Abstract: Methods for determining a quantitative composition of a multi-component medium comprising at least two known immiscible components comprises determining temperature dependencies of specific heat capacity of each of the components. A sample of the multi-component medium is weighed. Specific heat capacity of the sample is determined at least at i?1 temperature levels, where i is the number of components of the multi-component medium. On the basis of the results from determination of specific heat capacity of the components and the temperature dependencies of specific heat capacity of the components, weight coefficients are calculated for each component of the medium. Quantitative content of each of the components of the multi-component medium is determined on the basis of the obtained values of the weight coefficients of the components.