectively a constant value, and the remanence and the coercivity of the hard-to-demagnetize zone are respectively a constant value. Due to the gradient distribution of remanence and coercivity of the neodymium-iron-boron magnetic body provided by the present application, the remanence, coercivity, magnetic flux and surface magnetic field of the neodymium-iron-boron magnetic body are optimized.Type: GrantFiled: August 24, 2020Date of Patent: August 13, 2024Assignee: JL MAG RARE EARTH CO., LTD.Inventors: Minghuo Liao, Baogui Cai, Yong Liu, Haiming Wu
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Patent number: 12046399Abstract: A permanent magnet formed by additively manufacturing magnetic phases and buffer phases is disclosed. The buffer phase(s) may improve performance, enhance mechanical properties and allow the magnet to better tolerate stresses such that defects such as cracking do not occur or are less likely to occur. The buffer phase may be a magnetic or non-magnetic material.Type: GrantFiled: January 27, 2022Date of Patent: July 23, 2024Assignee: Ford Global Technologies, LLCInventors: Wanfeng Li, Chuanbing Rong, Michael W. Degner
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Patent number: 12046398Abstract: A method for producing a permanent or soft magnet including the following steps: a) providing: a solution containing a solvent in which are dispersed a set of objects which possess a permanent magnetic moment; a substrate on which are fixed to the surface or within a cavity that it may have, a 1st pad and a 2nd pad, said 1st pad includes a face facing and parallel to a face that the 2nd pad includes; b) the solution is deposited on the surface of the substrate or, as the case may be, within its cavity; c) the substrate is placed in a magnetic field so that the set of objects are grouped together between the face of the 1st pad and the face of the 2nd pad so as to form a permanent magnet.Type: GrantFiled: December 12, 2019Date of Patent: July 23, 2024Assignees: INSTITUT NATIONAL DES SCIENCES APPLIQUÉES, UNIVERSITE PAUL SABATIER (TOULOUSE III), CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUEInventors: Lise-Marie Lacroix, Guillaume Viau, Thierry Leichle, Pierre Moritz
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Patent number: 12037655Abstract: Provided is an electric resistance welded steel pipe or tube that develops no quench cracks despite having carbon content of 0.40% or more and has excellent fatigue strength. An electric resistance welded steel pipe or tube comprises: a chemical composition containing, in mass %, C: 0.40% to 0.55%, Si: 0.10% to 1.0%, Mn: 0.10% to 2.0%, P: 0.10% or less, S: 0.010% or less, Al: 0.010% to 0.100%, Cr: 0.05% to 0.30%, Ti: 0.010% to 0.050%, B: 0.0005% to 0.0030%, Ca: 0.0001% to 0.0050%, and N: 0.0005% to 0.0050%, with a balance consisting of Fe and inevitable impurities; and a ferrite decarburized layer at each of an outer surface and an inner surface, the ferrite decarburized layer having a depth of 20 ?m to 50 ?m from the surface.Type: GrantFiled: September 18, 2019Date of Patent: July 16, 2024Assignee: JFE STEEL CORPORATIONInventors: Masatoshi Aratani, Ryoji Matsui, Tomonori Kondou
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Patent number: 12030122Abstract: Provided is a method of manufacturing a soft magnetic dust core. The method includes: preparing coated powder including amorphous powder made of an Fe-B-Si-P-C-Cu-based alloy, an Fe-B-P-C-Cu-based alloy, an Fe-B-Si-P-Cu-based alloy, or an Fe-B-P-Cu-based alloy, with a first initial crystallization temperature Tx1 and a second initial crystallization temperature Tx2; and a coating formed on a surface of particles of the amorphous powder; applying a compacting pressure to the coated powder or a mixture of the coated powder and the amorphous powder at a temperature equal to or lower than Tx1?100 K; and heating to a maximum end-point temperature equal to or higher than Tx1?50 K and lower than Tx2 with the compacting pressure being applied.Type: GrantFiled: October 21, 2020Date of Patent: July 9, 2024Assignees: JFE STEEL CORPORATION, TOKIN CORPORATION, National Institute of Advanced Industrial Science and TechnologyInventors: Naomichi Nakamura, Makoto Nakaseko, Takuya Takashita, Mineo Muraki, Hoshiaki Terao, Raita Wada, Akiri Urata, Yu Kanamori, Makoto Yamaki, Koichi Okamoto, Toshinori Tsuda, Shoichi Sato, Kimihiro Ozaki
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Patent number: 12006560Abstract: Provided is an Fe-based nanocrystalline alloy powder. The Fe-based nanocrystalline alloy powder has a chemical composition, excluding inevitable impurities, represented by a composition formula of FeaSibBcPdCueMf, where the M in the composition formula is at least one element selected from the group consisting of Nb, Mo, Zr, Ta, W, Hf, Ti, V, Cr, Mn, C, Al, S, O, and N, 79 at %?a?84.5 at %, 0 at %?b<6 at %, 0 at %<c?10 at %, 4 at %<d?11 at %, 0.2 at %?e?0.53 at %, 0 at %?f?4 at %, a+b+c+d+e+f=100 at %, a degree of crystallinity is more than 10% by volume, and an Fe crystallite diameter of the Fe-based nanocrystalline alloy powder is 50 nm or less.Type: GrantFiled: February 27, 2023Date of Patent: June 11, 2024Assignee: JFE STEEL CORPORATIONInventors: Naoki Yamamoto, Takuya Takashita, Makoto Nakaseko, Akio Kobayashi, Akiri Urata, Miho Chiba