Patents by Inventor Dai Inoue
Dai Inoue has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Publication number: 20240294417Abstract: In a method of manufacturing porous glass base for optical fiber, a liquid organic siloxane raw material stored in a raw material tank of internal pressure P1 is controlled by a mass flow controller at a predetermined flow rate and pumped through pipe of internal pressure P2 to a vaporizer, the liquid raw material is vaporized in the vaporizer and supplied as a gas raw material to a burner, and the silica fine particles formed by burning the gas raw material in the burner are deposited to form a porous glass base material, where P1?P2 is satisfied.Type: ApplicationFiled: April 26, 2024Publication date: September 5, 2024Inventors: Naoto NODA, Dai INOUE, Hitoshi IINUMA, Hiromasa MIZUKAMI
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Patent number: 11999646Abstract: In a method of manufacturing porous glass base for optical fiber, a liquid organic siloxane raw material stored in a raw material tank of internal pressure P1 is controlled by a mass flow controller at a predetermined flow rate and pumped through pipe of internal pressure P2 to a vaporizer, the liquid raw material is vaporized in the vaporizer and supplied as a gas raw material to a burner, and the silica fine particles formed by burning the gas raw material in the burner are deposited to form a porous glass base material, where P1?P2 is satisfied.Type: GrantFiled: August 2, 2019Date of Patent: June 4, 2024Assignee: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Naoto Noda, Dai Inoue, Hitoshi Iinuma, Hiromasa Mizukami
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Publication number: 20230023064Abstract: Provided is a method for manufacturing an optical fiber glass preform in which a refractive index distribution is stable in a longitudinal direction of the glass preform. A method for manufacturing an optical fiber glass preform includes: depositing a porous glass preform by a vapor phase method; and sintering the porous glass preform in a heating region, when sintering the porous glass preform, the porous glass preform being inserted into a vessel of a sintering furnace, and an inside of the vessel being heated with a heater installed on an outer periphery of the vessel to form the heating region. The sintering is started after a surface temperature difference of the porous glass preform in a longitudinal direction is made 50° C. or lower.Type: ApplicationFiled: July 1, 2022Publication date: January 26, 2023Inventors: Hiroki KOJIMA, Dai INOUE
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Patent number: 11378738Abstract: An optical fiber includes a core with radius r1, a first clad layer with outermost radius r2 adjacent to the core at radial position r1 and covering the outer periphery of the core, a second clad layer with outermost radius r3 adjacent to the first clad layer at radial position r2 and covering the outer periphery of the first clad layer, and a third clad layer adjacent to the second clad layer at radial position r3 and covering the outer periphery of the second clad layer. The refractive index of the first clad layer decreases continuously from the inside to the outside, reaching a maximum value at radial position r1 and a minimum value at radial position r2. The refractive index of the second clad layer increases continuously from the inside to the outside, reaching a minimum value at radial position r2 and a maximum value at radial position r3.Type: GrantFiled: April 13, 2021Date of Patent: July 5, 2022Assignee: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Hiroki Kojima, Dai Inoue
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Publication number: 20210395131Abstract: A manufacturing method of a porous glass preform for optical fiber by depositing glass microparticles on a starting member, including supplying a vaporizer with organic silicon compound raw material in a liquid state and a carrier gas; in the vaporizer, mixing and vaporizing the organic silicon compound raw material in a liquid state and the carrier gas to convert the organic silicon compound raw material and the carrier gas into a raw material mixed gas; supplying a burner with the raw material mixed gas and a combustible gas, combusting the raw material mixed gas and the combustible gas in the burner, and ejecting SiO2 microparticles generated by the combustion from the burner; and depositing the SiO2 microparticles ejected from the burner on the starting member by repeatedly moving a single body, in which the vaporizer and the burner are synchronized, parallel to the starting member in a longitudinal direction thereof.Type: ApplicationFiled: September 1, 2021Publication date: December 23, 2021Inventors: Naoto NODA, Hitoshi IINUMA, Dai INOUE
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Publication number: 20210333471Abstract: An optical fiber includes a core with radius r1, a first clad layer with outermost radius r2 adjacent to the core at radial position r1 and covering the outer periphery of the core, a second clad layer with outermost radius r3 adjacent to the first clad layer at radial position r2 and covering the outer periphery of the first clad layer, and a third clad layer adjacent to the second clad layer at radial position r3 and covering the outer periphery of the second clad layer. The refractive index of the first clad layer decreases continuously from the inside to the outside, reaching a maximum value at radial position r1 and a minimum value at radial position r2. The refractive index of the second clad layer increases continuously from the inside to the outside, reaching a minimum value at radial position r2 and a maximum value at radial position r3.Type: ApplicationFiled: April 13, 2021Publication date: October 28, 2021Inventors: Hiroki KOJIMA, Dai INOUE
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Patent number: 11155488Abstract: A manufacturing method of a porous glass preform for optical fiber by depositing glass microparticles on a starting member, including supplying a vaporizer with organic silicon compound raw material in a liquid state and a carrier gas; in the vaporizer, mixing and vaporizing the organic silicon compound raw material in a liquid state and the carrier gas to convert the organic silicon compound raw material and the carrier gas into a raw material mixed gas; supplying a burner with the raw material mixed gas and a combustible gas, combusting the raw material mixed gas and the combustible gas in the burner, and ejecting SiO2 microparticles generated by the combustion from the burner; and depositing the SiO2 microparticles ejected from the burner on the starting member by repeatedly moving the vaporizer and the burner together, in a synchronized manner, parallel to the starting member in a longitudinal direction thereof.Type: GrantFiled: April 1, 2019Date of Patent: October 26, 2021Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Naoto Noda, Hitoshi Iinuma, Dai Inoue
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Publication number: 20210292222Abstract: A flow rate fluctuation of the liquid raw material of the organic siloxane supplied to the vaporizer is suppressed and a deposition density of the silica fine particles is uniformizes. The method of manufacturing the porous glass base material according to the present invention, a liquid organic siloxane raw material stored in a raw material tank of internal pressure P1 is controlled by a mass flow controller at a predetermined flow rate and pumped through pipe of internal pressure P2 to a vaporizer, the liquid raw material is vaporized in the vaporizer and supplied as a gas raw material to a burner, and the silica fine particles formed by burning the gas raw material in the burner are deposited to form a porous glass base material. The present invention is characterized by the method of manufacture described above, wherein P1?P2 is satisfied.Type: ApplicationFiled: August 2, 2019Publication date: September 23, 2021Inventors: Naoto NODA, Dai INOUE, Hitoshi IINUMA, Hiromasa MIZUKAMI
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Patent number: 10501361Abstract: An optical fiber base material manufacturing method includes: supplying oxygen, hydrogen, and silicide to a core deposition burner; depositing silicon dioxide; adjusting a drawing up speed so that a deposition tip position remains at the same position in accordance with growth of a porous base material; calculating an average of the drawing up speed at each preset time interval; calculating a difference of the calculated average from a preset value of the drawing up speed; correcting a flow rate of silicon tetrachloride when the supplied hydrogen is hydrogen produced or stored at normal temperature, and correcting a flow rate of hydrogen when the supplied hydrogen is hydrogen obtained by vaporizing liquid hydrogen, where when correcting the flow rate of hydrogen, a flow rate of hydrogen supplied to a cladding deposition burner is also corrected in a ratio of before and after the correction of the flow rate of the hydrogen.Type: GrantFiled: January 13, 2011Date of Patent: December 10, 2019Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Dai Inoue, Takaaki Nagao, Hiroyuki Koide
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Publication number: 20190300419Abstract: A manufacturing method of a porous glass preform for optical fiber by depositing glass microparticles on a starting member, including supplying a vaporizer with organic silicon compound raw material in a liquid state and a carrier gas; in the vaporizer, mixing and vaporizing the organic silicon compound raw material in a liquid state and the carrier gas to convert the organic silicon compound raw material and the carrier gas into a raw material mixed gas; supplying a burner with the raw material mixed gas and a combustible gas, combusting the raw material mixed gas and the combustible gas in the burner, and ejecting SiO2 microparticles generated by the combustion from the burner; and depositing the SiO2 microparticles ejected from the burner on the starting member by repeatedly moving the vaporizer and the burner together, in a synchronized manner, parallel to the starting member in a longitudinal direction thereof.Type: ApplicationFiled: April 1, 2019Publication date: October 3, 2019Inventors: Naoto NODA, Hitoshi IINUMA, Dai INOUE
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Patent number: 9527764Abstract: Provided is a quartz glass manufacturing method that involves using one or more burners, supplying hydrogen and oxygen to the one or more burners to generate an oxyhydrogen flame, introducing a silicide into the oxyhydrogen flame, forming a porous base material by depositing silicon dioxide generated from a flame hydrolysis reaction with the silicide, and heating and sintering the porous base material to form transparent glass, the method comprising supplying hydrogen that is stored or made at a normal temperature to the one or more burners; controlling a hydrogen flow rate using a measurement apparatus or control apparatus that performs measurement based on heat capacity of a gas; vaporizing liquid hydrogen stored in a low-temperature storage chamber, and supplying the vaporized liquid hydrogen to the one or more burners as backup hydrogen; switching from the hydrogen to the backup hydrogen; and when switching, adjusting the hydrogen flow rate to a value obtained by multiplying the hydrogen flow rate immediaType: GrantFiled: May 19, 2014Date of Patent: December 27, 2016Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Dai Inoue, Takaaki Nagao, Hiroyuki Koide
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Publication number: 20160214884Abstract: A method for producing a silica glass preform for an optical fiber includes processes for producing a silica glass soot body having a core portion added with a positive dopant and an intermediate portion having a refractive index lower than that of the core portion, heating the soot body at a temperature for transparently vitrifying the same in a helium atmosphere containing a negative dopant and forming a first core rod having the intermediate portion added with the negative dopant, giving a silica glass soot layer as a trench portion to an outer circumference of the first core rod, heating the soot layer at a temperature for transparently vitrifying the same in the helium atmosphere and forming a second core rod having the trench portion added with the negative dopant, and giving silica glass as a cladding portion to an outer circumference of the second core rod.Type: ApplicationFiled: November 6, 2014Publication date: July 28, 2016Applicant: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Dai INOUE, Hiroshi OYAMADA
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Patent number: 8925355Abstract: A method for manufacturing an optical fiber preform that includes preparing a glass cylinder with inner and outer surfaces forming at least part of a cladding portion are repeatedly polished, and a glass core rod that includes a core portion having a higher refractive index than the cladding portion; and inserting the core rod into the glass cylinder and heating the glass cylinder and core rod to form a single body. The repeated polishing of the inner surface of the glass cylinder includes passing pure water that does not contain a cutting fluid over the inner surface for at least the final polishing. The polishing is preferably performed using a polishing cloth to which are affixed diamond abrasive grains. The glass core rod and the glass cylinder are preferably formed of composite quartz glass.Type: GrantFiled: January 25, 2012Date of Patent: January 6, 2015Assignee: Shin-Etsu Chemical Co., Ltd.Inventor: Dai Inoue
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Publication number: 20140308621Abstract: A sintering apparatus comprising a furnace core tube having an opening in a top end through which the soot deposition body is inserted, and having atmospheric gas introduced therein from below and expelled upward; a shaft from which the soot deposition body hangs; a lid that has the shaft inserted therethrough and can cover the opening; a heating furnace that heats the soot deposition body; an internal lid in a top portion of the furnace core tube that divides the top portion of the furnace core tube into an upper region and a lower region; and a gas flow path that connects the two regions to each other and has the atmospheric gas flow therethrough. Total cross-sectional area, relative to movement direction of the atmospheric gas, of the gas flow path is less than cross-sectional area, relative to movement direction of the atmospheric gas, of the furnace core tube.Type: ApplicationFiled: April 8, 2014Publication date: October 16, 2014Applicant: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Dai INOUE, Kazuya UCHIDA
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Publication number: 20140283557Abstract: Provided is a quartz glass manufacturing method that involves using one or more burners, supplying hydrogen and oxygen to the one or more burners to generate an oxyhydrogen flame, introducing a silicide into the oxyhydrogen flame, forming a porous base material by depositing silicon dioxide generated from a flame hydrolysis reaction with the silicide, and heating and sintering the porous base material to form transparent glass, the method comprising supplying hydrogen that is stored or made at a normal temperature to the one or more burners; controlling a hydrogen flow rate using a measurement apparatus or control apparatus that performs measurement based on heat capacity of a gas; vaporizing liquid hydrogen stored in a low-temperature storage chamber, and supplying the vaporized liquid hydrogen to the one or more burners as backup hydrogen; switching from the hydrogen to the backup hydrogen; and when switching, adjusting the hydrogen flow rate to a value obtained by multiplying the hydrogen flow rate immediaType: ApplicationFiled: May 19, 2014Publication date: September 25, 2014Inventors: Dai INOUE, Takaaki Nagao, Hiroyuki KOIDE
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Patent number: 8839645Abstract: A method of manufacturing an optical fiber base material includes: forming a porous glass base material by depositing glass particles; providing a synthetic quartz glass vessel at least partly made of quartz glass which contains aluminum equal to or less than 0.01 ppm; introducing dehydration reaction gas and inert gas into the vessel; heating a portion made of quartz glass which contains aluminum equal to or less than 0.01 ppm in the vessel that contains the dehydration reaction gas and the inert gas; and inserting the porous glass base material into the heated vessel to dehydrate and sinter the porous glass base material.Type: GrantFiled: July 22, 2013Date of Patent: September 23, 2014Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Dai Inoue, Hiroyuki Koide, Takaaki Nagao
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Publication number: 20140230494Abstract: A method of manufacturing quartz glass includes depositing soot generated by flame hydrolysis of a raw material gas to a starting member, while the starting member is raised and rotated, to form a soot deposition member that includes an effective portion having a substantially constant outer diameter, the effective portion to become a material of a glass product, an upper ineffective portion formed at an upper end of the effective portion, and a lower ineffective portion formed at a lower end of the effective portion, each of the ineffective portions having an outer diameter changing in a tapering form, wherein the depositing includes forming the lower ineffective portion while decreasing a peripheral speed of a surface of the starting member to a predetermined final peripheral speed in a ratio of 1.3 m/minute or below per second during a period after the effective portion is formed.Type: ApplicationFiled: April 23, 2014Publication date: August 21, 2014Applicant: SHIN-ETSU CHEMICAL CO., LTD.Inventors: Dai Inoue, Makoto Yoshida
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Patent number: 8726693Abstract: There is provided an apparatus for supplying a hydrogen gas to a quartz glass manufacturing apparatus including a burner that generates an oxyhydrogen flame when supplied with the hydrogen gas, where the apparatus includes: a first hydrogen supply system that supplies a hydrogen gas in which isomers are in equilibrium; a second hydrogen supply system that supplies a hydrogen gas in which isomers are out of equilibrium; a flow rate control section that includes: a valve that changes a flow rate of the hydrogen gas to be supplied to the burner; a first flow rate measuring section that measures the flow rate of the hydrogen gas to be supplied to the burner by measuring a heat capacity; and a control section that controls the valve in such a manner that a measured value obtained by the first flow rate measuring section approaches a set value input from outside; a second flow rate measuring section that measures the flow rate of the hydrogen gas to be supplied to the burner by measuring a different factor than theType: GrantFiled: February 16, 2010Date of Patent: May 20, 2014Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Dai Inoue, Takaaki Nagao, Hiroyuki Koide
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Patent number: 8701447Abstract: A method of manufacturing an optical fiber base material includes: forming a porous glass base material by depositing glass particles; providing a vessel which employs a composite tube, the composite tube including a portion formed by jacketing a first quartz glass containing aluminum equal to or less than 0.01 ppm with a second quartz glass containing aluminum equal to or more than 15 ppm; introducing dehydration reaction gas and inert gas into the vessel; heating the jacketed portion in the vessel which contains the dehydration reaction gas and the inert gas; and inserting the porous glass base material into the heated vessel to dehydrate and sinter the porous glass base material.Type: GrantFiled: December 22, 2008Date of Patent: April 22, 2014Assignee: Shin-Etsu Chemical Co., Ltd.Inventors: Dai Inoue, Hiroyuki Koide, Takaaki Nagao
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Publication number: 20130298611Abstract: A method of manufacturing an optical fiber base material includes: forming a porous glass base material by depositing glass particles; providing a synthetic quartz glass vessel at least partly made of quartz glass which contains aluminum equal to or less than 0.01 ppm; introducing dehydration reaction gas and inert gas into the vessel; heating a portion made of quartz glass which contains aluminum equal to or less than 0.01 ppm in the vessel that contains the dehydration reaction gas and the inert gas; and inserting the porous glass base material into the heated vessel to dehydrate and sinter the porous glass base material.Type: ApplicationFiled: July 22, 2013Publication date: November 14, 2013Applicant: c/o Shin-Etsu Chemical Co., Ltd.Inventors: Dai Inoue, Hiroyuki Koide, Takaaki Nagao