Abstract: This invention provides a pressurizable zero-headspace extractor vessel useful in preparing mixtures of solid- and liquid-phase material for constituent analysis, for example for preparing environmental samples for analysis of toxic contaminants. The inventive extractor vessel has a sample chamber pressurizable either by gas or mechanical means. The sample chamber is constructed with a removable liner of polytetrafluorethylene to be resistant to both organic an metallic contaminants and has a more robust pressure-resistant support housing, in which the liner is a snug fit, formed of a structural material such as high-density polyethylene. The invention also provides a rotary agitation apparatus for rotating such extractors or bottles end-over-end, in which apparatus the bottles are mounted in a manner which automatically centers them on the axis of rotation.

Abstract: This invention provides a pressurizable zero-headspace extractor vessel useful in preparing mixtures of solid- and liquid-phase material for constituent analysis, for example for preparing environmental samples for analysis of toxic contaminants. The inventive extractor vessel has a sample chamber pressurizable either by gas or mechanically. The sample chamber is constructed with a removable liner of polytetrafluorethylene to be resistant to both organic an metallic contaminants and has a more robust pressure-resistant support housing, in which the liner is a snug fit, formed of a structural material such as high-density polyethylene. The invention also provides a rotary agitation apparatus for rotating such extractors or bottles end-over-end, in which apparatus the bottles are mounted in a manner which automatically centers them on the axis of rotation.