Abstract: Embodiments of a method for increasing the lifetime of a casting slurry are described. One feature of the disclosed embodiments comprises processing refractory materials that are used to form casting slurries to provide a substantial increase in slurry lifetime for slurries made using such processed materials compared to slurries made using materials not processed as described herein. One embodiment of the method comprises heat processing at least one refractory powder. Without limiting the invention to a theory of operation, processing is continued for a period of time sufficient to reduce the amount of hydration from a first hydration level to a second hydration level. A slurry is formed using the refractory powder at a hydration level which provides an increased slurry lifetime relative to the same material without processing according to the disclosed embodiments.

Abstract: Embodiments of a method for increasing the lifetime of a casting slurry are described. One feature of the disclosed embodiments comprises processing refractory materials that are used to form casting slurries to provide a substantial increase in slurry lifetime for slurries made using such processed materials compared to slurries made using materials not processed as described herein. One embodiment of the method comprises heat processing at least one refractory powder. Without limiting the invention to a theory of operation, processing is continued for a period of time sufficient to reduce the amount of hydration from a first hydration level to a second hydration level. A slurry is formed using the refractory powder at a hydration level which provides an increased slurry lifetime relative to the same material without processing according to the disclosed embodiments.

Abstract: A molten metal or molten metal alloy is filtered to remove contaminants. Filters may include imaging agents, especially those useful for N-ray radiography, X-ray analysis, and neutron activation. Currently preferred imaging agents include gadolinia and tungsten. Currently preferred refractory materials include yttria, zirconia, tantalum, tungsten and rhenium. A homogeneous distribution of refractory and imaging materials may be accomplished by vacuum impregnation, chemical vapor deposition, physical vapor deposition, chemical vapor infiltration, fusing, cocalcining, alloying, and physical mixing. Filters substantially resistant to chemical and mechanical degradation may be used. For example, filters may be constructed with at least an outer layer of the filter comprising yttria. Filters may define a porosity and mesh size for efficient filtration and to exclude the maximum allowed size of defects for the particular application.

Abstract: Methods for increasing the lifetime of a casting slurry are described. One feature of the invention is processing refractory powders at a first hydration level to produce powders having a second, lower hydration level before the processed materials are used to form casting slurries. Processing according to the disclosed methods results in a substantial increase in the lifetime of a slurry made using such processed materials compared to slurries made using materials not processed as described herein. One embodiment of the method comprises heat processing at least one refractory powder, typically refractory powders which have undergone hydration subsequent to commercial production, for a period of time sufficient to reduce the amount of hydration from a first hydration level to a second hydration level. A slurry is formed using the refractory powder at an hydration level which provides an increased slurry lifetime relative to the same material without processing according to the method of the present invention.

Abstract: Investment casting shells, methods for their manufacture and methods for casting metals and alloys using such shells are disclosed. One feature of the shells is that the facecoat plus interior backup layers are purposefully designed to have substantially similar coefficients of thermal expansion to the seal dip layers. This helps reduce the occurrence of dimensional casting defects caused by differential thermal expansions of the layers comprising the shell. One embodiment of such a shell comprises a facecoat, plural interior backup layers and plural intermediate backup layers wherein at least one of the plural intermediate backup layers comprises a material capable of undergoing a volumetric transformation during cool down, and wherein the seal-dip layers have a coefficient of thermal expansion that varies from the coefficient of thermal expansion of the facecoat and interior backup layers by less than about 10 percent.

Abstract: Methods and compositions for forming shells for investment casting and methods for casting metal articles using the shells are described. One embodiment of the method comprises serially immersing a pattern in at least one, and perhaps several different slurries, each of which slurries comprises refractory material and from about 0 to about 30 volume percent inorganic binder. This forms a facecoat and plural refractory backup layers about the pattern, the facecoat and at least one backup layer defining a shell. The facecoat and/or the shell is then infiltrated with a binder. Infiltrating the shell with a binder is a key feature of the present invention. Infiltration refers to any process whereby a binder can be introduced into the facecoat and/or the subsequent layers built up about the shell.

Abstract: Time-stable yttria slurries, and a method for forming such yttria slurries and articles therefrom are described. The method involves forming an intimate mixture comprising yttria and at least about 0.1 weight percent of a dopant material. An aqueous slurry is then formed comprising from about 1 weight percent to about 95 weight percent of the intimate mixture. The intimate mixture may be formed by heating the mixture to a temperature sufficient to calcine the mixture. Alternatively, the intimate mixture may be formed by heating the mixture to a temperature sufficient to fuse the mixture. The dopant also may be provided as a surface coating on the yttria particles.