Abstract: An electrode material of a supercapacitor includes a negative material prepared by the following steps: first dispersing graphite oxide in deionized water; after stirring and ultrasonic treatment, reducing the graphite oxide into reduced graphene oxide by using a hydrazine hydrate, and vacuum drying at 40-80° C.; dispersing the reduced graphene oxide in a DMF solution with 2,6-diaminoanthraquinone, and stirring and performing the ultrasonic treatment again; at 60-90° C., adding isoamyl nitrite, and reacting for 18-24 h; and washing reaction products with ethanol and deionized water for multiple times, and finally freeze drying to obtain a product.

Abstract: A preparation method of SnO2@Sn coated reduced graphene oxide composite material. By compounding reduced graphene oxide and SnO2, SnO2 undergoes conversion and alloying reactions to form Sn nanoparticles, and the three components have a synergistic effect and good reversibility. Nano SnO2@Sn particles are uniformly distributed on the ultrathin RGO nanosheets. RGO can effectively alleviate volume expansion caused by SnO2 and prevent SnO2@Sn nanoparticles from agglomeration during cycle. The adhesion of SnO2@Sn on RGO can also effectively reduce the repacking of RGO nanosheets, so that the composite material maintains a large surface area during the charge-discharge process, providing sufficient space for the storage of potassium ions. Therefore, the prepared SnO2@Sn coated reduced graphene oxide composite material (SnO2 @Sn@RGO) has excellent electrochemical performance, exhibits excellent cycle performance, rate capability and long-term cycle stability, and has a very ideal first coulomb efficient.

Abstract: A method for preparing a double-sided microlens array, which is used to prepare a uniform, large-area and easy-to-control microlens array on upper and lower surfaces of a sapphire glass lens. A complete laser wavefront is spatially divided into many tiny parts, and each part is focused on the focal plane by a corresponding small lens, and the light spots are overlapped to achieve uniform light in a specific area. The sapphire glass lens is applied to the deep ultraviolet LED inorganic module packaging device to reduce the total reflection loss between the deep ultraviolet LED package optical window-air interface, and focus the light passing through the lens on the focal plane, while increasing the emission of light Coupling ability, uniform light intensity of ultraviolet LED.

Abstract: A preparation method of fluorocarbon-coated VSe2 composite (VSe2@CF) anode electrode material, including: weighting and dissolving an acetylacetone oxovanadium (VO(acac)2) and a selenium dioxide in a solvent to prepare a first solution with a concentration of 0.5-2 mol/L, and stirring the first solution for 0.5 h to obtain a dark green solution; adding the dark green solution with an organic acid to obtain a second solution; transferring the second solution to a polytetrafluoroethylene-lined high-pressure hydrothermal reactor, and holding at a heat insulation temperature for 15-30 h to obtain a third solution; after the third solution is cooled, suction filtering the cooled third solution, and washing the filtered third solution repeatedly to obtain a precipitate; drying the precipitate to obtain a black powder; co-mixing a citric acid solution with the black powder, stirring, ball milling, and drying; and heating up, holding, and finally cooling naturally to room temperature under inert atmosphere.

Abstract: The disclosure relates to a method for preparing a 3D sponge structured carbonitride coated VSe2 composite (3D-VSe2@CN), belonging to the technical fields of electrode materials and preparation of batteries. In the disclosure, carbon, nitrogen and VSe2 are composited by using NaCl as a template so as to construct a 3D sponge structured carbonitride coated VSe2 composite. The 3D sponge structure can increase the structure stability of the material in the cyclic process, and the carbocanitride can increase the electron conductivity and activity sites of the material, so as to allow easier diffusion of potassium ions. Meanwhile, the stable structure can cause the clustering of VSe2 all the time. Thus, the prepared composite has good and stable rate capability and cycle stability. The process method is simple, low in cost, environmental-friendly, and suitable for large-scale industrial production.

Abstract: The disclosure relates to a Fe3C-doped graded porous carbon polymer potassium ion anode material as well as a preparation method and application thereof. In the method, previously prepared Fe2O3 is added into phenylamine, pyrrole, thiophene and cellulose acetate solutions, the above mixture is evaporated at the low temperature of 65-100° C., and then the evaporated product is calcinated to obtain a potassium battery anode material. This material consists of carbon nano sheets having different pore diameters, and has a graded porous structure of micropores, mesopores and macropores. Physical characterization results show that this material has the characteristics of large interlayer spacing, high specific surface area, rich defects and the like; electrochemical testing results show that this material has high reversible capacity and excellent cycle stability and rate performance.

Abstract: The present invention discloses a preparation method of 2,6-diaminoanthraquinone bifunctional covalently grafted graphene as a negative material of a supercapacitor, which includes: first dispersing graphite oxide in deionized water; after stirring and ultrasonic treatment, reducing the graphite oxide into reduced graphene oxide by using a hydrazine hydrate, and vacuum drying at 40-80° C.; dispersing the reduced graphene oxide in a DMF solution with 2,6-diaminoanthraquinone, and stirring and performing the ultrasonic treatment again; at 60-90° C., adding isoamyl nitrite, and reacting for 18-24 h; and washing reaction products with ethanol and deionized water for multiple times, and finally freeze drying to obtain a product.

Abstract: The disclosure provides a preparation method of a vanadium selenide/carbon cellulose composite, belonging to the technical fields of electrode materials of potassium ion batteries and preparation technologies thereof. Through compounding of carbon, carbon cellulose and vanadium diselenide (VSe2), a synergistic effect occurs between two components, and carbon cellulose-carbon coating is capable of increasing electron conductivity and potassium ion diffusion rate of a material while inhibiting the agglomeration of vanadium diselenide (VSe2). Therefore, the prepared vanadium selenide/carbon cellulose composite has excellent electrochemical performance and exhibits outstanding rate performance and cycling stability. The method is simple in process, low in cost, environmentally friendly, and suitable for large-scale industrial production.

Abstract: The present invention relates to a preparation method of a carbon quantum dot/carbon coated VSe2 composite material (VSe2@CQD), and belongs to the technical field of electrode material of a potassium ion battery and preparation thereof. By compositing the carbon, carbon quantum dots and vanadium diselenide (VSe2), the three components generate a synergistic effect. The carbon quantum dot/carbon coating can improve the electronic conductivity and lithium ion diffusion rate of the material, and also can inhibit the agglomeration of the vanadium diselenide (VSe2). Therefore, the prepared carbon quantum dot/carbon coated VSe2 composite material (VSe2@CQD) has excellent electrochemical performance and excellent rate performance and cycle stability. The method is simple in process, low in cost, environment-friendly, and suitable for large-scale industrial production.

Abstract: An LED flip-chip structure is provided, wherein a silica gel, a fluorescent glue, a lens, an anti-reflection film and a packaging adhesive layer is sequentially arranged on the LED chip. The silica gel and fluorescent glue are sequentially filled within an insulating reflective cup, outside which a metal reflective cup and a light absorption layer is sequentially provided. The packaging adhesive layer is filled between the reflective cup and the lens. A sapphire substrate is pretreated to form an inverted T-shaped structure, on which a layer of epitaxial wafer of ceramic film is grown, and then a layer of high temperature resistant conductive film is grown on upper surfaces of grooves at both sides. A protrusion of the inverted T-shaped structure is uniformly coated with a thermally conductive adhesive with a certain thickness.