Patents by Inventor Clive Randall

Clive Randall has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20250262667
    Abstract: Embodiments can relate to an improved hydroflux, additive or electroless plating assisted densification cold sintering process to densify powdered metals at lower compaction pressures and lower temperatures (e.g., 520 MPa and 140° C.). The process can involve inducing dissolution precipitation mechanisms at powder interfaces by introducing a transport phase (formed by the introduction of water during the process to suppress melting temperatures) that is not an aqueous solution. Particle interfaces in the cold sinter fuse together by the presence of the additional transport phase, thereby reducing the temperatures and pressures needed for compaction. Some embodiments involve the use of elements to form a eutectic at the desired low temperature, thereby stabilizing certain crystal structure shapes of isometric crystal systems, inducing rapid densification, and facilitating pore smoothing. Embodiments of the process can be used to generate a green compact via sintering that exhibits improved green strength.
    Type: Application
    Filed: May 5, 2025
    Publication date: August 21, 2025
    Inventors: Selda NAYIR, Ramakrishnan RAJAGOPALAN, Daudi WARYOBA, Clive RANDALL
  • Patent number: 12318841
    Abstract: Embodiments can relate to an improved hydroflux, additive or electroless plating assisted densification cold sintering process to densify powdered metals at lower compaction pressures and lower temperatures (e.g., 520 MPa and 140° C.). The process can involve inducing dissolution precipitation mechanisms at powder interfaces by introducing a transport phase (formed by the introduction of water during the process to suppress melting temperatures) that is not an aqueous solution. Particle interfaces in the cold sinter fuse together by the presence of the additional transport phase, thereby reducing the temperatures and pressures needed for compaction. Some embodiments involve the use of elements to form a eutectic at the desired low temperature, thereby stabilizing certain crystal structure shapes of isometric crystal systems, inducing rapid densification, and facilitating pore smoothing. Embodiments of the process can be used to generate a green compact via sintering that exhibits improved green strength.
    Type: Grant
    Filed: March 29, 2022
    Date of Patent: June 3, 2025
    Assignee: The Penn State Research Foundation
    Inventors: Selda Nayir, Ramakrishnan Rajagopalan, Daudi Waryoba, Clive Randall
  • Patent number: 11812665
    Abstract: A composition includes at least one Pb/Ni/Nb - Pb/Mg/W - Pb/Zr/Ti mixed oxide. A piezoelectric device may be made by providing at least two layers comprising the composition and coated with an outer electrode material; providing a plurality of layers comprising the composition and coated with an inner electrode material; combining or stacking a plurality of layers coated with inner electrode materials between two outer electrodes; and sintering or co-firing the inner electrode materials and outer electrode materials at a temperature at or below about 1000° C.
    Type: Grant
    Filed: May 3, 2019
    Date of Patent: November 7, 2023
    Assignee: QorTek, Inc.
    Inventors: Ahmet Erkan Gurdal, Sinan Dursun, Safakcan Tuncdemir, Clive Randall
  • Publication number: 20220384842
    Abstract: A lithium ion conductive solid electrolyte contains a lithium ion conductive powder having a garnet-type crystal structure including at least Li, La, Zr, and O, and a lithium ion conductive polymer. The lithium ion conductive solid electrolyte can maintain its shape without use of an additional polymer different from the lithium ion conductive polymer. The lithium ion conductive solid electrolyte exhibits an activation energy of 30 kJ/mol or less at 20° C. to 80° C.
    Type: Application
    Filed: October 23, 2020
    Publication date: December 1, 2022
    Inventors: Clive RANDALL, Enrique GOMEZ, Joo Hwan SEO, Masato IWASAKI, Hiroto NAKAYA
  • Publication number: 20220226895
    Abstract: Embodiments can relate to an improved hydroflux, additive or electroless plating assisted densification cold sintering process to densify powdered metals at lower compaction pressures and lower temperatures (e.g., 520 MPa and 140° C.). The process can involve inducing dissolution precipitation mechanisms at powder interfaces by introducing a transport phase (formed by the introduction of water during the process to suppress melting temperatures) that is not an aqueous solution. Particle interfaces in the cold sinter fuse together by the presence of the additional transport phase, thereby reducing the temperatures and pressures needed for compaction. Some embodiments involve the use of elements to form a eutectic at the desired low temperature, thereby stabilizing certain crystal structure shapes of isometric crystal systems, inducing rapid densification, and facilitating pore smoothing. Embodiments of the process can be used to generate a green compact via sintering that exhibits improved green strength.
    Type: Application
    Filed: March 29, 2022
    Publication date: July 21, 2022
    Inventors: Selda Nayir, Ramakrishnan RAJAGOPALAN, Daudi WARYOBA, Clive RANDALL
  • Publication number: 20200239371
    Abstract: Various examples disclosed relate to a substrate. The substrate includes a cold-sintered hybrid material. The cold-sintered hybrid material includes a polymer component and a ceramic component. The substrate further includes a conductor at least partially embedded within the cold-sintered hybrid material. The substrate further includes a via attached to the conductor. The cold-sintered hybrid material has a relative density in a range of from about 80% to about 99%.
    Type: Application
    Filed: August 24, 2018
    Publication date: July 30, 2020
    Inventors: Neal PFEIFFENBERGER, Thomas L. EVANS, Clive RANDALL, Jing GUO
  • Publication number: 20120090657
    Abstract: n-type and p-type thermoelectric materials having high figures of merit are herein disclosed. The n-type and p-type thermoelectric materials are used to generate and harvest energy in thermoelectric power generator and storage modules comprising at least one n-type thermoelectric element coupled to at least one p-type thermoelectric element.
    Type: Application
    Filed: June 15, 2010
    Publication date: April 19, 2012
    Inventors: Soonil Lee, Clive Randall, Rudeger H.T. Wilke, Susan Trolier-Mckinstry
  • Publication number: 20070172592
    Abstract: The invention relates to thin film single layers, electronic components such as multilayer capacitors which utilize thin film layers, and to their methods of manufacture. Chemical solution deposition and microcontact printing of dielectric and electrode layers are disclosed. High permittivity BaTiO3 multilayer thin film capacitors are prepared on Ni foil substrates by microcontact printing and by chemical solution deposition. Multilayer capacitors with BaTiO3 dielectric layers and LaNiO3 internal electrodes are prepared, enabling dielectric layer thicknesses of 1 ?m or less. Microcontact printing of precursor solutions of the dielectric and electrode layers is used.
    Type: Application
    Filed: October 28, 2005
    Publication date: July 26, 2007
    Applicants: The Penn State Research Foundation
    Inventors: Susan Trolier-McKinstry, Clive Randall, Hajime Nagata, Pascal Pinceloup, James Beeson, Daniel Skamser, Michael Randall, Azizuddin Tajuddin