Abstract: A method for securing qualitative and quantitative information of a high molecular weight additive in a polymer resin sample is disclosed herein. In some embodiments, the method includes separating a fraction of a polymer resin sample using size exclusion chromatography (SEC), wherein the fraction corresponding to a high molecular weight additive, pyrolyzing the fraction in a pyrolysis-gas chromatography/mass spectrometer (Py-GC/MS) to obtain a mass spectrum of the pyrolyzed fraction; identifying a structure of the high molecular weight additive by comparing m/z values for fragment peaks in the mass spectrum to m/z values for fragment peaks in a mass spectrum of a standard, and determining the amount of the high molecular weight additive in the polymer resin sample, relative to the total weight of the polymer resin sample by comparing a sum of areas of the fragment peaks to a calibration line of the standard.

Abstract: The present disclosure provides a method for analyzing an additive in a water-based polymer sample, comprising the steps of: (S1) putting the water-based polymer sample containing a polymer, the additive, and water as a solvent into a vial; (S2) putting a porous pouch containing a superabsorbent polymer (SAP) into the vial to absorb the water into the superabsorbent polymer; (S3) removing the porous pouch from the vial and collecting the concentrated polymer sample remaining in the vial; and (S4) performing a pyrolysis gas chromatography (Py-GC)/mass spectrometer (MS) analysis by introducing the concentrated polymer sample to the Py-GC/MS.

Abstract: The present invention relates to a method for analyzing the molecular weight of each polymer comprised in a polymer compound, and an analysis system used therefor. More specifically, the present invention relates to an analysis method of components of polymer compounds and molecular weight by component using a system in which size-exclusion chromatography (SEC)-pyrolysis gas chromatography (Py-GC)-mass spectrometry (MS) are connected in series and to an analysis system used in the method.

Abstract: The present disclosure relates to an apparatus and a method for analysis of a multi-layer adhesive film and provides the apparatus comprising a specimen tray unit; a blade unit; a liquid nitrogen supply unit; and a driving unit, and the method comprising a specimen fixing step; a specimen cooling step; a specimen pre-collection step; a specimen collection step; and a blade separation step.

Abstract: A method for analyzing an antioxidant content contained in a semiconductive material for a cable, which includes an amine-based antioxidant. The method can provide an accurate quantitative analysis value obtained by a comparison with the actual amount used, through gas chromatography (GC)/a flame ionization detector (FID).

Abstract: The present invention relates to a dianhydride analysis method. The method can stably analyze a dianhydride which has high reactivity and low solubility. Furthermore, the method can minimize the problem that a reaction product disturbs an analysis result, thereby improving accuracy of the analysis result.

Abstract: A pretreatment method for analyzing dioxin compounds and an analytical method using the same, in which a column packed with polymer beads that are capable of selectively adsorbing dioxin compounds is used in a purification step during pretreatment, thereby remarkably reducing a time required for pretreatment and improving a recovery rate of an internal standard for purification, are provided.

Abstract: A method for extracting electrolyte solution in lithium secondary battery includes (S1) freezing a secondary battery by impregnating in liquid nitrogen and then cutting it without disassembling; (S2) immersing the frozen cut secondary battery in an extraction solvent to extract an electrolyte solution contained in the battery; and (S3) calculating the total amount of the electrolyte solution with respect to the total size of the battery from the content of the extracted electrolyte solution, and then determining a ratio of total amount of the electrolyte solution to the content of the electrolyte solution used in manufacturing the secondary battery to obtain extraction efficiency. A system for extracting an electrolyte solution in a secondary battery is also provided.

Abstract: A method for simulataneously separating and detecting aldehydes or ketones from a plurality of samples containing the samein a simple and rapid manner by using a rotary microdevice capable of integrating derivatization and TLC separation of aldehydes and ketones, and the method providing reliable TLC separation, control of moving speed of an eluent on a TLC plate, and improved TLC resolution.

Abstract: A rotary analysis system comprising: a rotary unit including a rotary platform, and having a TLC plate on which movement of a fluid sample and an eluent is controlled by rotational motion of the rotary platform, and aldehydes or ketones in the sample are separated and deployed with the eluent; a shooting unit for capturing an image of components of the sample separated by the rotary unit; a control unit for controlling the rotation conditions of the rotary unit and the capturing conditions of the shooting unit; and an analysis unit for analyzing the image captured by the shooting unit, and the rotary analysis system capable of economically and simply separating and detecting aldehydes or ketones.

Abstract: A microdevice for detecting aldehydes or ketones by utilizing a rotary platform, the microdevice comprising a disc-shaped rotary platform and a microfluidic structure disposed on the rotary platform, and the microfluidic structure comprising a sample storage part, an eluent storage part, a separation part, a first microfluid flow channel, a second microfluid flow channel, and an absorption pad.

Abstract: The present invention relates to a micro device for solid phase extraction and more particularly provides a micro device which is configured to perform solid phase extraction by injecting a filler and a solvent and producing a uniform flow of the solvent.

Abstract: The present invention relates to a method for analyzing the molecular weight of each polymer comprised in a polymer compound, and an analysis system used therefor. More specifically, the present invention relates to an analysis method of components of polymer compounds and molecular weight by component using a system in which size-exclusion chromatography (SEC)-pyrolysis gas chromatography (Py-GC)-mass spectrometry (MS) are connected in series and to an analysis system used in the method.

Abstract: A qualitative and quantitative heavy metal analysis device and, more particularly, a qualitative and quantitative heavy metal analysis device implemented by a rotary platform are provided. The rotary platform device includes a main injection part which is positioned near a rotating shaft of a rotary platform, wherein the main injection part is configured to receive a fluid sample containing heavy metals, a pH adjusting part configured to adjust pH of the fluid sample, a detecting part coated with a chelating agent configured to initiate a color reaction with heavy metals in the fluid sample by spreading the pH-adjusted fluid sample into the detecting part, and a ruler for measuring a spreading distance of the color reaction, wherein the fluid sample moves from the main injection part through the pH adjusting part to the detecting part by a rotation of the rotary platform device.

Abstract: The present disclosure provides a method for analyzing an additive in a water-based polymer sample, comprising the steps of: (S1) putting the water-based polymer sample containing a polymer, the additive, and water as a solvent into a vial; (S2) putting a porous pouch containing a superabsorbent polymer (SAP) into the vial to absorb the water into the superabsorbent polymer; (S3) removing the porous pouch from the vial and collecting the concentrated polymer sample remaining in the vial; and (S4) performing a pyrolysis gas chromatography (Py-GC)/mass spectrometer (MS) analysis by introducing the concentrated polymer sample to the Py-GC/MS.

Abstract: The present disclosure relates to an apparatus and a method for analysis of a multi-layer adhesive film and provides the apparatus comprising a specimen tray unit; a blade unit; a liquid nitrogen supply unit; and a driving unit, and the method comprising a specimen fixing step; a specimen cooling step; a specimen pre-collection step; a specimen collection step; and a blade separation step.

Abstract: A method for securing qualitative and quantitative information of a high molecular weight additive in a polymer resin sample is disclosed herein. In some embodiments, the method includes separating a fraction of a polymer resin sample using size exclusion chromatography (SEC), wherein the fraction corresponding to a high molecular weight additive, pyrolyzing the fraction in a pyrolysis-gas chromatography/mass spectrometer (Py-GC/MS) to obtain a mass spectrum of the pyrolyzed fraction; identifying a structure of the high molecular weight additive by comparing m/z values for fragment peaks in the mass spectrum to m/z values for fragment peaks in a mass spectrum of a standard, and determining the amount of the high molecular weight additive in the polymer resin sample, relative to the total weight of the polymer resin sample by comparing a sum of areas of the fragment peaks to a calibration line of the standard.

Abstract: The present invention relates to a dianhydride analysis method. The method can stably analyze a dianhydride which has high reactivity and low solubility. Furthermore, the method can minimize the problem that a reaction product disturbs an analysis result, thereby improving accuracy of the analysis result.

Abstract: The present invention relates to a dianhydride analysis method, which can reliably analyze a dianhydride having high reactivity and low solubility. In addition, the present invention can analyze the structure of impurities by separating the impurities on the basis of having a similar retention time in HPLC analysis, and can analyze the purity of the dianhydride with or without chromophores.

Abstract: The present invention relates to an apparatus for measuring moisture of a solid sample, a method for measuring a moisture content of the solid sample, and a method for analyzing an imidization rate, and more particularly, to an apparatus for measuring moisture of a solid sample, a method for measuring a moisture content of the solid sample, and a method for analyzing an imidization rate, which detect the moisture content of the solid sample at a specific temperature by using a Karl-Fischer device capable of selectively detecting only the moisture content of the solid sample in the method for analyzing an imidization rate of the solid sample and calculate the imidization rate of the solid sample by using the detected moisture content.