Patents by Inventor Arthur G. Mack

Arthur G. Mack has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11827599
    Abstract: A method of preparing MEP including the steps of: (a) adding N-methylpyrrolidine to an excess amount of ethyl bromide located in a reactor, wherein the N-methylpyrrolidine will react with the ethyl bromide forming MEP, wherein the reaction will have a reaction temperature that can varies over time; (b) stopping addition of N-methylpyrrolidine when the excess of ethyl bromide to the N-methylpyrrolidine falls within a range of 3:1 to 1.5:1; (c) adding water to the reactor creating a two phase system to develop which includes: (i) a top layer containing aqueous MEP and (ii) a bottom layer containing ethyl bromide; (d) separating the top layer from the bottom layer yielding a first aqueous solution of MEP and a second solution of ethyl bromide; and (e) removing N-methylpyrrolidine and ethyl bromide from the first aqueous solution of MEP.
    Type: Grant
    Filed: November 9, 2022
    Date of Patent: November 28, 2023
    Assignee: TETRA Technologies, Inc.
    Inventor: Arthur G. Mack
  • Patent number: 11613687
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated divalent brine, and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor of at least 0.1, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the divalent brine; wherein the suppression factor fluid is in the absence of zinc; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Grant
    Filed: November 17, 2021
    Date of Patent: March 28, 2023
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventor: Arthur G. Mack
  • Patent number: 11453817
    Abstract: A composition for use in a wellbore activity, the composition comprising an iodide brine, the iodide brine operable to be used in the wellbore activity, the iodide brine comprising an iodide salt, an aqueous fluid, and an iodide protectant, the iodide protectant operable to prevent the presence of free iodine in the iodide brine, where the iodide protectant is present in the range between 0.001 v/v % and 5 v/v % of the iodide brine.
    Type: Grant
    Filed: October 24, 2017
    Date of Patent: September 27, 2022
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventors: Arthur G. Mack, Drew A. Fowler, Phillip A. Vincent
  • Patent number: 11292956
    Abstract: A composition for use in a wellbore activity, the composition comprising a stabilized divalent iodide brine, the stabilized divalent iodide brine comprises a divalent salt system, where the divalent salt system comprises a divalent iodide, an primary iodide stabilizer, the primary iodide stabilizer operable to remove free iodine, prevent the formation of free iodine, and suppress TCT, and an aqueous fluid, where the stabilized divalent iodide brine has a density greater than 11 lb/gal, where the stabilized divalent iodide brines has a TCT of less than or equal to 70 deg F.
    Type: Grant
    Filed: April 21, 2021
    Date of Patent: April 5, 2022
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventors: Arthur G. Mack, Drew A. Fowler
  • Publication number: 20220073806
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated divalent brine, and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor of at least 0.1, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the divalent brine; wherein the suppression factor fluid is in the absence of zinc; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Application
    Filed: November 17, 2021
    Publication date: March 10, 2022
    Applicant: TETRA TECHNOLOGIES, INC.
    Inventor: Arthur G. Mack
  • Patent number: 11261362
    Abstract: A composition for use in a wellbore activity, the composition comprising a stabilized monovalent iodide brine, the stabilized monovalent iodide brine comprises a monovalent salt system, the monovalent salt system comprises a monovalent iodide; a primary iodide stabilizer, the primary iodide stabilizer operable to remove free iodine, prevent the formation of free iodine, and suppress TCT; and an aqueous fluid, where the stabilized monovalent iodide brine has a density greater than 10 lb/gal, where the stabilized monovalent iodide brine has a TCT of less than or equal to 70 deg F.
    Type: Grant
    Filed: October 29, 2020
    Date of Patent: March 1, 2022
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventors: Arthur G. Mack, Drew A. Fowler
  • Patent number: 11208586
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated monovalent brine; and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the monovalent brine; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Grant
    Filed: April 24, 2020
    Date of Patent: December 28, 2021
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventor: Arthur G. Mack
  • Patent number: 11208585
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated divalent brine, and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor of at least 0.1, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the divalent brine; wherein the suppression factor fluid is in the absence of zinc; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Grant
    Filed: March 24, 2017
    Date of Patent: December 28, 2021
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventor: Arthur G. Mack
  • Patent number: 11208587
    Abstract: A stabilized composition for use as a well fluid is provided. The stabilized composition includes a brine, a polyol, the polyol in an amount operable to inhibit solid formation, the polyol further operable to dissolve within the brine; and a stabilization compound, the stabilization compound operable to stabilize the polyol, such that the polyol does not degrade at a bottom hole temperature.
    Type: Grant
    Filed: December 30, 2020
    Date of Patent: December 28, 2021
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventors: Arthur G. Mack, Stanley Gunawan, Katrina Schultz
  • Patent number: 11136486
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated monovalent brine; and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the monovalent brine; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Grant
    Filed: March 24, 2017
    Date of Patent: October 5, 2021
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventor: Arthur G. Mack
  • Patent number: 11104836
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated monovalent brine; and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the monovalent brine; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Grant
    Filed: December 30, 2019
    Date of Patent: August 31, 2021
    Assignee: TETRA TECHNOLOGIES, INC.
    Inventor: Arthur G. Mack
  • Publication number: 20210238468
    Abstract: A composition for use in a wellbore activity, the composition comprising a stabilized divalent iodide brine, the stabilized divalent iodide brine comprises a divalent salt system, where the divalent salt system comprises a divalent iodide, an primary iodide stabilizer, the primary iodide stabilizer operable to remove free iodine, prevent the formation of free iodine, and suppress TCT, and an aqueous fluid, where the stabilized divalent iodide brine has a density greater than 11 lb/gal, where the stabilized divalent iodide brines has a TCT of less than or equal to 70 deg F.
    Type: Application
    Filed: April 21, 2021
    Publication date: August 5, 2021
    Applicant: TETRA Technologies, Inc.
    Inventors: Arthur G. Mack, Drew A. Fowler
  • Patent number: 11021645
    Abstract: A composition for use in a wellbore activity, the composition comprising a stabilized divalent iodide brine, the stabilized divalent iodide brine comprises a divalent salt system, where the divalent salt system comprises a divalent iodide, an primary iodide stabilizer, the primary iodide stabilizer operable to remove free iodine, prevent the formation of free iodine, and suppress TCT, and an aqueous fluid, where the stabilized divalent iodide brine has a density greater than 11 lb/gal, where the stabilized divalent iodide brines has a TCT of less than or equal to 70 deg F.
    Type: Grant
    Filed: October 24, 2017
    Date of Patent: June 1, 2021
    Inventors: Arthur G. Mack, Drew A. Fowler
  • Publication number: 20210115316
    Abstract: A stabilized composition for use as a well fluid is provided. The stabilized composition includes a brine, a polyol, the polyol in an amount operable to inhibit solid formation, the polyol further operable to dissolve within the brine; and a stabilization compound, the stabilization compound operable to stabilize the polyol, such that the polyol does not degrade at a bottom hole temperature.
    Type: Application
    Filed: December 30, 2020
    Publication date: April 22, 2021
    Applicant: Tetra Technologies, Inc.
    Inventors: Arthur G. Mack, Stanley Gunawan, Katrina Schultz
  • Publication number: 20210040372
    Abstract: A composition for use in a wellbore activity, the composition comprising a stabilized monovalent iodide brine, the stabilized monovalent iodide brine comprises a monovalent salt system, the monovalent salt system comprises a monovalent iodide; a primary iodide stabilizer, the primary iodide stabilizer operable to remove free iodine, prevent the formation of free iodine, and suppress TCT; and an aqueous fluid, where the stabilized monovalent iodide brine has a density greater than 10 lb/gal, where the stabilized monovalent iodide brine has a TCT of less than or equal to 70 deg F.
    Type: Application
    Filed: October 29, 2020
    Publication date: February 11, 2021
    Applicant: Tetra Technologies, Inc.
    Inventors: Arthur G. Mack, Drew A. Fowler
  • Patent number: 10913884
    Abstract: A stabilized composition for use as a well fluid is provided. The stabilized composition includes a brine, a polyol, the polyol in an amount operable to inhibit solid formation, the polyol further operable to dissolve within the brine; and a stabilization compound, the stabilization compound operable to stabilize the polyol, such that the polyol does not degrade at a bottom hole temperature.
    Type: Grant
    Filed: March 24, 2017
    Date of Patent: February 9, 2021
    Inventors: Arthur G. Mack, Stanley Gunawan, Katrina Schultz
  • Patent number: 10851278
    Abstract: A composition for use in a wellbore activity, the composition comprising a stabilized monovalent iodide brine, the stabilized monovalent iodide brine comprises a monovalent salt system, the monovalent salt system comprises a monovalent iodide; a primary iodide stabilizer, the primary iodide stabilizer operable to remove free iodine, prevent the formation of free iodine, and suppress TCT; and an aqueous fluid, where the stabilized monovalent iodide brine has a density greater than 10 lb/gal, where the stabilized monovalent iodide brine has a TCT of less than or equal to 70 deg F.
    Type: Grant
    Filed: October 24, 2017
    Date of Patent: December 1, 2020
    Assignee: Tetra Technologies, Inc.
    Inventors: Arthur G. Mack, Drew A. Fowler
  • Publication number: 20200255715
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated monovalent brine; and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the monovalent brine; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Application
    Filed: April 24, 2020
    Publication date: August 13, 2020
    Inventor: Arthur G. Mack
  • Publication number: 20200131422
    Abstract: A method of using a suppression factor fluid during a well activity is provided. The method comprising the steps of introducing a suppression factor fluid into a wellbore, the suppression factor fluid comprising an untreated monovalent brine; and a suppression sugar alcohol, the suppression sugar alcohol in an amount operable to achieve a suppression factor, wherein a density upper limitation of the suppression factor fluid is greater than the density upper limitation of the monovalent brine; and completing the well activity in the wellbore, such that the suppression sugar alcohol inhibits crystallization during the well activity.
    Type: Application
    Filed: December 30, 2019
    Publication date: April 30, 2020
    Inventor: Arthur G. Mack
  • Publication number: 20190119557
    Abstract: A composition for use in a wellbore activity, the composition comprising an iodide brine, the iodide brine operable to be used in the wellbore activity, the iodide brine comprising an iodide salt, an aqueous fluid, and an iodide protectant, the iodide protectant operable to prevent the presence of free iodine in the iodide brine, where the iodide protectant is present in the range between 0.001 v/v % and 5 v/v % of the iodide brine.
    Type: Application
    Filed: October 24, 2017
    Publication date: April 25, 2019
    Applicant: TETRA Technologies, Inc.
    Inventors: Arthur G. MACK, Drew A. FOWLER, Phillip A. VINCENT