Abstract: A method and apparatus for the purification and collection of hydrogen isotopes in a flowing inert gaseous mixture containing impurities, wherein metal alloy getters having the capability of sorbing non-hydrogen impurities such as oxygen, carbon dioxide, carbon monoxide, methane, ammonia, nitrogen and water vapor are utilized to purify the gaseous mixture of impurities. After purification hydrogen isotopes may be more efficiently collected. A plurality of parallel process lines utilizing metal getter alloys can be used to provide for the continuous purification and collection of the hydrogen isotopes.

Abstract: A centrifugal separator has a housing with a generally cylindrical inner surface defining an inner chamber. A hollow rotor is disposed within the chamber for rotation therein. At least one inlet is provided for introducing a liquid mixture into the annular volume between the rotor and the housing, where it is then directed into the rotor. An upper rotor assembly separates the liquid mixture by phase densities with the disparate components directed to respective outlets. In one embodiment of the invention, the upper rotor assembly includes an easily removable weir ring to facilitate "tuning" of the separation process. The rotor of the separator is mounted on a unitary rotor shaft that extends axially through the separation chamber to upper and lower bearing assemblies in the separator housing.

Abstract: A centrifugal separator includes a rotor sleeve which reduces the fine scale mixing of liquid components. The rotor sleeve in the annular mixing zone minimizes liquid-liquid shear, but does not adversely affect the pumping action of the rotor. The separator comprises a housing having a generally cylindrical inner surface defining an interior chamber. A hollow rotor is disposed within the chamber for rotation therein, the rotor having upper and lower openings and a generally cylindrical rotor wall with an inner and outer surface. The outer surface of the rotor wall is spaced apart from the inner surface of the housing and thereby defines the annular mixing zone. The rotor sleeve comprises a cylinder only slightly larger than the rotor. The sleeve is fixed relative to the housing, thereby preventing liquid within the annular mixing zone from contacting the rotating outer surface of the rotor. The reduction in mixing action dramatically increases the separation efficiency for shear-sensitive liquid mixtures.

Abstract: This system measures tritium on-line and collects tritium from a flowing inert gas stream. It separates the tritium from other non-hydrogen isotope contaminating gases, whether radioactive or not. The collecting portion of the system is constructed of various zirconium alloys called getters. These alloys adsorb tritium in any of its forms at one temperature and at a higher temperature release it as a gas. The system consists of four on-line getters and heaters, two ion chamber detectors, two collection getters, and two guard getters. When the incoming gas stream is valved through the on-line getters, 99.9% of it is adsorbed and the remainder continues to the guard getter where traces of tritium not collected earlier are adsorbed. The inert gas stream then exits the system to the decay chamber.Once the on-line getter has collected tritium for a predetermined time, it is valved off and the next on-line getter is valved on.

Abstract: The invention is a process for the recovery of hazardous wastes such as heavy metals and radioactive elements from phenolic resin filter by a circulating a solution of 8 to 16 molar nitric acid at a temperature of 110 to 190 degrees F. through the filter. The hot solution dissolves the filter material and releases the hazardous material so that it can be recovered or treated for long term storage in an environmentally safe manner.

Abstract: The invention provides a method of separating a mixed component waste stream in a centrifugal separator. The mixed component waste stream is introduced into the separator and is centrifugally separated within a spinning rotor. A dual vortex separation occurs due to the phase density differences, with the phases exiting the rotor distinct from one another. In a preferred embodiment, aqueous solutions of organics can be separated with up to 100% efficiency. The relatively more dense water phase is centrifugally separated through a radially outer aperture in the separator, while the relatively less dense organic phase is separated through a radially inner aperture.