Abstract: A method of treating the surface of a metal casing used in a wellbore by conditioning the metal casing in a conditioning fluid to form a conditioned metal casing, contacting the conditioned metal casing with a treatment fluid to form a treated metal casing, and drying the treated metal casing. A method of increasing the bond strength between cement and a metal casing surface treated with a reactive organic compound by curing the treated metal casing with a cement slurry.

Abstract: A lost circulation material is placed in a cavity. The cavity is defined by an inner bore of a cylindrical wall, intermediate of a piston and a screen. A distance between the piston and the screen is defined as the height of the cavity, which is adjustable. The piston is slid longitudinally, such that the piston comes in contact with the lost circulation material. The lost circulation material is heated to a specified test temperature mimicking a downhole temperature. A compression test is performed on the lost circulation material. The compression test includes flowing a test fluid into the cavity and applying force on the piston to pressurize the test fluid to a specified test pressure mimicking a downhole pressure. The force on the piston is released. The pressure of the test fluid and the height of the cavity are measured throughout the compression test.

Abstract: This disclosure relates to methods of treating the surface of a metal casing, such as a casing used in a wellbore. The disclosure also relates to methods of increasing the bond strength between cement and a metal casing surface treated with a reactive organic compound.

Abstract: A lost circulation material is placed in a cavity. The cavity is defined by an inner bore of a cylindrical wall, intermediate of a piston and a screen. A distance between the piston and the screen is defined as the height of the cavity, which is adjustable. The piston is slid longitudinally, such that the piston comes in contact with the lost circulation material. The lost circulation material is heated to a specified test temperature mimicking a downhole temperature. A compression test is performed on the lost circulation material. The compression test includes flowing a test fluid into the cavity and applying force on the piston to pressurize the test fluid to a specified test pressure mimicking a downhole pressure. The force on the piston is released. The pressure of the test fluid and the height of the cavity are measured throughout the compression test.

Abstract: A method of analyzing a composite plug includes creating a composite plug, where the composite plug includes a formation layer, a cement layer, and an interface region between them, and the cement extends into the formation sample in the interface region. The method further includes imaging the composite plug to gather a series of discrete images, where each discrete image in the series depicts a cross section of the composite plug and the discrete images are taken at set increments throughout a depth of the composite plug. The method further includes analyzing each discrete image in the series of discrete images to determine a porosity measurement of each discrete image, determine a first and second boundary of the interface region from the porosity measurement of each discrete image, and determine a depth of the interface region by a number of discrete images between the first boundary and the second boundary.

Abstract: Systems and methods for testing shear bond strength of cement with a composite sample under downhole conditions form a bonding surface of the sample oriented at an angle between 50 and 70 degrees from a plane perpendicular to a longitudinal axis of the sample. The composite sample is formed by bonding the cement to the sample with the cement in contact with the bonding surface of the sample.

Abstract: A method of analyzing a composite plug includes creating a composite plug, where the composite plug includes a formation layer, a cement layer, and an interface region between them, and the cement extends into the formation sample in the interface region. The method further includes imaging the composite plug to gather a series of discrete images, where each discrete image in the series depicts a cross section of the composite plug and the discrete images are taken at set increments throughout a depth of the composite plug. The method further includes analyzing each discrete image in the series of discrete images to determine a porosity measurement of each discrete image, determine a first and second boundary of the interface region from the porosity measurement of each discrete image, and determine a depth of the interface region by a number of discrete images between the first boundary and the second boundary.

Abstract: Systems and methods for testing shear bond strength of cement with a composite sample under downhole conditions form a bonding surface of the sample oriented at an angle between 50 and 70 degrees from a plane perpendicular to a longitudinal axis of the sample. The composite sample is formed by bonding the cement to the sample with the cement in contact with the bonding surface of the sample.