Patents by Inventor Adel F. Halasa

Adel F. Halasa has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20240136550
    Abstract: A method of manufacturing a hydrogen fuel cell hose and component parts is disclosed herein, including blending a formaldehyde-based, semi-crystalline engineering thermoplastic with graphene, wherein the graphene has a thickness of less than about 3.2 nm, a particle size of between about 50 nm and about 10 ?m, and contains greater than about 95% carbon, exfoliating the graphene into plates, wherein the graphene plates having substantially no carboxylic acid, alcohols, ketones, aldehydes, or hydroxyl groups on the graphene plate surface or graphene plate edges, and aligning the graphene plates into perpendicular alignment, such that the graphene plates provide a barrier to migration of oxygen, nitrogen, moisture, or water vapor molecules.
    Type: Application
    Filed: May 24, 2023
    Publication date: April 25, 2024
    Inventors: Douglas PASCHALL, Michael Brendan RODGERS, Adel F. HALASA
  • Publication number: 20230391989
    Abstract: Graphene is an allotrope or one of the several physical forms of carbon, other examples being graphite, fullerenes, and diamond. At the atomic level, it is in the form a sheet with a thickness nominally under 1.0 nanometer and up to 1 micron in diameter. Sheets of such dimensions when added to other composites facilitate increases in thermal and electrical conductivity and in the case of elastomer nanocomposites, improvements in hysteresis, compounding ingredient dispersion, aging resistance, and reductions in permeability. In the case of conveyor belt cover compounds, natural rubber based formulations are preferred due to high tensile strength, tear strength and damage resistance, and high resistance to abrasion. Graphene as a performance additive enables further improvement in these critical properties.
    Type: Application
    Filed: June 6, 2023
    Publication date: December 7, 2023
    Inventors: Douglas PASCHALL, Michael Brendan RODGERS, Adel F. HALASA
  • Publication number: 20230383091
    Abstract: A method for improving processing speed, dimensional stability, and physical properties in extruded elastomers is herein disclosed, including the steps of mixing natural rubber with pristine graphene, the pristine graphene acting as a nucleating agent for strain induced crystallization of the natural rubber, and the pristine graphene inducing additional shear during mixing.
    Type: Application
    Filed: May 24, 2023
    Publication date: November 30, 2023
    Inventors: Douglas PASCHALL, Michael Brendan RODGERS, Adel F. HALASA
  • Patent number: 11753529
    Abstract: The introduction of graphene as an additive in rubber compounds is disclosed. The product shows increased barrier protection for tire sidewalls, with no tradeoffs in other characteristics.
    Type: Grant
    Filed: July 14, 2022
    Date of Patent: September 12, 2023
    Inventors: Douglas Paschall, Adel F. Halasa, Michael Brendan Rodgers
  • Patent number: 11738599
    Abstract: The introduction of graphene as an additive in rubber compounds is disclosed. The product shows increased barrier protection for tire innerliners, with no tradeoffs in other characteristics.
    Type: Grant
    Filed: July 15, 2022
    Date of Patent: August 29, 2023
    Inventors: Douglas Paschall, Adel F. Halasa, Michael Brendan Rodgers
  • Patent number: 11655355
    Abstract: The introduction of graphene as an additive in rubber compounds is disclosed. The product shows increased barrier protection for tire innerliners, with no tradeoffs in other characteristics. A rubber compound is disclosed herein including butyl rubber and graphene plate, wherein the graphene plate has a thickness of less than about 3.2 nm, a particle size of between about 50 nm and about 10 ?m, and contains greater than about 95% carbon.
    Type: Grant
    Filed: May 11, 2022
    Date of Patent: May 23, 2023
    Assignee: AKRON POLYMER SOLUTIONS, INC.
    Inventors: Douglas Paschall, Adel F. Halasa
  • Publication number: 20230130750
    Abstract: An aircraft tire component is disclosed herein, including natural rubber, a peptizer, carbon black, graphene, wherein the graphene has a thickness of less than about 3.2 nm, a particle size of between about 50 nm and about 10 ?m, and contains greater than about 95% carbon, aliphatic hydrocarbon resin, treated distillate aromatic extract, N-(1,3-dimethylbutyl)-N?-phenyl-1,4-benzenediamine, 2,2,4-trimethyl-1,2-dihydroquinoline, paraffinic wax, microcrystalline wax, zinc oxide, stearic acid, N-tert-butyl-benzothiazole sulfonamide, sulfur, and pre vulcanization inhibitor, wherein the aircraft tire component is chosen from the group consisting of a tread, an inner liner, and a sidewall.
    Type: Application
    Filed: December 15, 2022
    Publication date: April 27, 2023
    Inventors: Douglas PASCHALL, Michael Brendan RODGERS, Adel F. HALASA
  • Patent number: 11597821
    Abstract: The introduction of graphene as an additive in truck tire treads is disclosed. The product shows increased electrical resistance in tire treads, with no tradeoffs in other characteristics.
    Type: Grant
    Filed: July 14, 2022
    Date of Patent: March 7, 2023
    Inventors: Douglas Paschall, Adel F. Halasa, Michael Brendan Rodgers
  • Publication number: 20230034747
    Abstract: The introduction of graphene as an additive in rubber compounds is disclosed. The product shows increased barrier protection for tire sidewalls, with no tradeoffs in other characteristics.
    Type: Application
    Filed: July 14, 2022
    Publication date: February 2, 2023
    Inventors: Douglas PASCHALL, Adel F. HALASA, Michael Brendan RODGERS
  • Publication number: 20230031239
    Abstract: The introduction of graphene as an additive in truck tire treads is disclosed. The product shows increased electrical resistance in tire treads, with no tradeoffs in other characteristics.
    Type: Application
    Filed: July 14, 2022
    Publication date: February 2, 2023
    Inventors: Douglas PASCHALL, Adel F. HALASA, Michael Brendan RODGERS
  • Publication number: 20230033641
    Abstract: The introduction of graphene as an additive in rubber compounds is disclosed. The product shows increased barrier protection for tire innerliners, with no tradeoffs in other characteristics.
    Type: Application
    Filed: July 15, 2022
    Publication date: February 2, 2023
    Inventors: Douglas PASCHALL, Adel F. HALASA, Michael Brendan RODGERS
  • Publication number: 20220363874
    Abstract: The introduction of graphene as an additive in rubber compounds is disclosed. The product shows increased barrier protection for tire innerliners, with no tradeoffs in other characteristics. A rubber compound is disclosed herein including butyl rubber and graphene plate, wherein the graphene plate has a thickness of less than about 3.2 nm, a particle size of between about 50 nm and about 10 ?m, and contains greater than about 95% carbon.
    Type: Application
    Filed: May 11, 2022
    Publication date: November 17, 2022
    Inventors: Douglas PASCHALL, Adel F. HALASA
  • Patent number: 5629256
    Abstract: The subject invention relates to an anionic polymerization technique for synthesizing rubbery polymers of conjugated diolefin monomers, such as rubbery copolymer of .alpha.-methylstyrene and 1,3-butadiene. These rubbery copolymers exhibit an excellent combination of properties for utilization in tire tread rubber compounds. They have high trans-isomer contents which leads to good treadwear characteristics and a broad molecular weight distribution which enhances processability.
    Type: Grant
    Filed: July 29, 1996
    Date of Patent: May 13, 1997
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Adel F. Halasa, Laurie E. Austin, Susan A. Weakland
  • Patent number: 5627237
    Abstract: This invention reveals a pneumatic tire having an outer circumferential tread wherein said tread is a sulfur-cured rubber composition comprised of, based on 100 parts by weight of rubber, (1) from about 5 to about 50 parts of 3,4-polyisoprene rubber, wherein said 3,4-polyisoprene rubber has (a) a 3,4-isomer content of from 75 percent to 95 percent, (b) a 1,2-isomer content of from 5 percent to 25 percent, (c) a glass transition temperature from 0.degree. to 25.degree. C. and (d) a number average molecular weight which is within the range of 30,000 to 180,000; and (2) from about 50 to about 95 parts of a rubbery polymer which is co-curable with the 3,4-polyisoprene rubber.
    Type: Grant
    Filed: May 6, 1996
    Date of Patent: May 6, 1997
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Adel F. Halasa, Wen-Liang Hsu, David J. Zanzig, Gerald L. Allen, Laurie E. Austin
  • Patent number: 5623035
    Abstract: The subject invention relates to an anionic polymerization technique for synthesizing rubbery polymers of conjugated diolefin monomers, such as a rubbery copolymer of .alpha.-methylstyrene and 1,3-butadiene. These rubbery copolymers exhibit an excellent combination of properties for utilization in tire tread rubber compounds. They have high trans-isomer contents which leads to good treadwear characteristics and a broad molecular weight distribution which enhances processability.
    Type: Grant
    Filed: July 21, 1995
    Date of Patent: April 22, 1997
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Adel F. Halasa, Laurie E. Austin, Susan A. Weakland
  • Patent number: 5620939
    Abstract: This invention reveals an initiator system which is comprised of (a) a lithium initiator, (b) a sodium alkoxide, and (c) a polar modifier; wherein the molar ratio of the sodium alkoxide to the polar modifier is within the range of about 0.1:1 to about 10:1; and wherein the molar ratio of the sodium alkoxide to the lithium initiator is within the range of about 0.01:1 to about 20:1.
    Type: Grant
    Filed: April 1, 1996
    Date of Patent: April 15, 1997
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Adel F. Halasa, Wen-Liang Hsu, David J. Zanzig, Paul H. Sandstrom, Steven K. Henning, Danielle Lucas
  • Patent number: 5616653
    Abstract: The subject invention discloses a process for preparing a coupled styrene-isoprene-butadiene rubber which is particularly valuable for use in making automobile tire tread rubber compounds which comprises the steps of (1) solution terpolymerizing in an organic solvent from about 5 weight percent to about 40 weight percent styrene, from about 1 weight percent to about 10 weight percent isoprene, and from about 50 weight percent to about 94 weight percent 1,3-butadiene, based on total monomers, to a conversion of at least about 90% to produce a living styrene-isoprene-butadiene polymer, wherein the terpolymerization is initiated with an organolithium compound, and wherein the terpolymerization is conducted in the presence of a polar modifier at a molar ratio of the polar modifier to the organolithium compound, which is within the range of about 0.5:1 to about 5:1, and wherein the terpolymerization is conducted at a temperature which is within the range of about 20.degree. C. to about 150.degree. C.
    Type: Grant
    Filed: July 29, 1996
    Date of Patent: April 1, 1997
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Wen-Liang Hsu, Adel F. Halasa, Barry A. Matrana, Scott M. Christian, Laurie E. Austin, Bill B. Gross
  • Patent number: 5612436
    Abstract: The subject invention discloses an isoprene-butadiene diblock rubber which is particularly valuable for use in making treads for tires which have improved wear characteristics without compromising traction characteristics or rolling resistance. Said isoprene-butadiene diblock rubber is comprised of (1) a first block which is comprised of repeat units which are derived from 1,3-butadiene and (2) a second block which is comprised of repeat units which are derived from both 1,3-butadiene and isoprene, wherein the repeat units derived from isoprene and 1,3-butadiene in the second block are in an essentially random order, wherein the diblock rubber has a glass transition temperature which is within the range of about -100.degree. C. to about -70.degree. C., and wherein the diblock rubber has a Mooney viscosity which is within the range of about 50 to about 140.
    Type: Grant
    Filed: September 8, 1995
    Date of Patent: March 18, 1997
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Adel F. Halasa, Wen-Liang Hsu, David J. Zanzig, Paul H. Sandstrom, Laurie E. Austin
  • Patent number: 5595951
    Abstract: The subject invention discloses a process for preparing an initiator which contains a plurality of lithium atoms and which is particularly useful for initiating the polymerization of diolefin monomers into rubbery polymers; said process being comprised of reacting an alkyl lithium compound with an unsaturated hydrocarbon containing allylic, benzylic or aryl hydrogen atoms, wherein said process is conducted in the presence of a member selected from the group consisting of alkali metal alkoxides, alkali metal phenoxides, and chelating tertiary alkyl 1,2-ethylene diamines. After the initiators of this invention have been prepared they can be employed to initiate the polymerization of diolefin monomers into rubbery polymers. They can, of course, also be employed to initiate the copolymerization of diolefin monomers and vinyl aromatic monomers into rubbery polymers. These rubbery polymers can then be used in making tire tread compounds for automobiles and trucks.
    Type: Grant
    Filed: March 16, 1995
    Date of Patent: January 21, 1997
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: Adel F. Halasa, George Jalics
  • Patent number: 5552490
    Abstract: The subject invention relates to a technique for synthesizing rubbery copolymers of styrene and isoprene. These rubbery copolymers exhibit an excellent combination of properties for utilization in tire tread rubber compounds. By utilizing these styrene-isoprene rubbers in tire treads, tires having improved wet skid resistance can be built without sacrificing rolling resistance or tread wear characteristics.
    Type: Grant
    Filed: May 12, 1995
    Date of Patent: September 3, 1996
    Assignee: The Goodyear Tire & Rubber Company
    Inventors: David J. Zanzig, Paul H. Sandstrom, Joseph K. Hubbell, Wen-Liang Hsu, Adel F. Halasa, John J. A. Verthe