Abstract: The present disclosure belongs to the technical field of separation and purification of glycolic acid, and in particular, to a method and device for separation and purification of glycolic acid by a rectification-crystallization coupling process and use. Bio-based platform compound molecules are used as raw materials to synthesize the glycolic acid, and the obtained crude glycolic acid is separated and purified using the rectification-crystallization coupling process to obtain high-purity glycolic acid. The method initiates system separation and purification under a new glycolic acid synthesis route, which has the difficulty that the glycolic acid is easy to polymerize during concentration, so there are technical barriers to equipment design of vacuum rectification and adjustment of process parameters. In addition, during crystallization, there are technical barriers to equipment design of a crystallization kettle and adjustment of process parameters.

Abstract: A method for producing chemicals from crude oil by double-tube parallel multi-zone catalytic conversion is provided. The method may include the following steps: feeding the crude oil directly or separating the crude oil into light and heavy components by flash evaporation or distillation after desalination and dehydration; strengthening the contact and reaction between oil gas and catalyst by using two parallel reaction tubes with novel structure, controlling the reaction by zones, carrying out optimal combination on feeding modes according to different properties of reaction materials, controlling suitable reaction conditions for different materials, and increasing the production of light olefins and aromatics.

Abstract: A method for preparing titanium-containing molecular sieves include the following steps: irradiating a mixed solution containing a silicon source, a template and a titanium source by a light source containing ultraviolet light before crystallization, and then subjecting the mixed solution to crystallization and post-treatment to obtain the titanium-containing molecular sieve. In the method for preparing titanium-containing molecular sieve of the present invention, the mixed solution containing the silicon source, the template and the titanium source is treated with the ultraviolet light, and free radicals generated by the ultraviolet light can effectively dissociate titanium oligomers and accelerate the hydrolysis of the silicon source, and thus match the hydrolysis rate of a silicon-titanium precursor, thereby preventing a titanium monomer from self-polymerization to form non-framework titanium.

Abstract: A method for homogenizing the compositions and mechanical performances of nickel-based material brazed joints, includes three homogenized manufacturing steps: Step I, assembling the welding sample, placing it into the vacuum furnace, and then heating up to 830˜860° C. and holding the temperature; then heating up again to 1050˜1100° C. and holding the temperature; allowing for slow self-cooling in vacuum till it reaches 620˜640° C.; then filling the furnace with nitrogen and starting the vacuum furnace fan at the same time, so that the sample is cooled down to 40˜60° C.; Step II, raising the temperature up to 1140˜1160° C. and holding, then cooling it down to the room temperature through water-quenching; Step III, raising the temperature of the welding sample up to 680˜750° C. again, and cooling it down to the room temperature through air cooling.

Abstract: A method for preparing titanium-containing molecular sieves include the following steps: irradiating a mixed solution containing a silicon source, a template and a titanium source by a light source containing ultraviolet light before crystallization, and then subjecting the mixed solution to crystallization and post-treatment to obtain the titanium-containing molecular sieve. In the method for preparing titanium-containing molecular sieve of the present invention, the mixed solution containing the silicon source, the template and the titanium source is treated with the ultraviolet light, and free radicals generated by the ultraviolet light can effectively dissociate titanium oligomers and accelerate the hydrolysis of the silicon source, and thus match the hydrolysis rate of a silicon-titanium precursor, thereby preventing a titanium monomer from self-polymerization to form non-framework titanium.

Abstract: A method for homogenizing the compositions and mechanical performances of nickel-based material brazed joints, includes three homogenized manufacturing steps: Step I, assembling the welding sample, placing it into the vacuum furnace, and then heating up to 830˜860° C. and holding the temperature; then heating up again to 1050˜1100° C. and holding the temperature; allowing for slow self-cooling in vacuum till it reaches 620˜640° C.; then filling the furnace with nitrogen and starting the vacuum furnace fan at the same time, so that the sample is cooled down to 40˜60° C.; Step II, raising the temperature up to 1140˜1160° C. and holding, then cooling it down to the room temperature through water-quenching; Step III, raising the temperature of the welding sample up to 680˜750° C. again, and cooling it down to the room temperature through air cooling.

Abstract: A process for the fluid catalytic cracking of oxygenated hydrocarbon compounds from biological origin. The process comprises contacting a feed comprising the oxygenated hydrocarbon compounds from biological origin and an amount of sulphur with a fluid cracking catalyst at a temperature of equal to or more than 400° C. to produce a products stream. The process further comprises separating fluid cracking catalyst from the products stream and separating a light fraction from the products stream; and removing hydrogen sulphide from the light fraction by means of an amine treating process. Activated carbon is used to treat at least part of an amine solution used in the amine treating process or to treat at least part of the feed to the amine treating process.

Abstract: A process for the fluid catalytic cracking of oxygenated hydrocarbon compounds from biological origin. The process comprises (a) contacting a feed comprising the oxygenated hydrocarbon compounds with a fluid catalytic cracking catalyst at elevated temperature to produce a cracked products stream, the feed comprising an amount of sulphur; (b) separating catalyst from the cracked products stream; (c) separating a light fraction from the cracked products stream; and (d) removing hydrogen sulphide from the light fraction by means of an amine treating process. The fluid catalytic cracking process involves the presence or use of water and/or steam and comprises a working-up process of the cracked products stream. In the working-up process, one or more chemical additives for reducing or hindering the formation of foam in amine liquids selected from defoamers and demulsifiers are added to the amine solvent in one or more amine treaters.

Abstract: A process for the fluid catalytic cracking of oxygenated hydrocarbon compounds from biological origin. The process comprises (a) contacting a feed comprising the oxygenated hydrocarbon compounds from biological origin with a fluid cracking catalyst at a temperature of equal to or more than 400° C. to produce a products stream; (b) separating fluid cracking catalyst from the products stream and separating a fraction comprising one or more C1-C4 hydrocarbon compounds from the products stream; and (c) processing the fraction comprising one or more C1-C4 hydrocarbon compounds in a work-up process, which comprises one or more oil/water separation steps. One or more de-emulsifiers are added to one or more oil/water separation steps.

Abstract: A riser reactor for propylene production, comprises pipelines with an upper part and a lower part, the upper part is a straight pipeline, and the lower part is a expanding-diameter pipeline, and the expanding-diameter pipeline is a circular truncated cone-shaped pipeline with an angle of 1˜60 o between generatrix and axes, wherein, the diameter of upper surface of the circular truncated cone-shaped pipeline is larger than or equal to the diameter of the straight pipeline. Employed the riser reactor, propylene is produced by the method of catalytic cracking with stratified injections of heavy oil and light olefins. Average gas linear velocity in axial direction of the straight pipeline of riser reactor is 3˜25 m/s, and that in the expanding-diameter pipeline is 0.1 to 5 m/s. The outlet temperature of the riser reactor is 460 to 600° C., and the light olefins are no more than 50% of the total feedstock by weight.

Abstract: The present invention relates to a catalytic cracking process and a device used in the process in particular, the present invention provides a catalytic cracking process, which comprises which comprises: 1) catalytic cracking a feedstock in the first riser for less than about 1.5 second and sending the resultant stream into the first separating device,; 2) catalytic cracking the recycle oil obtained from the first separating device in the second riser for less than about 1.

Abstract: The present invention relates to a catalytic cracking process and a device used in the process in particular, the present invention provides a catalytic cracking process, which comprises which comprises:

Abstract: This invention relates to a new two-stage riser catalytic cracking process, particularly to an improvement of the conventional riser reactor and reaction-regeneration system by application of a two-stage riser reactor to fulfill the aims of the concatenation of oil-vapor, catalyst in relays as result in shortening reaction time and increasing average performance of the catalyst.