Patents by Inventor Dimitri Golubev

Dimitri Golubev has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Publication number: 20240183610
    Abstract: A SPECTRA process for low-temperature fractionation of air is proposed, in which bottoms liquid from an additional second rectification column used to obtain oxygen is evaporated in a second condenser evaporator arrangement. In this second condenser evaporator arrangement, gas that has been evaporated beforehand in a first condenser evaporator arrangement, which is used for condensation of tops gas from a first rectification column, is partially condensed after recompression. The invention also relates to a corresponding plant.
    Type: Application
    Filed: March 10, 2022
    Publication date: June 6, 2024
    Inventors: Dimitri GOLUBEV, Xiaohua FAN
  • Patent number: 11959701
    Abstract: An air separation unit and associated method for separating air by cryogenic distillation using a distillation column system including a higher pressure column, a lower pressure column, an intermediate pressure kettle column, and an argon column arrangement is provided. The disclosed air separation unit and method is particularly suited for production of high purity nitrogen for electronics applications and includes nitrogen recycle circuit necessary to attain the higher purity nitrogen products. In addition to the intermediate pressure kettle column, the present air separation unit and associated method employs a once-through argon condenser, preferably disposed within the lower pressure column as well as a once-through kettle column reboiler, a once-through kettle column condenser.
    Type: Grant
    Filed: July 28, 2022
    Date of Patent: April 16, 2024
    Assignee: Praxair Technology, Inc.
    Inventors: Neil M. Prosser, Dimitri Golubev
  • Publication number: 20240035742
    Abstract: An air separation unit and associated method for separating air by cryogenic distillation using a distillation column system including a higher pressure column, a lower pressure column, an intermediate pressure kettle column, and an argon column arrangement is provided. The disclosed air separation unit and method is particularly suited for production of high purity nitrogen for electronics applications and includes nitrogen recycle circuit necessary to attain the higher purity nitrogen products. In addition to the intermediate pressure kettle column, the present air separation unit and associated method employs a once-through argon condenser, preferably disposed within the lower pressure column as well as a once-through kettle column reboiler, a once-through kettle column condenser.
    Type: Application
    Filed: July 28, 2022
    Publication date: February 1, 2024
    Inventors: Neil M. Prosser, Dimitri Golubev
  • Publication number: 20240003620
    Abstract: A process for cryogenic separation of air using an air separation plant configured as a high air pressure air separation plant is provided, wherein of the air initially compressed several partial air streams are formed which are at least in part further compressed, cooled in a main heat exchanger and expanded before being introduced into the column system. The partial air streams include a first partial air stream and a second partial air stream whose air is compressed in parallel in a first warm booster and a second warm booster and thereafter expanded in a first expander and a second expander mechanically coupled to the first booster and to the second booster, respectively. A corresponding air separation plant is also part of the present invention.
    Type: Application
    Filed: November 22, 2021
    Publication date: January 4, 2024
    Inventor: Dimitri GOLUBEV
  • Patent number: 11846468
    Abstract: The invention relates to a method for a low-temperature air separation in which an air separation unit is used comprising a first rectification column and a second rectification column. The first rectification column is operated at a first pressure level, and the second rectification column is operated at a second pressure level below the first pressure level. Fluid which is oxygen-enriched compared to atmospheric air is drawn from the first rectification column in the form of one or more first material flows. At least one fraction of the fluid which has been drawn from the first rectification column in the form of the one or more first material flows is heated in a heat exchanger; a fraction of the fluid which has been heated in the heat exchanger is compressed using a compressor and is returned to the first rectification column.
    Type: Grant
    Filed: October 22, 2019
    Date of Patent: December 19, 2023
    Assignee: Linde GmbH
    Inventors: Christian Kunz, Stefan Lochner, Wolfgang Haag, Lars Kirchner, Tobias Lautenschlager, Dimitri Golubev
  • Publication number: 20230358468
    Abstract: In this process and apparatus for cryogenic separation of air, the separation column system comprises a high-pressure column, a low-pressure column and a crude argon column. A mixed gas stream produced by mixing gaseous oxygen and a gas stream from the evaporation space of the argon top condenser, is work expanded in a mixed gas turbine.
    Type: Application
    Filed: September 9, 2021
    Publication date: November 9, 2023
    Inventor: Dimitri GOLUBEV
  • Publication number: 20230168030
    Abstract: The invention relates to a process for cryogenic fractionation of air using an air fractionation plant comprising a rectification column system comprising a high-pressure column operated at a pressure level of 9 to 14.5 bar, a low-pressure column operated at a pressure level of 2 to 5 bar, and an argon column. It is envisaged that a recirculating stream is formed using the second tops gas or a portion thereof, which is heated, compressed, cooled again, and after partial or complete liquefaction or in the unliquefied state is introduced partially or completely, or in fractions, into the first rectification column and/or into the second rectification column. The present invention also relates to a corresponding system.
    Type: Application
    Filed: April 6, 2021
    Publication date: June 1, 2023
    Inventor: Dimitri GOLUBEV
  • Publication number: 20230125267
    Abstract: According to the present invention, a method for cryogenic separation of air using an air separation unit comprising a rectification column is provided. Feed air is compressed, cooled and rectified in the rectification column obtaining an overhead gas, wherein a part of the overhead gas of the rectification column is condensed using fluid withdrawn from the rectification column, wherein the condensed overhead gas is used at least in part as a liquid reflux to the rectification column, wherein a first part of the fluid which is used for cooling the overhead gas of the rectification column is, after its use for cooling, compressed and reintroduced into the rectification column, and wherein a second part of the fluid which is used for cooling the overhead gas of the rectification column is, after its use for cooling, expanded and withdrawn from the air separation unit.
    Type: Application
    Filed: March 2, 2021
    Publication date: April 27, 2023
    Inventors: Dimitri GOLUBEV, Eric DOPPLER
  • Patent number: 11602713
    Abstract: A method for cryogenic separation of air uses an air separation plant, wherein, in a mass transfer column, a liquid first fluid and a gaseous second fluid are subjected to mass transfer with one another. A gaseous third fluid is removed from the column and is at least partly discharged from the air separation plant. A liquid fourth fluid is removed from the column and is at least partly fed into a low-pressure column. The first fluid is formed using at least a part of an oxygen-rich liquid removed from the low-pressure column. The second fluid is formed using an oxygen-enriched liquid removed from a high-pressure column. The oxygen-enriched liquid removed from the high-pressure column and bottom liquid of the mass transfer column are mixed and partly evaporated in a condenser-evaporator. A liquid fifth fluid is removed from the mass transfer column between a feed point for the first fluid and a feed point for the oxygen-enriched liquid, and is at least partly fed into the low-pressure column.
    Type: Grant
    Filed: April 18, 2019
    Date of Patent: March 14, 2023
    Assignee: Linde Aktiengesellschaft
    Inventor: Dimitri Golubev
  • Publication number: 20230038170
    Abstract: The invention relates to a process for low-temperature separation of air, in which an air separation plant having a first rectification column and a second rectification column is used, the first rectification column being supplied with cooled compressed air and the second rectification column being supplied with liquid from the first rectification column or liquid formed herefrom. By means of a first condenser-evaporator, head gas of the first rectification column is condensed and liquid from the second rectification column or liquid formed herefrom is evaporated, thereby producing a first evaporation product. The invention also relates to a corresponding air separation plant.
    Type: Application
    Filed: March 5, 2021
    Publication date: February 9, 2023
    Inventor: Dimitri GOLUBEV
  • Publication number: 20220260312
    Abstract: A SPECTRA process for low-temperature fractionation of air, in which bottoms liquid from an additional second rectification column used to obtain oxygen is evaporated in a second condenser-evaporator. In this second condenser-evaporator, gas that has been evaporated beforehand in a first condenser-evaporator, which is used for condensation of tops gas from a first rectification column, is condensed at the pressure level of the previous evaporation. The invention likewise provides a corresponding plant.
    Type: Application
    Filed: November 24, 2020
    Publication date: August 18, 2022
    Inventors: Stefan LOCHNER, Dimitri GOLUBEV
  • Publication number: 20220228804
    Abstract: A method for low-temperature air separation, in which an air-separation system having a column system is used that has a first column, a second column, a third column, and a fourth column, wherein fluid from the first column is fed at least into the second column, fluid from the second column is fed at least into the third column, fluid from the third column is fed at least into the fourth column, and fluid from the fourth column is fed at least into the third column, and wherein the fluid fed from the third column into the fourth column includes at least a portion of a side flow, which is withdrawn from the third column and has a lower oxygen content and a higher argon content than the third sump liquid. The present invention also relates to a corresponding system.
    Type: Application
    Filed: May 6, 2020
    Publication date: July 21, 2022
    Inventor: Dimitri GOLUBEV
  • Publication number: 20220026145
    Abstract: A method for obtaining one or more air products, wherein an air separation system having a rectification column system is used, in which pressurized air is processed in an adjustable total air volume, wherein the total air volume is set to a first value during a first operating period and set to a second value that is different from the first value during a second operating period, and wherein the setting of the total air volume is changed from the first value to the second value in a third operating period from a first time to a second time. The second operating period is after the first operating period, the third operating period is between the first operating period and the second operating period. In the third operating period, a setting of a volume of a fluid, is changed from a third time up to a fourth time.
    Type: Application
    Filed: October 8, 2019
    Publication date: January 27, 2022
    Inventors: Dirk SCHWENK, Dimitri GOLUBEV
  • Publication number: 20210381762
    Abstract: A method for obtaining one or more air products by means of an air separation unit comprising a first booster, a second booster, a first decompression machine, and a rectification column system which has a high-pressure column operated at a first pressure level and a low-pressure column operated at a second pressure level below the first pressure level. All of the air supplied to the rectification column system is first compressed to a third pressure level, which lies at least 3 bar above the first pressure level, as a feed air quantity. A first fraction of the feed air quantity is supplied to a first booster at the third pressure level and at a temperature level of ?140 to ?70 ° C. and is compressed to a fourth pressure level using the first booster.
    Type: Application
    Filed: October 9, 2019
    Publication date: December 9, 2021
    Inventors: Dimitri GOLUBEV, Daniel Palaniswamy OTTE
  • Publication number: 20210381761
    Abstract: The invention relates to a method for a low-temperature air separation in which an air separation unit is used comprising a first rectification column and a second rectification column. The first rectification column is operated at a first pressure level, and the second rectification column is operated at a second pressure level below the first pressure level. Fluid which is oxygen-enriched compared to atmospheric air is drawn from the first rectification column in the form of one or more first material flows. At least one fraction of the fluid which has been drawn from the first rectification column in the form of the one or more first material flows is heated in a heat exchanger; a fraction of the fluid which has been heated in the heat exchanger is compressed using a compressor and is returned to the first rectification column.
    Type: Application
    Filed: October 22, 2019
    Publication date: December 9, 2021
    Inventors: Christian KUNZ, Stefan LOCHNER, Wolfgang HAAG, Lars KIRCHNER, Tobias LAUTENSCHLAGER, Dimitri GOLUBEV
  • Patent number: 11098950
    Abstract: The invention proposes a process and an air separation plant comprising a rectification column system comprising a high-pressure column, a low-pressure column, a main heat exchanger, and a main air compressor. The total air supplied to the rectification column system is compressed in the main air compressor to a first pressure level. The high-pressure column is operated at a second pressure level, at least 3 bar below the first pressure level. A gaseous, nitrogen-rich fluid is removed from the high-pressure column and warmed up in the gaseous state without prior liquefaction. A first partial quantity of the gaseous, nitrogen-rich fluid is warmed to a first temperature level of ?150 to ?100° C., supplied at this first temperature level to a booster and compressed further to a third pressure level. The first partial quantity is then warmed to a second temperature level and discharged from the air separation plant.
    Type: Grant
    Filed: June 1, 2018
    Date of Patent: August 24, 2021
    Assignee: LINDE AKTIENGESELLSCHAFT
    Inventor: Dimitri Golubev
  • Patent number: 10845118
    Abstract: A distillation column system and a plant are for production of oxygen by cryogenic fractionation of air. The distillation column system has a high-pressure column and a low-pressure column, a main condenser, and an argon column with an argon column top condenser. The low-pressure column comprises an upper mass transfer region, a lower mass transfer region and a middle mass transfer region. The argon column top condenser is arranged within the low-pressure column between the upper and middle mass transfer regions and is configured as a forced-flow evaporator.
    Type: Grant
    Filed: August 11, 2016
    Date of Patent: November 24, 2020
    Assignee: LINDE AKTIENGESELLSCHAFT
    Inventor: Dimitri Golubev
  • Patent number: 10488106
    Abstract: A method and apparatus for producing compressed nitrogen and liquid nitrogen. A separation system has a high-pressure column, a low-pressure column with a top condenser and a main condenser. Air is compressed in an air compressor, purified, cooled in a heat exchanger and introduced into the high-pressure column. A first part of the gaseous top nitrogen from the low-pressure column becomes compressed nitrogen product. A second part of the gaseous top nitrogen is condensed in the condensing space of the top condenser and vapor is drawn off as a residual gas stream. The vapor is expanded in a first expansion machine. A second compressed nitrogen stream from the top of the high-pressure column is expanded in a second expansion machine and then drawn off as compressed nitrogen product. A part of the nitrogen condensed in the top condenser is drawn off as liquid nitrogen product.
    Type: Grant
    Filed: July 7, 2017
    Date of Patent: November 26, 2019
    Assignee: LINDE AKTIENGESELLSCHAFT
    Inventor: Dimitri Golubev
  • Patent number: 10480853
    Abstract: A method and plant for the cryogenic separation of air, the plant having an air compressor, a heat exchanger and a distillation column system having a low-pressure column at a first pressure and a high-pressure column at a second pressure. Feed air is compressed in the air compressor to a third pressure at least 2 bar above the second pressure A first fraction of compressed feed air is cooled in the heat exchanger and expanded in a first expansion turbine. A second fraction is cooled in the heat exchanger and expanded in a second expansion turbine A third fraction is compressed to a fourth pressure, cooled in the heat exchanger and then expanded. The third fraction is compressed to the fourth pressure in sequence in a recompressor, a hot first turbine booster and a second turbine booster. A dense fluid expander is used to expand the third fraction.
    Type: Grant
    Filed: July 28, 2015
    Date of Patent: November 19, 2019
    Assignee: LINDE AKTIENGESELLSCHAFT
    Inventors: Tobias Lautenschlager, Dimitri Golubev
  • Patent number: 10458702
    Abstract: A method and device used to variably obtain a compressed-gas product by means low-temperature separation of air in a distillation column system. In a first operating mode, a first amount of first compressed-gas product is obtained, and, in a second operating mode, a second, smaller amount is obtained. In the first operating mode, a first amount of air is compressed in the main air compressor, and in the second operating mode, a second, larger amount is compressed in the main air compressor.
    Type: Grant
    Filed: June 25, 2015
    Date of Patent: October 29, 2019
    Assignee: LINDE AKTINGESELLSCHAFT
    Inventor: Dimitri Golubev