Abstract: A process and an apparatus for the separation of a homogeneous catalyst solution from crude monoethylene glycol (MEG) and for purifying MEG is provided. The apparatus includes a catalyst separation section, an MEG rectification section, a stripping section and a pasteurization section, wherein the MEG rectification and pasteurization sections are located within a MEG purification column, and the catalyst separation section is either located in the MEG purification column or in a separate upstream vessel, and wherein the catalyst separation section includes a crude MEG vapor feed inlet to the MEG rectification section.

Abstract: A heat integration system for removing heat of reaction from an EC-1 Reactor and generating Chilled liquid for use by one or more Consumer Units, in a catalytic process for producing EC from EO for conversion into MEG wherein the system comprises an EC-1 Reactor Cooler suitable for removing heat from an EC-1 Reactor, an Intermediate Loop which is in communication with the Reactor Cooler and with an absorption Refrigeration Unit, and which is suitable for conducting Intermediate liquid therebetween, the absorption Refrigeration Unit being suitable for generating Chilled liquid, and a Chilled liquid loop suitable for conducting Chilled liquid generated in the absorption Refrigeration Unit for use by one or more Consumer Units.

Abstract: A process and an apparatus for the separation of a homogeneous catalyst solution from crude monoethylene glycol (MEG) and for purifying MEG is disclosed. The process comprises separating catalyst solution by evaporating crude MEG and feeding crude MEG to a rectification section, a stripping section, and thence to a pasteurisation section, each section operated at subatmospheric pressure of 0.5=105 Nm?2 or less, the rectification and pasteurisation sections being at pressure less than that of the catalyst separation section, wherein the process provides a pressure differential across the catalyst separation and rectification sections and wherein vapour phase crude MEG from the catalyst separation section is fed as substantially vapour phase feed to the rectification section.

Abstract: A process and an apparatus for the separation of a homogeneous catalyst solution from crude monoethylene glycol (MEG) and for purifying MEG is disclosed. The process comprises separating catalyst solution by evaporating crude MEG and feeding crude MEG to a rectification section, a stripping section, and thence to a pasteurisation section, each section operated at subatmospheric pressure of 0.5×105 Nm?2 or less, the rectification and pasteurisation sections being at pressure less than that of the catalyst separation section, wherein the process provides a pressure differential across the catalyst separation and rectification sections and wherein vapour phase crude MEG from the catalyst separation section is fed as substantially vapour phase feed to the rectification section.

Abstract: Integrated preparation and separation process comprising a preparation process wherein a byproduct is produced; and a gas separation process wherein a first component is separated from a mixture of components by diffusion of the first component through a porous partition into a stream of sweeping component; wherein the byproduct produced in the preparation process is subsequently used as the sweeping component in the separation process, and an industrial set-up for use in such a process.

Abstract: The invention provides a process for the preparation of an alkaline glycol from an alkaline carbonate, wherein alkaline carbonate is hydrolyzed in the presence of catalyst in a baffled reactor. The baffled reactor has at least four compartments, the compartments are formed by internal baffles and the internal baffles provide a sinuous route for reaction fluid through the reactor.

Abstract: The invention provides a process for the preparation of an alkylene glycol from an alkylene carbonate, wherein alkylene carbonate is hydrolysed in the presence of catalyst in a baffled reactor. The baffled reactor has at least four compartments, the compartments are formed by internal baffles and the internal baffles provide a sinuous route for reaction fluid through the reactor.

Abstract: A heat integration system for removing heat of reaction from an EC-1 Reactor and generating Chilled liquid for use by one or more Consumer Units, in a catalytic process for producing EC from EO for conversion into MEG wherein the system comprises an EC-1 Reactor Cooler suitable for removing heat from an EC-1 Reactor, an Intermediate Loop which is in communication with the Reactor Cooler and with an absorption Refrigeration Unit, and which is suitable for conducting Intermediate liquid therebetween, the absorption Refrigeration Unit being suitable for generating Chilled liquid, and a Chilled liquid loop suitable for conducting Chilled liquid generated in the absorption Refrigeration Unit for use by one or more Consumer Units, the system being such that the absorption Refrigeration Unit uses heat generated in the EC-1 Reactor to generate Chilled liquid for the Chilled liquid loop and Consumer Unit(s), wherein the system additionally comprises a Shutdown Cooler having an independent cooling source which is suita