Abstract: A monitoring cell, used to perform a measurement in an NMR spectrometer of a reaction fluid produced by a reaction vessel, has a body having inlet and outlet transport coaxial capillaries for transporting the reaction fluid between the body and the reaction vessel. Cooling lines are also positioned coaxially with the transport capillaries to transport cooling liquid between the body and the reaction vessel. The cell further has a hollow sample probe for insertion into the NMR spectrometer and a coupler section that removably connects the sample probe to the body so that the inlet transport capillary extends through the body into the interior of the sample probe and the outlet transport capillary is sealed to the sample probe to allow reaction fluid that enters the sample probe via the inlet transport capillary to exit the sample probe via the outlet transport capillary.

Abstract: A monitoring cell, used to perform a measurement in an NMR spectrometer of a reaction fluid produced by a reaction vessel, has a body having inlet and outlet transport coaxial capillaries for transporting the reaction fluid between the body and the reaction vessel. Cooling lines are also positioned coaxially with the transport capillaries to transport cooling liquid between the body and the reaction vessel. The cell further has a hollow sample probe for insertion into the NMR spectrometer and a coupler section that removably connects the sample probe to the body so that the inlet transport capillary extends through the body into the interior of the sample probe and the outlet transport capillary is sealed to the sample probe to allow reaction fluid that enters the sample probe via the inlet transport capillary to exit the sample probe via the outlet transport capillary.

Abstract: Embodiments of the invention provide dry gaseous fluid pump apparatus comprising: a fluid inlet and a fluid outlet; at least one pump body having an internal wall defining an internal pump chamber thereof; a compression member provided within the pump chamber; and valve means being operable selectively to allow fluid to be drawn from the fluid inlet and into the pump chamber when at least a portion of the compression member is translated in a first direction and to be exhausted from the pump chamber through the fluid outlet when said at least a portion of the compression member is translated in a second direction opposite the first, the valve means being arranged to be actuated by actuator means under the control of control means to perform at least one selected from amongst the functions of allowing fluid to be drawn from the fluid inlet into the pump chamber and allowing fluid to be exhausted from the pump chamber through the fluid outlet, the apparatus comprising a linear drive assembly operable to drive t

Abstract: A monitoring cell, used to perform a measurement in an NMR spectrometer of a reaction fluid produced by a reaction vessel, has a body having inlet and outlet transport coaxial capillaries for transporting the reaction fluid between the body and the reaction vessel. Cooling lines are also positioned coaxially with the transport capillaries to transport cooling liquid between the body and the reaction vessel. The cell further has a hollow sample probe for insertion into the NMR spectrometer and a coupler section that removably connects the sample probe to the body so that the inlet transport capillary extends through the body into the interior of the sample probe and the outlet transport capillary is sealed to the sample probe to allow reaction fluid that enters the sample probe via the inlet transport capillary to exit the sample probe via the outlet transport capillary.

Abstract: Each NMR rotor bearing in an NMR magic angle spinning assembly is constructed of a porous ceramic material and has no inlet channels or nozzles. Instead, pressurized gas is forced through pores in the bearing ceramic material from an annular groove at the bearing periphery to the central aperture. Since the pores are small and very numerous, the gas pressure is effectively balanced around the periphery of the central aperture. In addition, if contaminants block one or more pores during operation, the pores are so numerous that the balanced pressure can still be maintained in the central aperture, thereby preventing an imbalance that could destroy the rotor.

Abstract: A monitoring cell, used to perform a measurement in an NMR spectrometer of a reaction fluid produced by a reaction vessel, has a body having inlet and outlet transport coaxial capillaries for transporting the reaction fluid between the body and the reaction vessel. Cooling lines are also positioned coaxially with the transport capillaries to transport cooling liquid between the body and the reaction vessel. The cell further has a hollow sample probe for insertion into the NMR spectrometer and a coupler section that removably connects the sample probe to the body so that the inlet transport capillary extends through the body into the interior of the sample probe and the outlet transport capillary is sealed to the sample probe to allow reaction fluid that enters the sample probe via the inlet transport capillary to exit the sample probe via the outlet transport capillary.

Abstract: A closed container having a single opening is sealed by a plug fabricated from a self-sealing elastomer. Before insertion, the plug is transfixed with a tube to allow air to escape as the plug is pushed into the container. The plug and tube are then inserted into a container. After the plug has been seated in the container, the tube is withdrawn, allowing the self-sealing elastomeric material to close the canal formed by the tube and to form a hermetic seal.

Abstract: Each NMR rotor bearing in an NMR magic angle spinning assembly is constructed of a porous ceramic material and has no inlet channels or nozzles. Instead, pressurized gas is forced through pores in the bearing ceramic material from an annular groove at the bearing periphery to the central aperture. Since the pores are small and very numerous, the gas pressure is effectively balanced around the periphery of the central aperture. In addition, if contaminants block one or more pores during operation, the pores are so numerous that the balanced pressure can still be maintained in the central aperture, thereby preventing an imbalance that could destroy the rotor.

Abstract: Apparatus for preventing energy leakage from a transmission line treats the line as a “partially closed” vessel. A gas stream with a pressure slightly different from ambient pressure is provided to the interior of the transmission line and a conduit that allows gas to pass between the transmission line and the ambient environment is provided. The gas flow rate at the conduit is then detected and monitored. If the flow rate falls outside a predetermined threshold, an electrical energy leakage is indicated. In another embodiment, the pressure of the input gas to the transmission line is continuously checked by a pressure switch, which will detect a change in pressure if the transmission integrity is compromised and disable the energy source.

Abstract: In a nuclear magnetic resonance probe, the sample coil is connected to the RF excitation source via transmission lines that are arranged to generate one or more nodal points at the 1H excitation frequency along their lengths and a balanced magnetic filed profile within the sample coil. Heat exchangers are then connected directly to the inner conductor of the transmission line at these nodal points. The transmission line inner conductors are in direct contact with the sample coil and efficiently cool the coil to cryogenic temperatures without interfering with the 1H resonance or RF profile.

Abstract: A multi-stage reciprocating vacuum pump includes first (2) and second (4) pump chambers located in the pump housing (1) and in which respective pistons (6, 8) reciprocate, first and second conduits (14, 20) for communicating, respectively outlet and suction (15, 16) sides of the first pump chamber (2) with the suction side (17) of the second pump chamber (4), and shut-off elements (18, 21; 25) associated with the first and second conduits (14, 20) for selectively communicating the first and second conduits (14, 20) with the suction side (17) of the second pump chamber (4); and the method of operating the pump includes manipulating the shut-off elements so that the first and second conduits (14, 20) are selectively connected to the suction side (17) of the second pump chamber (4).

Abstract: A valve arrangement for a vacuum pump includes a valve head displaceable substantially perpendicular to a flow direction of a fluid through the valve arrangement, a valve seat, and a valve spring for biasing the valve head into a flat abutment engagement with the valve seat, with the valve spring being formed of at least one substantially hollow body made of an elastomeric material.

Abstract: A multi-stage reciprocating vacuum pump includes first (2) and second (4) pump chambers located in the pump housing (1) and in which respective pistons (6, 8) reciprocate, first and second conduits (14, 20) for communicating, respectively outlet and suction (15, 16) sides of the first pump chamber (2) with the suction side (17) of the second pump chamber (4), and shut-off elements (18, 21; 25) associated with the first and second conduits (14, 20) for selectively communicating the first and second conduits (14, 20) with the suction side (17) of the second pump chamber (4); and the method of operating the pump includes manipulating the shut-off elements so that the first and second conduits (14, 20) are selectively connected to the suction side (17) of the second pump chamber (4).

Abstract: A valve arrangement for a vacuum pump includes a valve head displaceable substantially perpendicular to a flow direction of a fluid through the valve arrangement, a valve seat, and a valve spring for biasing the valve head into a flat abutment engagement with the valve seat, with the valve spring being formed of at least one substantially hollow body made of an elastomeric material.

Abstract: A multistage vacuum pump is achieved by utilizing a single piston and cylinder assembly having opposite end portions with substantially equal diameters and an enlarged diameter central portion. One end of the cylinder is closed by a valve and a first stage pumping chamber is defined between the valve and the piston. The enlarged diameter portion of the piston has an axial extent less than the axial extent of the enlarged diameter portion of the cylinder to define second and third stage pumping chambers on opposite sides of the enlarged diameter portion of the piston. The three pumping chambers are interconnected by passage means to an inlet and outlet to provide a sequential reduction in pressure. A single drive unit may be connected to a plurality of pumping units for reciprocating the piston in each pumping unit.

Abstract: A multistage vacuum pump is achieved by utilizing a single piston and cylinder assembly having opposite end portions with substantially equal diameters and an enlarged diameter central portion. One end of the cylinder is closed by a valve and a first stage pumping chamber is defined between the valve and the piston. The enlarged diameter portion of the piston has an axial extent less than the axial extent of the enlarged diameter portion of the cylinder to define second and third stage pumping chambers on opposite sides of the enlarged diameter portion of the piston. The three pumping chambers are interconnected by passage means to an inlet and outlet to provide a sequential reduction in pressure. A single drive unit may be connected to a plurality of pumping units for reciprocating the piston in each pumping unit.

Abstract: A vacuum pump includes two pairs of piston and cylinder assemblies mounted on opposite sides of a crankshaft in a common plane with the gas inlets for the first and second cylinders of a first pair of piston and cylinder assemblies being connected to the device to be evacuated and the gas outlets thereof being connected to a common outlet having a spring biased one-way valve controlling the outlet and to a passage connected to the inlet of a third cylinder in said second pair of piston and cylinder assemblies. The gas outlet of the third cylinder is connected to the inlet of the fourth cylinder and the gas outlet of the fourth cylinder is connected to the common outlet through spring biased one-way valves.

Abstract: A reciprocatory piston and cylinder machine particularly suitable for use as a vacuum pump includes a cylinder (17), a cylindrical piston (16) relatively slidably reciprocable within the cylinder (17), and means for substantially sealing the annular space between the piston (16) and cylinder (17) in lieu of oil or other liquid lubricant. The sealing means comprises a sleeve (102) of a low-friction material disposed under circumferential tension, and preferably also under longitudinal tension, on the cylindrical surface of the piston (16). Also disclosed is a reciprocatory piston and cylinder machine of particular prior construction having a one-way valve (42) in an exhaust port (30) ahead of a head portion (24) of the piston (16). The arrangement is such that, as the front face of the piston head portion (24) approaches the closed cylinder end (52), the piston head portion 24 physically moves the one-way valve (42) so as to open the exhaust port (30).

Abstract: A reciprocatory piston and cylinder machine particularly suitable for use as a vacuum pump includes a cylinder (17), a cylindrical piston (16) relatively slidably reciprocable within the cylinder (17), and means for substantially sealing the annular space between the piston (16) and cylinder (17) in lieu of oil or other liquid lubricant. The sealing means comprises a sleeve (102) of a low-friction material disposed under circumferential tension, and preferably also under longitudinal tension, on the cylindrical surface of the piston (16). Also disclosed is a reciprocatory differential piston and cylinder machine of particular prior construction having a one-way valve (42) in an exhaust port (30) ahead of a head portion (24) of the piston (16). The arrangement is such that, as the front face (28) of the piston head portion (24) approaches the cylinder end face (52), the front face (28) physically moves the one-way valve (42) so as to open the exhaust port (30).

Abstract: A porting and ducting arrangement for a pair of adjacent hollow cylinders includes respective pluralities of passages extending longitudinally in the walls of the cylinders. Each passage is provided with a port in communication with the interior of the associated cylinder. Plural recesses in the end of the cylinders or in a cover are each in communication with a separate passage or group of passages when the cover is applied to the cylinders. There are a pair of such recesses thereby associated with each cylinder and at least one recess of each pair is in communication with a recess of the other pair via duct means in the cover. Gasket means is retained between the cylinders and the cover to seal each recess of each pair of recesses with respect to the other recess of the pair.