Abstract: Devices and methods are provided to apply thin layers of antimicrobial coatings onto a wide variety of substrates and articles. The methods can be performed at moderate temperatures and pressures, allowing for the coating of sensitive substrates and articles.

Abstract: A method of fabricating a fully-dense three-dimensional metal article is disclosed. According to a first embodiment of the invention, the interior portion of the article is formed by way of selective laser sintering, in a cross-section of a layer of powder. After formation of the layer of powder, the laser is directed to form a gas-impervious skin around the interior portion of the article in that layer. The process is repeated, until the article is completed. The article surrounded by the skin is then subjected to hot isostatic pressing to densify the article; the skin, which serves as the "can" for the hot isostatic pressing, may or may not be removed from the article, as desired. According to a second embodiment of the invention, the can is formed first by way of laser generation, and is then filled with the metal powder, prior to hot isostatic pressing.

Abstract: A high temperature, high strength in-situ reinforced ceramic composite adapted for use in various applications including missile radomes in which microwave transparency is required in a high temperature environment. The material is manufactured by a pressureless sintering process, in which silicon nitride and barium aluminosilicate are blended together, isostatically pressed into a desired shape and thereafter sintered.

Abstract: A process for producing a green composite structure by isostatic compression and filtration. A suspension of colloidal size matrix powders is established in a carrier liquid. The suspension is incorporated into a die chamber having a filter opening containing a filter which is permeable to filtrate from the suspension under applied pressure but substantially impermeable to the matrix powders. An elevated pressure is isostatically imposed on the colloidal suspension within the die chamber. The pressure is maintained for a period of time to expel at least 20% of the liquid originally in the colloidal suspension through the filter opening. A specific die chamber comprises a rigid cage structure and an expandable bladder within the cage structure into which the colloidal suspension is introduced. The cage structure is disposed within a pressure vessel which can be initially evacuated to cause the bladder to conform to the cage structure and then pressurized with fluid for the isostatic compression procedure.

Abstract: A process for the production of reinforced refractory composite structures which may be of high density and shaped in desired three dimensional configurations. The shaped composite structures are produced by forming a suspension of particulate materials including a colloidal refractory power, colloidal sintering aid, and refractory reinforcement whiskers in a carrier liquid. The colloidal suspension is conformed to a desired configuration and brought into contact with a semipermeable membrane. A pressure is imposed on the suspension in the desired configuration to expel liquid from the suspension through the membrane to arrive at a green composite having a density of at least 40% of theoretical density. After drying, the green composite is then sintered under conditions to form an intergranular liquid phase in the composite providing further densification. A specific composite is a silicon carbide reinforced silicon nitride composite.