Abstract: An adsorption-desorption process for separation of a component from a feed mixture of components wherein at least two components of the feed mixture are adsorbed by an adsorbent material during the adsorption step of the adsorption-desorption process and the adsorbent material has a greater affinity for a first one of said adsorbed components than for a second one of the adsorbed components, the process comprising charging the feed mixture to an inlet end of a bed of the adsorbent material, passing the feed mixture through the bed under such conditions that the adsorbent material adsorbs said first and second components of the feed mixture, withdrawing an effluent from an outlet end of the bed, the effluent consisting essentially of feed mixture decreased in content of the materials adsorbed by the bed, after the adsorbent material is substantially saturated, desorbing the first and second components from the adsorbent material in at least two steps at substantially the same pressure but at different temperat