Abstract: An NMR rotor comprises a receptacle for inserting a sample container into a homogeneous region of an NMR magnetic field with flux density B, the field vector of which in the homogeneous region extends in the vertical direction along a z-axis. The rotor passes through regions with inhomogeneous magnetic field components and a flux density gradient dB/dz when the sample container is introduced. The rotor includes at least two different materials, one with diamagnetic properties and another with non-diamagnetic properties. The different materials are arranged to be geometrically distributed in the rotor so that the magnetic force on the rotor under the effect of a product t of magnetic flux density B and flux density gradient dB/dz, the magnitude of which exceeds 1400 T2/m, either acts in the same direction as the weight force of the rotor or is smaller in magnitude than the weight force of the rotor.

Abstract: An adjustment device (1) for an RF resonant circuit (96) of an NMR probe (90) has a plurality of movable elements (6) which are arranged in succession, such that adjacent movable elements mutually engage, so as to be movable relative to one another in a limited range. The movable elements each have at least one electrical functional part (20; 20a-20b) for adjusting the RF resonant circuit. N outwardly oriented electrical contact elements (15; 15a-15b; 23, 24) include at least two functional part terminals (21, 22), and the electrical contact elements are each connected to a functional part terminal. The adjustment device also includes a first connection assembly (11) for slidingly contacting at least a portion of the movable elements from outside, to contact the contact elements in dependence on the movement position of the movable elements, as well as a movement device (4), configured to move one of the movable elements.

Abstract: An adjustment device (1) for an RF resonant circuit (96) of an NMR probe (90) has a plurality of movable elements (6) which are arranged in succession, such that adjacent movable elements mutually engage, so as to be movable relative to one another in a limited range. The movable elements each have at least one electrical functional part (20; 20a-20b) for adjusting the RF resonant circuit. N outwardly oriented electrical contact elements (15; 15a-15b; 23, 24) include at least two functional part terminals (21, 22), and the electrical contact elements are each connected to a functional part terminal. The adjustment device also includes a first connection assembly (11) for slidingly contacting at least a portion of the movable elements from outside, to contact the contact elements in dependence on the movement position of the movable elements, as well as a movement device (4), configured to move one of the movable elements.

Abstract: A transport device for transporting an NMR sample to the probe head (16) of an NMR spectrometer by means of a transport system (12) is characterized in that the transport device comprises a shuttle (15) adapted for use with a transport system. The transport system is structured to transport an HR-NMR sample spinner or an NMR MAS rotor (5). The shuttle includes a locking device for the NMR MAS rotor, the locking device being formed such that the NMR MAS rotor is released by unlocking the locking device and can be transferred to and received by the NMR MAS probe head. It is therefore possible to rapidly change from NMR spectroscopy of liquids to NMR spectroscopy of solids, and vice versa, simply by exchanging the probe head, without converting the transport system.

Abstract: An NMR probe head has a capacitor with a dielectric (5), which surrounds a cavity (15) in which a capacitor piston (7) is disposed. A sliding bush (9) has a through hole (16) in which a piston operating rod (8) extends. The piston operating rod (8) is connected to a piezo-electric actuator and to the capacitor piston (7) in such a way that it displaces the capacitor piston linearly when a sawtooth voltage is applied to the piezo-electric actuator. The sliding bush thereby applies braking friction to the piston operating rod during linear displacement of the capacitor piston and only allows the piston operating rod to slide through during the steep edges of the sawtooth voltage. This avoids the disadvantages of prior art, wherein the NMR probe head remains compact and the material cost and manufacturing complexity are reduced.

Abstract: A transport device for transporting an NMR sample to the probe head (16) of an NMR spectrometer by means of a transport system (12) is characterized in that the transport device comprises a shuttle (15) adapted for use with a transport system. The transport system is structured to transport an HR-NMR sample spinner or an NMR MAS rotor (5). The shuttle includes a locking device for the NMR MAS rotor, the locking device being formed such that the NMR MAS rotor is released by unlocking the locking device and can be transferred to and received by the NMR MAS probe head. It is therefore possible to rapidly change from NMR spectroscopy of liquids to NMR spectroscopy of solids, and vice versa, simply by exchanging the probe head, without converting the transport system.

Abstract: An NMR (nuclear magnetic resonance) apparatus has a magnet system disposed in a cryostat (1), the cryostat having at least one nitrogen tank (3b) for receiving liquid nitrogen (5b) and a room temperature bore (7) for receiving an NMR probehead (8), wherein part(s) of the probehead or the overall probehead can be cooled to cryogenic temperatures by supplying liquid nitrogen (5b) via a supply line (14). The nitrogen tank (3b) of the cryostat (1) is connected to the NMR probehead (8) by means of a supply line (14) in such a fashion that liquid nitrogen (5b) is removed from the nitrogen tank (3b) and guided to the NMR probehead (8). The overall apparatus is therefore more compact, the operating comfort of the apparatus is increased, and the costs for acquisition, operation and maintenance are considerably reduced compared to previous comparable devices.

Abstract: An NMR probe head has a capacitor with a dielectric (5), which surrounds a cavity (15) in which a capacitor piston (7) is disposed. A sliding bush (9) has a through hole (16) in which a piston operating rod (8) extends. The piston operating rod (8) is connected to a piezo-electric actuator and to the capacitor piston (7) in such a way that it displaces the capacitor piston linearly when a sawtooth voltage is applied to the piezo-electric actuator. The sliding bush thereby applies braking friction to the piston operating rod during linear displacement of the capacitor piston and only allows the piston operating rod to slide through during the steep edges of the sawtooth voltage. This avoids the disadvantages of prior art, wherein the NMR probe head remains compact and the material cost and manufacturing complexity are reduced.

Abstract: An NMR (nuclear magnetic resonance) apparatus has a magnet system disposed in a cryostat (1), the cryostat having at least one nitrogen tank (3b) for receiving liquid nitrogen (5b) and a room temperature bore (7) for receiving an NMR probehead (8), wherein part(s) of the probehead or the overall probehead can be cooled to cryogenic temperatures by supplying liquid nitrogen (5b) via a supply line (14). The nitrogen tank (3b) of the cryostat (1) is connected to the NMR probehead (8) by means of a supply line (14) in such a fashion that liquid nitrogen (5b) is removed from the nitrogen tank (3b) and guided to the NMR probehead (8). The overall apparatus is therefore more compact, the operating comfort of the apparatus is increased, and the costs for acquisition, operation and maintenance are considerably reduced compared to previous comparable devices.

Abstract: A transport device for conveying an object to be transported (18) between an input point (A) and a supply point (Z), where the object to be transported (18) can be supplied to an RT tube (4) of a cryostat (1), wherein the input point (A) is both horizontally and also vertically spaced apart from the supply point (Z), wherein a transport tube (14) is provided for pneumatically conveying the object to be transported within the transport tube (14) from a first transfer point (B) to a second transfer point (C), is characterized in that the transport tube (14) is vertically arranged, a first transport container (TB1) and a second transport container (TB2) are provided for receiving the object to be transported (18), a first transfer device is disposed between the input point (A) and the first transfer point (B), and a second transfer device is provided between the second transfer point (C) and the supply point (Z).

Abstract: A transport device for conveying an object to be transported (18) between an input point (A) and a supply point (Z), where the object to be transported (18) can be supplied to an RT tube (4) of a cryostat (1), wherein the input point (A) is both horizontally and also vertically spaced apart from the supply point (Z), wherein a transport tube (14) is provided for pneumatically conveying the object to be transported within the transport tube (14) from a first transfer point (B) to a second transfer point (C), is characterized in that the transport tube (14) is vertically arranged, a first transport container (TB1) and a second transport container (TB2) are provided for receiving the object to be transported (18), a first transfer device is disposed between the input point (A) and the first transfer point (B), and a second transfer device is provided between the second transfer point (C) and the supply point (Z).

Abstract: Measuring module for the measurement of an object (6), having a measuring chamber (4), with a contact element (5a, 5b), wherein the object to be measured (6) is thermally connected to a first contact surface (9a) of the contact element (5a, 5b), and having a cold head (1b, 2b, 2c) that can be thermally connected to a second contact surface (9b) of the contact element (5a, 5b), wherein the contact element (5a, 5b) consists of material with high thermal conductivity, characterized in that the cryo-refrigerator (1a, 2a) together with the cold head is housed in a refrigerating chamber (3) that is physically separated from the measuring chamber (4) and can be evacuated separately from the latter, and the contact element (5a, 5b) is thermally insulated from the outside wall of the measuring module, is part of a separating wall between the measuring chamber (4) and the refrigerating chamber (3), and makes a local thermal connection between the measuring chamber (4) and the refrigerating chamber (3), and with a conta

Abstract: Measuring module for the measurement of an object (6), having a measuring chamber (4), with a contact element (5a, 5b), wherein the object to be measured (6) is thermally connected to a first contact surface (9a) of the contact element (5a, 5b), and having a cold head (1b, 2b, 2c) that can be thermally connected to a second contact surface (9b) of the contact element (5a, 5b), wherein the contact element (5a, 5b) consists of material with high thermal conductivity, characterized in that the cryo-refrigerator (1a, 2a) together with the cold head is housed in a refrigerating chamber (3) that is physically separated from the measuring chamber (4) and can be evacuated separately from the latter, and the contact element (5a, 5b) is thermally insulated from the outside wall of the measuring module, is part of a separating wall between the measuring chamber (4) and the refrigerating chamber (3), and makes a local thermal connection between the measuring chamber (4) and the refrigerating chamber (3), and with a conta

Abstract: A magnetic resonance (MR) probe head comprises a detecting device with at least one antenna system which is cryogenically cooled by a cooling device, and a cooled preamplifier in a preamplifier housing which is spatially separated from the detecting device, and a thermally insulating connecting means via which the detecting device and the preamplifier housing are connected, wherein the connecting means comprises at least one cooling line for supplying and/or returning a cooling fluid, and with at least one RF line for transmitting the electric signals. The connecting means is implemented as a mechanically flexible connecting line with mechanically flexible RF lines and cooling lines disposed therein. The MR probe head is easy to handle and can be highly sensitive, wherein the detecting device can be quickly installed, removed and put into operation.

Abstract: An NMR apparatus comprising an NMR magnet system disposed in a first cryocontainer (2) of a cryostat (9), and an NMR probe head (1), wherein the first cryocontainer (2) is installed in an evacuated outer jacket and is surrounded by a radiation shield (24) and/or a further cryocontainer (3), wherein a cooling device is provided for cooling the NMR probe head (1) and a cryocontainer (2, 3), which comprises a cold head (4, 4a, 4b, 4c) with several cold stages (12a, 12b, 12c, 18a, 18b, 18c, 19a), wherein one cold stage (12a, 12b, 12c, 18a, 18b, 18c, 19a) is connected to a heat-transferring device, and wherein a cooling circuit is provided between the cooling device and the NMR probe head (1), is characterized in that the cooling device is disposed in a separate, evacuated housing (6) which is positioned directly above the cryostat (9), wherein the heat-transferring device is inserted directly into suspension tubes (29a, 29c) of the cryocontainer (2, 3) and/or is in contact with the radiation shield (24).

Abstract: A magnetic resonance (MR) probe head comprises a detecting device (3) with at least one antenna system which is cryogenically cooled by a cooling device, and a cooled preamplifier (16) in a preamplifier housing (15a) which is spatially separated from the detecting device (3), and a thermally insulating connecting means via which the detecting device (3) and the preamplifier housing are connected, wherein the connecting means (15c) comprises at least one cooling line (9, 9a, 9b) for supplying and/or returning a cooling fluid, and with at least one RF line (10) for transmitting the electric signals. The connecting means is implemented as a mechanically flexible connecting line (8) with mechanically flexible RF lines (10) and cooling lines (9, 9a, 9b) disposed therein. The MR probe head is easy to handle and can be highly sensitive, wherein the detecting device can be quickly installed, removed and put into operation.

Abstract: An NMR spectrometer comprising an NMR magnet system (27) disposed in a helium tank of a cryostat and an NMR probe head (11) disposed in a room temperature bore of the cryostat, which contains a cooled RF resonator (9) for receiving NMR signals from a sample to be investigated, and a cooled pre-amplifier (10), wherein the NMR probe head (11) is cooled by a common multi-stage compressor-operated refrigerator (2), wherein the refrigerator (2) comprises a cold head and several heat exchangers (5, 6) at different temperature levels, wherein the refrigerator (2) is disposed at a spatial separation from the cryostat in a separate, evacuated and thermally insulated housing (1) and wherein at least one cooling circuit with cooling lines, which are thermally insulated by a transfer line (13, 14) is disposed between the housing (1) containing the heat exchangers (5, 6) and the NMR probe head (11), is characterized in that additional cooling lines to an LN2 tank (18) or radiation shield (21) disposed in the cryostat and