Abstract: A method for inhibiting scale formation in an oil or gas well is provided. Specifically, the method is a novel "squeeze" application. The squeeze comprises injecting three solutions into the oil or gas well: (1) the preflush solution, (2) the pill solution, and (3) the overflush solution. After the injection of the three solutions, the well is shut-in for about 24 to about 48 hours. The squeeze application is useful regardless of whether the mechanism for inhibitor fixation is adsorption or precipitation.

Abstract: A process for measurement of low levels of phosphonates in brine waters wherein the phosphonate samples are acidified with hydrochloric acid promptly upon removal from an oil or gas well to prevent phosphonate precipitation or adsorption. The hydrochloric acid acidified phosphonate is digested in the presence of an oxidizing agent at elevated temperature and pressure for sufficient time to oxidize substantially all of the phosphonate to orthophosphate. The phosphorous containing compound is extracted with an organic extractant, preferably selected from the group consisting of methyl iso-butyl ketone/cyclohexane mixture and ethyl acetate, followed by color development for absorption spectrophotometry.