Patents by Inventor Antonio Clareti Pereira

Antonio Clareti Pereira has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 9663842
    Abstract: It is described a method for recovering rare earth elements from low grade ores including a first metal selected group containing at least one of iron and aluminum and a second metal selected from the group consisting of at least of the rare earth elements (lanthanum, cerium, praseodymium, neodymium, promethium, samarium, europium, gadolinium, terbium, dysprosium, holmium, erbium, thulium, ytterbium, lutetium, yttrium and scandium), the method comprising the steps of: (i) contacting the ore with sulfuric acid to obtain sulfates of the first group of metals, (ii) subjecting the mixture to high temperatures in order to convert the first group of sulfates into phosphates or other stable species and the second group into sulfates, (iii) adding water to the cool mixture, selectively dissolving the rare earth elements and (iv) subjecting the rare earth solution to a purification process.
    Type: Grant
    Filed: May 3, 2013
    Date of Patent: May 30, 2017
    Assignee: VALE S.A.
    Inventors: Tiago Valentim Berni, Antonio Clareti Pereira, Flávia Dutra Mendes, João Alberto Lessa Tude
  • Patent number: 9169534
    Abstract: A method of recovering base metals from sulphide ores and concentrates includes mixing the base metals ore with ferric salts, heating the mixture, adding water to form a pulp, and stirring and filtering the pulp.
    Type: Grant
    Filed: July 23, 2013
    Date of Patent: October 27, 2015
    Assignee: VALE S.A.
    Inventors: Tiago Valentim Berni, Antonio Clareti Pereira, Felipe Hilario Guimarães
  • Patent number: 8961649
    Abstract: A method for recovering base metal values from oxide ore is provided by the present disclosure. The ore includes a first metal selected from the group consisting at least one of iron and aluminum and a second metal selected from the group consisting of at least one of nickel, cobalt and copper. The method includes the steps of: contacting the oxide ore with hydrogen chloride gas to obtain chlorides of the first and second metals and subjecting at least the first and second metals to pyrohydrolysis at a predetermined temperature to decompose the chlorides of the first metal into oxides. The method also includes the step of mixing the oxides of the first metal and the chlorides of the second metal in an aqueous solution to dissolve the chlorides of the second metal and recovering the dissolved ions of the second metal from the aqueous solution.
    Type: Grant
    Filed: August 26, 2008
    Date of Patent: February 24, 2015
    Assignee: Vale Canada Limited
    Inventors: Antonio Clareti Pereira, Flavia Dutra Mendes, Tiago Valentim Berni, Ahmed Vahed
  • Patent number: 8802042
    Abstract: A method for recovering base metal values from oxide ore is provided, where the ore includes a first group metal selected from nickel, cobalt and copper. The method includes reducing ore particle size to suit the latter unit operation, favoring contact for the metal elements, contacting the ore with ferric or ferrous chloride, hydrated or anhydrous, to produce a mix of ore and iron (II or III) chloride subjecting the mixture of the ore and ferric or ferrous chloride to enough energy to decompose the chlorides into hydrochloric acid and a iron oxides from the second group, forming their respective chlorides, selectively dissolve the produced base metal chlorides, leaving the metal as oxides and in the solid state, and recovering the dissolved base metal values from aqueous solution.
    Type: Grant
    Filed: July 14, 2010
    Date of Patent: August 12, 2014
    Assignee: Vale S.A.
    Inventors: Antonio Clareti Pereira, Tiago Valentim Berni
  • Patent number: 8747795
    Abstract: Aspects of the present invention refers to a process for production of nickel carbonate including preparing a magnesium salt solution, contacting the solution with a stream of gaseous CO2, keeping pH between 4 and 10 and temperature between 0 and 100° C., during up to 5 hours to produce a first mixture, contacting the first mixture with a nickel sulphate solution to produce a second mixture, performing a separation of liquid and solid portions of the second mixture, and feeding the magnesium salt solution with the liquid portion. This process recycles the reagent used for producing nickel carbonate and yields a final product that is easy to handle and transport.
    Type: Grant
    Filed: March 26, 2012
    Date of Patent: June 10, 2014
    Assignee: Vale S.A.
    Inventors: Tiago Valentim Berni, Antonio Clareti Pereira, Felipe Hilario Guimar{hacek over (a)}es
  • Publication number: 20140020510
    Abstract: The present invention discloses a new recovery of base metals from sulphide ores and concentrates, which comprises mixing the base metal's ore with ferric salts, heating the said mixture; adding water to form a pulp, stirring and filtering the pulp.
    Type: Application
    Filed: July 23, 2013
    Publication date: January 23, 2014
    Applicant: VALE S/A
    Inventors: Tiago Valentim BERNI, Antonio Clareti PEREIRA, Felipe Hilario GUIMARÃES
  • Patent number: 8628739
    Abstract: The present invention refers to a direct purification process of a nickel laterite leaching effluent including adjusting a pH of a leaching solution, employing an ion exchange resin to adsorb nickel and copper selectively over ferric or ferrous iron, and recovering nickel.
    Type: Grant
    Filed: February 1, 2012
    Date of Patent: January 14, 2014
    Assignee: Vale
    Inventors: Tiago Valentim Berni, Antonio Clareti Pereira
  • Patent number: 8597601
    Abstract: A process to use ferric sulphate equilibrium to reduce overall acid consumption and iron extraction, the process comprising the steps of: (i) sulphating; (ii) selective pyrolysis and (iii) selective dissolution.
    Type: Grant
    Filed: June 1, 2012
    Date of Patent: December 3, 2013
    Assignee: Vale S.A.
    Inventors: Tiago Valentim Berni, Antonio Clareti Pereira, Flavia Dutra Mendes
  • Patent number: 8470272
    Abstract: The present invention resides in a process of recovering nickel and cobalt, regenerating the main raw materials, said process including the steps of: granulometric separation; leaching; neutralization; MHP production in only one stage and the pressure crystallization of magnesium sulphite. The process proposes a way to recovery nickel and cobalt from laterite ores through the atmospheric and heap leaching with staged addition of ore—by size separation—and H2SO4, decreasing the nickel losses and simplifying the neutralization circuit and producing a more purified MHP. The present process route is employed for nickel extraction, including the one from high magnesium containing lateritic ores.
    Type: Grant
    Filed: June 1, 2009
    Date of Patent: June 25, 2013
    Assignee: Vale S.A.
    Inventors: Antonio Clareti Pereira, Felipe Hilario Guimaraes, Joao Alberto de Lessa Tude, Lino Rodrigues de Freitas, Tiago Valentim Berni
  • Publication number: 20130028816
    Abstract: A process to use ferric sulphate equilibrium to reduce overall acid consumption and iron extraction, the process comprising the steps of: (i) sulphating; (ii) selective pyrolysis and (iii) selective dissolution.
    Type: Application
    Filed: June 1, 2012
    Publication date: January 31, 2013
    Applicant: Vale S/A
    Inventors: Tiago Valentim BERNI, Antonio Clareti Pereira, Flavia Dutra Mendes
  • Publication number: 20120269713
    Abstract: Aspects of the present invention refers to a process for production of nickel carbonate including preparing a magnesium salt solution, contacting the solution with a stream of gaseous CO2, keeping pH between 4 and 10 and temperature between 0 and 100° C., during up to 5 hours to produce a first mixture, contacting the first mixture with a nickel sulphate solution to produce a second mixture, performing a separation of liquid and solid portions of the second mixture, and feeding the magnesium salt solution with the liquid portion. This process recycles the reagent used for producing nickel carbonate and yields a final product that is easy to handle and transport.
    Type: Application
    Filed: March 26, 2012
    Publication date: October 25, 2012
    Applicant: Vale S/A
    Inventors: Tiago Valentim BERNI, Antonio Clareti Pereira, Felipe Hilário Guimarães
  • Publication number: 20120213681
    Abstract: The present invention refers to a direct purification process of a nickel laterite leaching effluent including adjusting a pH of a leaching solution, employing an ion exchange resin to adsorb nickel and copper selectively over ferric or ferrous iron, and recovering nickel.
    Type: Application
    Filed: February 1, 2012
    Publication date: August 23, 2012
    Applicant: VALE S.A.
    Inventors: Tiago Valentim Berni, Antonio Clareti Pereira
  • Patent number: 8173086
    Abstract: A method for recovering base metal values from oxide ore is provided, where the ore includes a first group metal selected from iron, magnesium and aluminum and a second group metal selected from nickel, cobalt and copper. The method includes reducing ore particle size to suit the latter unit operations, favoring contact of the metal elements, contacting the ore with ferric or ferrous chloride, hydrated or anhydrous, to produce a mix of ore and iron(II or III) chloride, subjecting the mixture of the ore and ferric or ferrous chloride to enough energy to decompose the chlorides into hydrochloric acid and a iron oxide, contacting the readily-formed hydrochloric acid with the base metal oxides from the second group, forming their respective chlorides, selectively dissolve the produced base metal chlorides, leaving the metals as oxides and in the solid state, and recovering the dissolved base metal values from aqueous solution.
    Type: Grant
    Filed: July 13, 2010
    Date of Patent: May 8, 2012
    Assignee: Vale S.A.
    Inventors: Antonio Clareti Pereira, Tiago Valentim Berni
  • Publication number: 20110142736
    Abstract: A method for recovering base metal values from oxide ore is provided, where the ore includes a first group metal selected from iron, magnesium and aluminum and a second group metal selected from nickel, cobalt and copper. The method includes reducing ore particle size to suit the latter unit operations, favoring contact of the metal elements, contacting the ore with ferric or ferrous chloride, hydrated or anhydrous, to produce a mix of ore and iron(II or III) chloride, subjecting the mixture of the ore and ferric or ferrous chloride to enough energy to decompose the chlorides into hydrochloric acid and a iron oxide, contacting the readily-formed hydrochloric acid with the base metal oxides from the second group, forming their respective chlorides, selectively dissolve the produced base metal chlorides, leaving the metals as oxides and in the solid state, and recovering the dissolved base metal values from aqueous solution.
    Type: Application
    Filed: July 13, 2010
    Publication date: June 16, 2011
    Applicant: VALE S.A.
    Inventors: Antonio Clareti Pereira, Tiago Valentim Berni
  • Publication number: 20110110832
    Abstract: The present invention resides in a process of recovering nickel and cobalt, regenerating the main raw materials, said process including the steps of: granulometric separation; leaching; neutralization; MHP production in only one stage and the pressure crystallization of magnesium sulphite. The process proposes a way to recovery nickel and cobalt from laterite ores through the atmospheric and heap leaching with staged addition of ore—by size separation—and H2SO4, decreasing the nickel losses and simplifying the neutralization circuit and producing a more purified MHP. The present process route is employed for nickel extraction, including the one from high magnesium containing lateritic ores.
    Type: Application
    Filed: June 1, 2009
    Publication date: May 12, 2011
    Applicant: VALE S.A.
    Inventors: Antonio Clareti Pereira, Felipe Hilario Guimaraes, Joao Alberto de Lessa Tude, Lino Rodrigues de Freitas, Tiago Valentim Berni
  • Publication number: 20090241731
    Abstract: A method for recovering base metal values from oxide ore is provided by the present disclosure. The ore includes a first metal selected from the group consisting at least one of iron and aluminum and a second metal selected from the group consisting of at least one of nickel, cobalt and copper. The method includes the steps of: contacting the oxide ore with hydrogen chloride gas to obtain chlorides of the first and second metals and subjecting at least the first and second metals to pyrohydrolysis at a predetermined temperature to decompose the chlorides of the first metal into oxides. The method also includes the step of mixing the oxides of the first metal and the chlorides of the second metal in an aqueous solution to dissolve the chlorides of the second metal and recovering the dissolved ions of the second metal from the aqueous solution.
    Type: Application
    Filed: August 26, 2008
    Publication date: October 1, 2009
    Applicant: VALE INCO LIMITED
    Inventors: Antonio Clareti Pereira, Flavia Dutra Mendes, Tiago Valentim Berni, Ahmed Vahed