Patents by Inventor Dae Sup Kil

Dae Sup Kil has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 11362326
    Abstract: An embodiment of the present invention provides a method for preparing a silicon-carbon-graphene composite, comprising the steps of: (step 1) adding a carbon precursor solution to silicon and performing wet grinding so as to prepare a suspension: (step 2) forming a silicon-carbon composite by spray drying the suspension; and (step 3) spray drying and heat treating a solution comprising the silicon-carbon composite and graphene oxide.
    Type: Grant
    Filed: May 23, 2017
    Date of Patent: June 14, 2022
    Assignee: Korea Institute of Geoscience and Mineral Resources
    Inventors: Hee-Dong Jang, Han-Kwon Chang, Dae-Sup Kil, Ji-Hyuk Choi, Sun-Kyung Kim
  • Publication number: 20190355985
    Abstract: An embodiment of the present invention provides a method for preparing a silicon-carbon-graphene composite, comprising the steps of: (step 1) adding a carbon precursor solution to silicon and performing wet grinding so as to prepare a suspension: (step 2) forming a silicon-carbon composite by spray drying the suspension; and (step 3) spray drying and heat treating a solution comprising the silicon-carbon composite and graphene oxide.
    Type: Application
    Filed: May 23, 2017
    Publication date: November 21, 2019
    Applicant: Korea Institute of Geoscience And Mineral Resources
    Inventors: Hee-Dong JANG, Han-Kwon CHANG, Dae-Sup Kil, Ji-Hyuk Choi, Sun-Kyung Kim
  • Patent number: 9296617
    Abstract: Disclosed is a method for selectively separating and recovering silicon from waste silicon sludge generated during a semiconductor manufacturing process. With the method for separating and recovering silicon from the silicon sludge, oil components, iron, silicon carbide that are included in the silicon sludge may be removed and silicon may be selectively separated and recovered. In addition, silicon may be efficiently recovered without injection of an additive for precipitating a specific component or without a separate device such as a magnetic separator, or the like, for removing iron.
    Type: Grant
    Filed: October 17, 2012
    Date of Patent: March 29, 2016
    Assignee: Korea Institute of Geoscience and Mineral Resources
    Inventors: Hee Dong Jang, Han Kwon Chang, Dae Sup Kil
  • Patent number: 9238854
    Abstract: Disclosed is a method of producing carbide and carbon nitride powders containing a binder, and cermet obtained from the same. The method includes preparing Ti—Ni alloy powders for Ti alloy powders and graphite, planetary-pulverizing the Ti—Ni alloy powders and the graphite, mortar-pulverizing the alloy powders and the graphite which are subject to the planetary-pulverizing, and performing heat treatment for the Ti—Ni alloy powders and the graphite that are pulverized. Cermet, which is made of the composite powders of carbide and carbon nitride/metal including both TiC which is ceramic material and Ni which is metal is provided.
    Type: Grant
    Filed: March 14, 2013
    Date of Patent: January 19, 2016
    Assignee: KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCES
    Inventors: Han-Jung Kwon, Sun-A Jung, Sung-Wook Cho, Dae-Sup Kil, Ji-Woong Kim, Ki-Min Roh, Jae-Won Lim
  • Patent number: 9102555
    Abstract: The present invention provides a method for removing phosphorus and nitrogen contained in sewage or wastewater using iron ore wastewater. According to the method of the present invention, in which the phosphorus and nitrogen contained in sewage or wastewater are crystallized in the form of struvite using iron ore wastewater containing a large amount of Mg2+ produced in a process of upgrading low-grade iron ore and removed, it is possible to reduce the cost of Mg2+ and the cost of iron ore wastewater treatment, thereby earning economic profits. Moreover, it is possible to prevent water pollution by the removal of the phosphorus and nitrogen contained in sewage or wastewater. Furthermore, it is possible to use struvite crystals obtained as a by-product as a time-release compound fertilizer so as to reduce the amount of fertilizer used and the number of fertilizations, thereby reducing soil contamination.
    Type: Grant
    Filed: November 29, 2011
    Date of Patent: August 11, 2015
    Assignee: Korea Institute of Geosciences and Mineral Resources
    Inventors: Yong Jae Suh, Myung Eun Ju, Dae Sup Kil, Hee Dong Jang
  • Patent number: 8940179
    Abstract: The present invention relates to a method for preparing magnetite nanoparticles from low-grade iron ore using solvent extraction and magnetite nanoparticles prepared by the same. According to the method for magnetite nanoparticles from low-grade iron ore of the present invention, it is possible to prepare high-purity magnetite nanoparticles having a purity of 99% or higher by solvent extraction using low-grade iron ore as a starting material, and thus it is possible to reduce the processing cost and the amount of energy used, thus supplying a high-efficiency magnetite nanoparticle adsorbent, which can be industrially applied to wastewater treatment or desalination plant, in large quantities at low cost. In particular, it is possible to effectively treat livestock wastewater, heavy metal wastewater, oil discharged into rivers, etc. at low cost, thus significantly contributing to the prevention of environmental pollution.
    Type: Grant
    Filed: November 16, 2012
    Date of Patent: January 27, 2015
    Assignee: Korea Institute of Geoscience and Mineral Resources
    Inventors: Yong Jae Suh, Dae Sup Kil, Hee Dong Jang
  • Patent number: 8815267
    Abstract: The present invention provides a hybrid powder of halloysite nanotubes and light-scattering nanoparticles, a method for preparing the same, and a UV-screening cosmetic composition containing the same as an active ingredient. The hybrid powder of halloysite nanotubes and light-scattering nanoparticles according to the present invention, in which the light-scattering nanoparticles are loaded into the halloysite nanotubes, can prevent the light-scattering nanoparticles from penetrating the skin, which minimizes side effects, and has excellent UV-screening effect. Thus, the hybrid powder of halloysite nanotubes and light-scattering nanoparticles according to the present invention can be effectively used as a UV-screening cosmetic composition.
    Type: Grant
    Filed: September 26, 2011
    Date of Patent: August 26, 2014
    Inventors: Yong Jae Suh, Myung Eun Ju, Dae Sup Kil, Sung Wook Cho
  • Publication number: 20130277201
    Abstract: Disclosed is a method for selectively separating and recovering silicon from waste silicon sludge generated during a semiconductor manufacturing process. With the method for separating and recovering silicon from the silicon sludge, oil components, iron, silicon carbide that are included in the silicon sludge may be removed and silicon may be selectively separated and recovered. In addition, silicon may be efficiently recovered without injection of an additive for precipitating a specific component or without a separate device such as a magnetic separator, or the like, for removing iron.
    Type: Application
    Filed: October 17, 2012
    Publication date: October 24, 2013
    Inventors: Hee Dong Jang, Han Kwon Chang, Dae Sup Kil
  • Patent number: 8540957
    Abstract: The present invention provides a method for preparing microtubular halloysite nanopowders by cutting halloysite nanotubes at a high pressure, microtubular halloysite nanopowders prepared by the method, and a cosmetic composition comprising the microtubular halloysite nanopowders. According to the method of the present invention, it is possible to prepare the halloysite nanopowders with a tubular shape using natural halloysite and effectively select a halloysite nanopowder having a desired shape. The microtubular halloysite nanopowders can be used in many industrial fields and used as a container or a carrier for nanoparticles or organic materials such as drugs, air fresheners, cosmetics, agricultural chemical materials, etc.
    Type: Grant
    Filed: November 28, 2010
    Date of Patent: September 24, 2013
    Assignee: Korea Institute of Geoscience and Mineral Resources
    Inventors: Yong Jae Suh, Young Mi Heo, Dae Sup Kil, Sung Wook Cho
  • Patent number: 8512672
    Abstract: Provided are a method for preparing zinc oxide (ZnO) nanoparticles and a method for preparing ZnO nanofluid using the same. The method for preparing ZnO nanoparticles includes: a) heating deionized water; b) dissolving zinc (Zn) salt in the deionized water to prepare a precursor solution; c) adding solid alkali salt to the precursor solution to prepare a dispersion of ZnO nanoparticles; and d) separating the ZnO nanoparticles by solid-liquid separation and washing them with deionized water. Highly pure, crystalline ZnO nanoparticles with spherical shape and very narrow particle size distribution of 10 to 50 nm can be prepared quickly and at large scale and low cost using inexpensive materials via a stable low-temperature process, without using a dispersant. The associated low-temperature, normal-pressure process produces few harmful materials and may be easily employed for production of ZnO nanoparticles.
    Type: Grant
    Filed: August 24, 2010
    Date of Patent: August 20, 2013
    Assignee: Korea Institute of Geoscience and Mineral Resources
    Inventors: Hyo-sook Lee, Yong Jae Suh, Dae Sup Kil, Kuk Cho
  • Publication number: 20130105401
    Abstract: The present invention provides a method for removing phosphorus and nitrogen contained in sewage or wastewater using iron ore wastewater. According to the method of the present invention, in which the phosphorus and nitrogen contained in sewage or wastewater are crystallized in the form of struvite using iron ore wastewater containing a large amount of Mg2+ produced in a process of upgrading low-grade iron ore and removed, it is possible to reduce the cost of Mg2+ and the cost of iron ore wastewater treatment, thereby earning economic profits. Moreover, it is possible to prevent water pollution by the removal of the phosphorus and nitrogen contained in sewage or wastewater. Furthermore, it is possible to use struvite crystals obtained as a by-product as a time-release compound fertilizer so as to reduce the amount of fertilizer used and the number of fertilizations, thereby reducing soil contamination.
    Type: Application
    Filed: November 29, 2011
    Publication date: May 2, 2013
    Inventors: Yong Jae Suh, Myung Eun Ju, Dae Sup Kil, Hee Dong Jang
  • Publication number: 20130078293
    Abstract: The present invention provides a hybrid powder of halloysite nanotubes and light-scattering nanoparticles, a method for preparing the same, and a UV-screening cosmetic composition containing the same as an active ingredient. The hybrid powder of halloysite nanotubes and light-scattering nanoparticles according to the present invention, in which the light-scattering nanoparticles are loaded into the halloysite nanotubes, can prevent the light-scattering nanoparticles from penetrating the skin, which minimizes side effects, and has excellent UV-screening effect. Thus, the hybrid powder of halloysite nanotubes and light-scattering nanoparticles according to the present invention can be effectively used as a UV-screening cosmetic composition.
    Type: Application
    Filed: September 26, 2011
    Publication date: March 28, 2013
    Inventors: Yong Jae Suh, Myung Eun Ju, Dae Sup Kil, Sung Wook Cho
  • Patent number: 8337805
    Abstract: The present invention provides a method for preparing magnetite nanoparticles from low-grade iron ore and magnetite nanoparticles prepared by the same. According to the method of the present invention, in which iron ore leachate is obtained by adding low-grade iron ore powder to an acidic solution, Si and Mg that inhibit the formation of magnetite nanoparticles present in the leachate are selectively removed, iron hydroxide (Fe(OH)3) is allowed to be precipitated from a supernatant containing Fe2+ ions and Fe3+ ions, a mixed iron solution containing Fe2+ ions and Fe3+ ions is prepared using the iron hydroxide (Fe(OH)3), and the mixed iron solution is added to an alkaline solution to react, thereby preparing magnetite nanoparticles.
    Type: Grant
    Filed: November 29, 2011
    Date of Patent: December 25, 2012
    Assignee: Korea Institute of Geoscience and Mineral Resources
    Inventors: Yong Jae Suh, Myung Eun Ju, Dae Sup Kil, Hee Dong Jang
  • Patent number: 8187562
    Abstract: Disclosed is a method for producing a cerium dioxide nanopowder by flame spray pyrolysis. The method comprises dissolving a cerium compound in an organic solvent to prepare a precursor solution, atomizing the precursor solution into microdroplets using an ultrasonic atomizer, transferring the microdroplets together with an argon gas as a carrier gas to a central portion of a high-temperature diffusion flame burner, subjecting the microdroplets to pyrolysis and oxidation in the central portion of the diffusion flame burner to produce a cerium dioxide nanopowder, and collecting the cerium dioxide nanopowder using a collector. According to the method, a cerium dioxide nanopowder can be continuously produced on a large scale by flame spray pyrolysis. In addition, the particle size and uniformity of the cerium dioxide nanopowder can be controlled by appropriately selecting the kind of the solvent and the concentration of the raw material.
    Type: Grant
    Filed: November 24, 2010
    Date of Patent: May 29, 2012
    Assignee: Korea Institute of Geoscience and Mineral Resources (KIGAM)
    Inventors: Han Kwon Chang, Hee Dong Jang, Dae Sup Kil, Kuk Cho, Sung-Wook Cho
  • Publication number: 20120107214
    Abstract: The present invention provides a method for preparing microtubular halloysite nanopowders by cutting halloysite nanotubes at a high pressure, microtubular halloysite nanopowders prepared by the method, and a cosmetic composition comprising the microtubular halloysite nanopowders. According to the method of the present invention, it is possible to prepare the halloysite nanopowders with a tubular shape using natural halloysite and effectively select a halloysite nanopowder having a desired shape. The microtubular halloysite nanopowders can be used in many industrial fields and used as a container or a carrier for nanoparticles or organic materials such as drugs, air fresheners, cosmetics, agricultural chemical materials, etc.
    Type: Application
    Filed: November 28, 2010
    Publication date: May 3, 2012
    Applicant: KOREA INSTITUTE OF GEOSCIENCE AND MINERAL RESOURCES
    Inventors: Yong Jae SUH, Young Mi Heo, Dae Sup Kil, Sung Wook Cho
  • Publication number: 20110281112
    Abstract: Disclosed is a method for producing a cerium dioxide nanopowder by flame spray pyrolysis. The method comprises dissolving a cerium compound in an organic solvent to prepare a precursor solution, atomizing the precursor solution into microdroplets using an ultrasonic atomizer, transferring the microdroplets together with an argon gas as a carrier gas to a central portion of a high-temperature diffusion flame burner, subjecting the microdroplets to pyrolysis and oxidation in the central portion of the diffusion flame burner to produce a cerium dioxide nanopowder, and collecting the cerium dioxide nanopowder using a collector. According to the method, a cerium dioxide nanopowder can be continuously produced on a large scale by flame spray pyrolysis. In addition, the particle size and uniformity of the cerium dioxide nanopowder can be controlled by appropriately selecting the kind of the solvent and the concentration of the raw material.
    Type: Application
    Filed: November 24, 2010
    Publication date: November 17, 2011
    Inventors: Han Kwon CHANG, Hee Dong Jang, Dae Sup Kil, Kuk Cho, Sung-Wook Cho
  • Publication number: 20110230332
    Abstract: There is provided a method for manufacturing oligomer/halloysite composite material including the steps of: adding halloysite powder to an oligomer solution to be mixed; heating the mixed material to expand air inside of halloysite nanotube; and filling the oligomer solution inside of the halloysite nanotube by cooling the mixed material to a room temperature.
    Type: Application
    Filed: May 27, 2011
    Publication date: September 22, 2011
    Applicant: Korea Institute of Geoscience and Mineral Resources (KIGAM)
    Inventors: Kang-Sup CHUNG, Yong-Jae SUH, Dae-Sup KIL, Hwan LEE
  • Publication number: 20110049415
    Abstract: Provided are a method for preparing zinc oxide (ZnO) nanoparticles and a method for preparing ZnO nanofluid using the same. The method for preparing ZnO nanoparticles includes: a) heating deionized water; b) dissolving zinc (Zn) salt in the deionized water to prepare a precursor solution; c) adding solid alkali salt to the precursor solution to prepare a dispersion of ZnO nanoparticles; and d) separating the ZnO nanoparticles by solid-liquid separation and washing them with deionized water. Highly pure, crystalline ZnO nanoparticles with spherical shape and very narrow particle size distribution of 10 to 50 nm can be prepared quickly and at large scale and low cost using inexpensive materials via a stable low-temperature process, without using a dispersant. The associated low-temperature, normal-pressure process produces few harmful materials and may be easily employed for production of ZnO nanoparticles.
    Type: Application
    Filed: August 24, 2010
    Publication date: March 3, 2011
    Applicant: Korea Institute of Geoscience and Mineral Resources (KIGAM)
    Inventors: Hyo-sook Lee, Yong Jae Suh, Dae Sup Kil, Kuk Cho
  • Patent number: 7550618
    Abstract: The present invention relates to a preparation of iron(II) acetate powder from low grade magnetite and comprises the following steps: (a) adding organic acid to low grade magnetite powder to obtain iron solution; (b) adding hydroxide to the iron solution to obtain iron hydroxide; and (c) adding acetic acid to the iron hydroxide, thereby obtaining iron(II) acetate. According to the present invention, it is possible to obtain high purity iron(II) acetate using low grade magnetite and there are advantages of mass producible environmentally-friendly simple process and prevention of corrosion of facilities.
    Type: Grant
    Filed: December 20, 2007
    Date of Patent: June 23, 2009
    Assignee: Korea Institute of Geoscience & Mineral Resources
    Inventors: Hee Dong Jang, Yong Jae Suh, Dae Sup Kil, Kee Kahb Koo, Jae Kyeong Kim, Han Sang Oh
  • Publication number: 20090130485
    Abstract: There is provided a method for manufacturing oligomer/halloysite composite material including the steps of: adding halloysite powder to an oligomer solution to be mixed; heating the mixed material to expand air inside of halloysite nanotube; and filling the oligomer solution inside of the halloysite nanotube by cooling the mixed material to a room temperature.
    Type: Application
    Filed: February 5, 2008
    Publication date: May 21, 2009
    Applicant: Korea Institute of Geoscience and Mineral Resources (KIGAM)
    Inventors: Kang-Sup CHUNG, Yong-Jae SUH, Dae-Sup KIL, Hwan LEE