Patent number: 9085506
Abstract: The invention relates to an improved process for preparing 3-aminomethyl-3,5,5-trimethylcyclohexylamine, referred to hereinafter as isophoronediamine or, in abbreviated form, IPDA, by: I. preparation of isophorone by catalyzed aldol condensations with acetone as reactant; II. reaction of isophorone with HCN to form isophoronenitrile (IPN, 3-cyano-3,5,5-trimethylcyclohexanone); III. catalytic hydrogenation and/or catalytic reductive amination (also referred to as aminative hydrogenation) of 3-cyano-3,5,5-trimethylcyclohexanone, hereinafter called isophoronenitrile or, in abbreviated form, IPN, to give the isophoronediamine.
Type:
Grant
Filed:
November 18, 2011
Date of Patent:
July 21, 2015
Assignee:
Evonik Degussa GmbH
Inventors:
Markus Galle, Gerda Grund, Axel Hengstermann, Michael D Hinton, Rolf Hirsch, Robert Jansen, Cord Knoop, Christian Lettmann, Juergen Lippe, Martin Maier, Joerg-Joachim Nitz, Matthias Orschel, Martina Ortelt, Norbert Richter, Armin Rix, Markus Schwarz, Guido Streukens
Publication number: 20130253226
Abstract: The invention relates to an improved process for preparing 3-aminomethyl-3,5,5-trimethylcyclohexylamine, referred to hereinafter as isophoronediamine or, in abbreviated form, IPDA, by: I. preparation of isophorone by catalyzed aldol condensations with acetone as reactant; II. reaction of isophorone with HCN to form isophoronenitrile (IPN, 3-cyano-3,5,5-trimethylcyclohexanone); III. catalytic hydrogenation and/or catalytic reductive amination (also referred to as aminative hydrogenation) of 3-cyano-3,5,5-trimethylcyclohexanone, hereinafter called isophoronenitrile or, in abbreviated form, IPN, to give the isophoronediamine.
Type:
Application
Filed:
November 18, 2011
Publication date:
September 26, 2013
Applicant:
Evonik Degussa GmbH
Inventors:
Markus Galle, Gerda Grund, Axel Hengstermann, Michael D. Hinton, Rolf Hirsch, Robert Jansen, Cord Knoop, Christian Lettmann, Juergen Lippe, Martin Maier, Joerg-Joachim Nitz, Matthias Orschel, Martina Ortelt, Norbert Richter, Armin Rix, Markus Schwarz, Guido Streukens