Patents by Inventor Douglas H. Adamson
Douglas H. Adamson has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Patent number: 11731143Abstract: A machine or apparatus featuring a first processor and a second processor. The first processor is configured to receive a mixture of fluid, valuable material and unwanted material and a functionalized polymer coated member configured to attach to the valuable material in an attachment rich environment, and provide an enriched functionalized polymer coated member having the valuable material attached thereto. The second processor is configured to receive a fluid and the enriched functionalized polymer coated member in a release rich environment to release the valuable material, and provide the valuable material released from the enriched functionalized polymer coated member.Type: GrantFiled: May 25, 2012Date of Patent: August 22, 2023Assignee: CiDRA CORPORATE SERVICES INC.Inventors: Paul J. Rothman, Mark R. Fernald, Francis K. Didden, Christian V. O'Keefe, Douglas H. Adamson
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Publication number: 20230257271Abstract: Systems and methods are provided that may utilize a glass substrate to selectively withdraw exfoliated graphene from a high-energy interface between immiscible solvents. The exfoliated graphene preferentially adheres to the surface of the glass substrate for withdrawal from the noted high energy interface, leaving behind the graphite (which is too large to be effectively adsorbed relative to the glass substrate). The disclosed systems and methods are easily implemented and offer significant advantages for graphene production relative to conventional systems and methods, e.g., the disclosed systems/methods do not require the input of heat or mechanical energy which translates to processes that are both cheaper to run and do not result in damage to the graphene. Still further, the disclosed systems/methods do not require chemical modification of the graphene, again lowering the cost considerably and not damaging the graphene structure.Type: ApplicationFiled: February 17, 2022Publication date: August 17, 2023Applicant: University of ConnecticutInventors: Douglas H. Adamson, Richard Parnas, Prabodha Abeykoon
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Publication number: 20230235186Abstract: The present disclosure provides advantageous sheet stabilized emulsion based inks, and improved methods for fabricating and using such inks. More particularly, the present disclosure provides improved methods for fabricating conductive inks derived from water-in-oil emulsions stabilized by sheets exfoliated from layered materials (e.g., substantially pristine and non-oxidized graphite or hexagonal boron nitride), and related methods of use. A layered material (e.g., substantially pristine and non-oxidized graphite or hexagonal boron nitride) can be exfoliated into individual sheets, and these sheets can be utilized to stabilize water-in-oil emulsions. In certain embodiments, by utilizing long chain alkanes (e.g., hexadecane), one can advantageously fabricate emulsions with high viscosity and stability. In this form, the emulsions can be used as inks, thereby advantageously providing an inexpensive route to printing electrically conducting and/or insulating lines and shapes.Type: ApplicationFiled: January 27, 2023Publication date: July 27, 2023Applicant: University of ConnecticutInventors: Douglas H. Adamson, Feiyang Chen, Elizabeth Brown
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Publication number: 20220194858Abstract: Porous, electrically conductive ceramic foams incorporating continuous self-assembled graphene networks are described. The disclosed approach uses interfacial trapping to spontaneously exfoliate and assemble pristine graphite, not graphite oxide, in a ceramic sol-gel. The composite foams display electrical conductivity and joule heating, with anticipated applications as, for example, catalyst supports, thermoelectrics, and porous electrodes.Type: ApplicationFiled: December 15, 2021Publication date: June 23, 2022Applicant: University of ConnecticutInventors: Douglas H. Adamson, Garrett Kraft
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Patent number: 11355259Abstract: The present disclosure provides advantageous graphene/graphite stabilized composites (e.g., graphene/graphite stabilized emulsion-templated foam composites), and improved methods for fabricating such graphene/graphite stabilized composites. More particularly, the present disclosure provides improved methods for fabricating pristine, graphene/graphite/polymer composite foams derived from emulsions stabilized by graphene/graphite kinetic trapping. In exemplary embodiments, the present disclosure provides that, instead of viewing the insolubility of pristine graphene/graphite as an obstacle to be overcome, it is utilized as a means to create or fabricate water/oil emulsions, with graphene/graphite stabilizing the spheres formed. These emulsions are then the frameworks used to make foam composites that have shown bulk conductivities up to about 2 S/m, as well as compressive moduli up to about 100 MPa and breaking strengths of over 1200 psi, with densities as low as about 0.25 g/cm3.Type: GrantFiled: October 8, 2020Date of Patent: June 7, 2022Assignee: University of ConnecticutInventors: Douglas H. Adamson, Steven Woltornist, Andrey V. Dobrynin
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Publication number: 20210379603Abstract: An engineered collection medium for use in mineral separation is described. The engineered collection medium has a solid phase body configured with a three-dimensional open-cell structure like foam or sponge to provide collection surfaces. The three-dimensional surface structure is made of a hydrophobic material which is a reaction product of isocyanate and polyol promotes the attraction of mineral particles to the collection surfaces as a hydrophobic foam. The hydrophobic foam can be in the form of a cube, sphere, or sheet and can be used in a filter or conveyor belt in a processor.Type: ApplicationFiled: February 7, 2019Publication date: December 9, 2021Inventors: Paul J. ROTHMAN, Mark R. FERNALD, Francis DIDDEN, Christian V. O'KEEFE, Douglas H. ADAMSON, Paul DOLAN, Timothy J. BAILEY, Michael Stephen RYAN, Weiguo HUANG, Kevin Rodney LASSILA, Michael D. COPPOLA, Allison K. GREENE
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Patent number: 11135597Abstract: A synthetic bead for use in mineral separation is described. The synthetic bead has a surface made of a synthetic material such as polymer and the synthetic material is functionalized with molecules having a functional group for attaching mineral particles to the surface in a separation process. The synthetic beads can be placed in flotation cell containing a mixture of water, valuable material and unwanted material or in a pipeline where the mixture is transported from one location to another. The enriched synthetic beads carrying the mineral particles are separated from the unwanted materials in the mixture. The mineral particles are then released from the synthetic beads by means of low pH treatment, ultrasonic agitation, thermal or electromagnetic treatment.Type: GrantFiled: April 12, 2018Date of Patent: October 5, 2021Assignee: CIDRA CORPORATE SERVICES LLCInventors: Paul J. Rothman, Mark R. Fernald, Francis K. Didden, Christian V. O'Keefe, Douglas H. Adamson
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Patent number: 11117141Abstract: Apparatus for use in, or forming part of, a separation process to be implemented in separation processor technology, the apparatus comprising synthetic bubbles or beads configured with a polymer or polymer-based material functionalized to attach to a valuable material in a mixture so as to form an enriched synthetic bubbles or beads having the valuable material attached thereto, and also configured to be separated from the mixture based at least partly on a difference in a physical property between the enriched synthetic bubbles or beads having the valuable material attached thereto and the mixture.Type: GrantFiled: October 26, 2017Date of Patent: September 14, 2021Assignee: CIDRA CORPORATE SERVICES INC.Inventors: Paul J. Rothman, Mark R. Fernald, Francis K. Didden, Christian V. O'Keefe, Alan D. Kersey, Douglas H. Adamson
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Patent number: 11004606Abstract: The present disclosure provides advantageous composite films/coatings, and improved methods for fabricating such composite films/coatings. More particularly, the present disclosure provides improved methods for fabricating composite films by trapping at least a portion of a layered material (e.g., hexagonal boron nitride sheets/layers) at an interface of a phase separated system and then introducing the layered material to a polymer film. The present disclosure provides for the use of boron nitride layers to increase the properties (e.g., dielectric constant and breakdown voltage) of polymer films. The exemplary films can be produced by an advantageous climbing technique. Exemplary boron nitride films are composed of overlapping boron nitride sheets with a total thickness of about one nanometer, with the film then transferred onto a polymer film, thereby resulting in significant increases in both dielectric and breakdown properties of the polymer film.Type: GrantFiled: July 17, 2018Date of Patent: May 11, 2021Assignee: University of ConnecticutInventors: Douglas H. Adamson, Zhenhua Cui, Andrey V. Dobrynin
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Publication number: 20210027907Abstract: The present disclosure provides advantageous graphene/graphite stabilized composites (e.g., graphene/graphite stabilized emulsion-templated foam composites), and improved methods for fabricating such graphene/graphite stabilized composites. More particularly, the present disclosure provides improved methods for fabricating pristine, graphene/graphite/polymer composite foams derived from emulsions stabilized by graphene/graphite kinetic trapping. In exemplary embodiments, the present disclosure provides that, instead of viewing the insolubility of pristine graphene/graphite as an obstacle to be overcome, it is utilized as a means to create or fabricate water/oil emulsions, with graphene/graphite stabilizing the spheres formed. These emulsions are then the frameworks used to make foam composites that have shown bulk conductivities up to about 2 S/m, as well as compressive moduli up to about 100 MPa and breaking strengths of over 1200 psi, with densities as low as about 0.25 g/cm3.Type: ApplicationFiled: October 8, 2020Publication date: January 28, 2021Applicant: University of ConnecticutInventors: Douglas H. Adamson, Steven Woltornist, Andrey V. Dobrynin
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Publication number: 20200407571Abstract: The present disclosure provides advantageous sheet stabilized emulsion based inks, and improved methods for fabricating and using such inks. More particularly, the present disclosure provides improved methods for fabricating conductive inks derived from water-in-oil emulsions stabilized by sheets exfoliated from layered materials (e.g., substantially pristine and non-oxidized graphite or hexagonal boron nitride), and related methods of use. A layered material (e.g., substantially pristine and non-oxidized graphite or hexagonal boron nitride) can be exfoliated into individual sheets, and these sheets can be utilized to stabilize water-in-oil emulsions. In certain embodiments, by utilizing long chain alkanes (e.g., hexadecane), one can advantageously fabricate emulsions with high viscosity and stability. In this form, the emulsions can be used as inks, thereby advantageously providing an inexpensive route to printing electrically conducting and/or insulating lines and shapes.Type: ApplicationFiled: October 31, 2018Publication date: December 31, 2020Applicant: University of ConnecticutInventors: Douglas H. Adamson, Feiyang Chen, Elizabeth Brown
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Patent number: 10835905Abstract: An engineered collection medium for use in mineral separation is described. The engineered collection medium has a solid phase body configured with a three-dimensional open-cell structure like foam or sponge to provide collection surfaces. The surfaces are functionalized with a hydrophobic chemical having molecules with a functional group for attaching mineral particles to the collection surfaces. The engineered collection medium can be a foam block, a filter or conveyor belt to be placed in a slurry to collect mineral particles in the slurry. The engineered collection medium carrying the mineral particles is provided to a release apparatus where the mineral particles can be released by using mechanical agitation, sonic agitation and so forth.Type: GrantFiled: January 9, 2017Date of Patent: November 17, 2020Assignee: CIDRA CORPORATE SERVICES INC.Inventors: Paul J. Rothman, Mark R. Fernald, Francis Didden, Christian V. O'Keefe, Douglas H. Adamson, Paul Dolan, Timothy J. Bailey, Michael Ryan
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Patent number: 10832828Abstract: The present disclosure provides advantageous graphene/graphite stabilized composites (e.g., graphene/graphite stabilized emulsion-templated foam composites), and improved methods for fabricating such graphene/graphite stabilized composites. More particularly, the present disclosure provides improved methods for fabricating pristine, graphene/graphite/polymer composite foams derived from emulsions stabilized by graphene/graphite kinetic trapping. In exemplary embodiments, the present disclosure provides that, instead of viewing the insolubility of pristine graphene/graphite as an obstacle to be overcome, it is utilized as a means to create or fabricate water/oil emulsions, with graphene/graphite stabilizing the spheres formed. These emulsions are then the frameworks used to make foam composites that have shown bulk conductivities up to about 2 S/m, as well as compressive moduli up to about 100 MPa and breaking strengths of over 1200 psi, with densities as low as about 0.25 g/cm3.Type: GrantFiled: March 2, 2017Date of Patent: November 10, 2020Assignee: University of ConnecticutInventors: Douglas H. Adamson, Steven Woltornist, Andrey V. Dobrynin
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Patent number: 10751693Abstract: Apparatus or recovering a mineral particle of interest from a slurry in a mineral extraction process, featuring a core or substrate; and multiple layers arranged on the core or substrate, each layer of the multiple layers configured with a respective outer surface having a plurality of molecules attached thereto, the molecules comprising a functional group selected for attracting and attaching one or more mineral particles of interest to the molecules. Each layer is made from a polymer having a thickness of less than or equal to about 125 microns. The polymer is selected from a group consisting of polydimethylsiloxane or dimethyl siloxane.Type: GrantFiled: June 1, 2015Date of Patent: August 25, 2020Assignee: CiDRA Corporate Service Inc.Inventors: Paul J. Rothman, Mark R. Fernald, Christian V. O'Keefe, Douglas H. Adamson
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Patent number: 10357782Abstract: Apparatus, such as a flotation separation device, features a flotation cell or column configured to receive a mixture of water, valuable material and unwanted material; receive polymer-based materials, including polymer bubbles or beads, configured to attach to the valuable material in the mixture; and provide enriched polymer-based materials, including enriched polymer bubbles or beads, having the valuable material attached thereon.Type: GrantFiled: May 25, 2012Date of Patent: July 23, 2019Assignee: CiDRA Corporate Services LLCInventors: Paul J. Rothman, Mark R. Fernald, Francis K. Didden, Christian V. O'Keefe, Alan D. Kersey, Douglas H. Adamson
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Publication number: 20190201914Abstract: A synthetic bead for use in mineral separation is described. The synthetic bead has a surface made of a synthetic material such as polymer and the synthetic material is functionalized with molecules having a functional group for attaching mineral particles to the surface in a separation process. The synthetic beads can be placed in flotation cell containing a mixture of water, valuable material and unwanted material or in a pipeline where the mixture is transported from one location to another. The enriched synthetic beads carrying the mineral particles are separated from the unwanted materials in the mixture. The mineral particles are then released from the synthetic beads by means of low pH treatment, ultrasonic agitation, thermal or electromagnetic treatment.Type: ApplicationFiled: April 12, 2018Publication date: July 4, 2019Inventors: Paul J. ROTHMAN, Mark R. FERNALD, Francis K. DIDDEN, Christian V. O'KEEFE, Douglas H. ADAMSON
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Patent number: 10266413Abstract: A method to fractionate and isolate components of oxidized graphene material is provided that includes fractionating a system that includes graphene oxide, a solvent and water, wherein the fractionation creates two phases or fractions: (i) a water phase or fraction that contains highly oxidized graphene oxide, and (ii) a solvent-in-water emulsion phase or fraction that contains a graphene-based material. The graphene-based material is recovered from the solvent-in-water phase or fraction. Fractionation of the solvent-in-water emulsion phase or fraction may be repeated. The graphene-based material (uGO) may be used in a range of applications, e.g., a medical device, a nanoelectronic, an electromechanical system, a sensor, a composite, a catalysis, and energy storage device, and an optics application.Type: GrantFiled: November 3, 2017Date of Patent: April 23, 2019Assignee: University of ConnecticutInventors: Douglas H. Adamson, Harish Kumar
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Patent number: 10245597Abstract: Apparatus is provided featuring a first and second cells. The first cell receives an ore slurry having mineral particles of interest, receives unexpanded polymer microspheres comprising a surface having mineral collector chemistry attached thereto with molecules for attaching the mineral particles of interest, causes the unexpanded polymer microspheres to expand substantially in volume into expanded polymer microspheres having a substantially increased sphere surface area, and provides an expanded polymer microsphere foam layer comprising the expanded polymer microspheres with attached mineral particles of interest. The second cell receives the expanded polymer microsphere foam layer, and causes the expanded polymer microspheres to collapse substantially in volume into collapsed polymer microspheres having a substantially reduced sphere surface area that results in a mechanical shearing off of the attached mineral particles of interest.Type: GrantFiled: April 1, 2013Date of Patent: April 2, 2019Assignee: CiDRA Corporate Services Inc.Inventors: Francis K. Didden, Alan D. Kersey, Michael A. Davis, Paul J. Rothman, Mark R. Fernald, Christian V. O'Keefe, Douglas H. Adamson
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Publication number: 20180323009Abstract: The present disclosure provides advantageous composite films/coatings, and improved methods for fabricating such composite films/coatings. More particularly, the present disclosure provides improved methods for fabricating composite films by trapping at least a portion of a layered material (e.g., hexagonal boron nitride sheets/layers) at an interface of a phase separated system and then introducing the layered material to a polymer film. The present disclosure provides for the use of boron nitride layers to increase the properties (e.g., dielectric constant and breakdown voltage) of polymer films. The exemplary films can be produced by an advantageous climbing technique. Exemplary boron nitride films are composed of overlapping boron nitride sheets with a total thickness of about one nanometer, with the film then transferred onto a polymer film, thereby resulting in significant increases in both dielectric and breakdown properties of the polymer film.Type: ApplicationFiled: July 17, 2018Publication date: November 8, 2018Applicant: University of ConnecticutInventors: Douglas H. Adamson, Zhenhua Cui, Andrey V. Dobrynin
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Patent number: 10060570Abstract: Apparatus, including a pipeline, featuring at least one pipe liner or coating configured to line or coat a pipe for receiving a process fluid flow, configured with at least one chemical taggant or tracer, and also configured to respond to the process fluid flow, and provide an indication about a degree of liner or coating wear or a location of wear in the pipe. The apparatus may also include the pipe having the at least one pipe liner or coating configured therein.Type: GrantFiled: January 9, 2014Date of Patent: August 28, 2018Assignee: CiDRA CORPORATE SERVICES, INC.Inventors: Alan D. Kersey, Michael Puig, Francis K. Didden, Douglas H. Adamson