Abstract: A process and apparatus for freeze drying of liquid material in a vessel in which the vessels are moved automatically through various stages including loading vessels onto racks, washing vessels in an inverted position, sterilizing vessels and racks, filling vessels with a liquid material, rotating the vessels and the liquid material contained within each vessel at a speed that allows the liquid to form a shell against the inner surface of the vessel, subjecting the vessels and the liquid material contained therein to freezing conditions sufficient to freeze the material into the form of a shell and then moving the rack and the vessels containing the frozen material through a vacuum drying chamber in which the frozen liquid material is dried.

Abstract: An apparatus for metering required proportions of different fluid ingredients to make a required mixture (e.g. a colored paint) includes a rack of storage containers for the ingredients, each provided with a valve-controlled outlet and a receiving container mounted on a weighing device which is presentable to a chosen sequence of storage containers in turn to receive the required contribution from each. Metering of the necessary ingredient additions is effected automatically by a valve actuator carried by the support for the weighing device. Data processing control to optimize operation is described.