Patents by Inventor Ehrfried Parr
Ehrfried Parr has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Patent number: 4620399Abstract: According to the invention there are produced sodium Zeolite A granulates having the following parameters:______________________________________ Adsorption Data: (p/po = 0.8, 20.degree. C.) ______________________________________ H.sub.2 O > 22.0% NH.sub.3 > 11.0% CO.sub.2 .ltoreq. 0.1% O.sub.2 .ltoreq. 0.1% N.sub.2 .ltoreq. 0.1% Ar .ltoreq. 0.1% CH.sub.3 OH .ltoreq. 0.2% CH.sub.3 --CH.sub.2 --OH .ltoreq. 0.2% ______________________________________The zeolite granulate is produced by having zeolite A powder present in a mixer, adding alkali silicate solution, mixing until there are obtained zeolite granulates having a particle size of at least 0.1 mm, in a given case post-rolling the granulates, first drying the moist zeolite granulates with air in a fluidized bed drier at a temperature of 20.degree. to 39.degree. C., during which the carbon dioxide content of the drying air is adjusted to less than 200 ppm, subsequently drying in a second drying step at a temperature of 40.degree.-120.degree. C.Type: GrantFiled: May 28, 1985Date of Patent: November 4, 1986Assignee: DeGussa AGInventors: Hans Strack, Peter Kleinschmit, Ehrfried Parr
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Patent number: 4551322Abstract: There are produced crystalline zeolite powders of Type A with the composition1.0.+-.0.2 M.sub.2/n O:Al.sub.2 O.sub.3 :1.85.+-.0.5 SiO.sub.2.y H.sub.2 Owhere M is a metal cation, n is its valence and y has a value up to 6 with 50 weight % of the particles not over 4.9.mu. and with a particle spectrum______________________________________ Fraction (.mu.) Portion (weight %) ______________________________________ <3 10 to 60 <5 55 to 95 <10 93 to 99 <15 96 to 100 ______________________________________by hydrothermally crystallizing a SiO.sub.2, Al.sub.2 O.sub.3, Na.sub.2 O and water containing alkali aluminate, water, silicate synthesis mixture with an optional tempering step wherein in a given case during the crystallization or tempering step instead of stirring shearing forces are employed. The process comprises mixing with stirring (1) an aqueous alkali silicate solution and (2) an aqueous sodium hydroxide with a NaOH content of 0.Type: GrantFiled: March 14, 1983Date of Patent: November 5, 1985Assignees: Degussa Aktiengesellschaft, Henkel Kommandelgesellschaft auf AktienInventors: Hans Strack, Wolfgang Roebke, Dieter Kneitel, Ehrfried Parr
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Patent number: 4542115Abstract: According to the invention there are produced sodium Zeolite A granulates having the following parameters:______________________________________ Adsorption Data: (p/po = 0.8, 20.degree. C.) ______________________________________ H.sub.2 O >22.0% NH.sub.3 >11.0% CO.sub.2 .ltoreq.0.1% O.sub.2 .ltoreq.0.1% N.sub.2 .ltoreq.0.1% Ar .ltoreq.0.1% CH.sub.3 OH .ltoreq.0.2% CH.sub.3 --CH.sub.2 --OH .ltoreq.0.2% ______________________________________The zeolite granulate is produced by having zeolite A powder present in a mixer, adding alkali silicate solution, mixing until there are obtained zeolite granulates having a particle size of at least 0.1 mm, in a given case post-rolling the granulates, first drying the moist zeolite granulates with air in a fluidized bed drier at a temperature of 20.degree. to 39.degree. C., during which the carbon dioxide content of the drying air is adjusted to less than 200 ppm, subsequently drying in a second drying step at a temperature of 40.degree.-120.degree. C.Type: GrantFiled: August 9, 1982Date of Patent: September 17, 1985Assignee: Degussa AktiengesellschaftInventors: Hans Strack, Peter Kleinschmit, Ehrfried Parr
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Patent number: 4305916Abstract: There are produced crystalline zeolite powders of Type A with the composition1.0.+-.0.2M.sub.2/n O:Al.sub.2 O.sub.3 :1.85.+-.0.5SiO.sub.2.yH.sub.2 Owhere M is a metal cation, n is it valence and y has a value up to 6 with 50 weight % of the particles not over 4.3.mu. and with a particle spectrum:______________________________________ Fraction (.mu.) Portion (weight %) ______________________________________ <3 18 to 38 <5 70 to 82 <10 93 to 99 <15 96 to 100 ______________________________________by hydrothermally crystallizing a SiO.sub.2, Al.sub.2 O.sub.3, Na.sub.2 O and water containing alkali aluminate, water, silicate synthesis mixture with an optional tempering step wherein in a given case during the crystallization or tempering step instead of stirring shearing forces are employed. The process comprises providing an aqueous alkali aluminate liquor having a temperature of 30.degree. to 100.degree. C. and containing 0.1 to 100 grams of Al.sub.2 O.sub.3 /l and 1 to 200 grams of Na.sub.Type: GrantFiled: October 27, 1977Date of Patent: December 15, 1981Assignee: Degussa & Henkel Kommanditgesellschaft Auf AktienInventors: Hans Strack, Wolfgang Roebke, Dieter Kneitel, Ehrfried Parr
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Patent number: 4303626Abstract: There are produced crystalline zeolite powders of Type A with the composition1.0.+-.0.2 M.sub.2/n O:Al.sub.2 O.sub.3 :1.85.+-.0.5 SiO.sub.2 .multidot.y H.sub.2 Owhere M is a metal cation, n is its valence and y has a value up to 6 with 50 weight % of the particles not over 6.2.mu. and with a particle spectrum:______________________________________ Fraction (.mu.) Portion (weight %) ______________________________________ <3 10 to 60 <5 25 to 95 <10 80 to 99 <15 92 to 100 ______________________________________by hydrothermally crystallizing a SiO.sub.2, Al.sub.2 O.sub.3, Na.sub.2 O and water containing alkali aluminate, water, silicate synthesis mixture with an optional tempering step wherein in a given case during the crystallization or tempering step instead of stirring shearing forces are employed. The process comprises providing an aqueous alkali aluminate liquor having a temperature of 50.degree. to 90.degree. C. and containing 0.1 to 100 grams of Al.sub.2 O.sub.3 /l and 1 to 200 grams of Na.Type: GrantFiled: October 27, 1977Date of Patent: December 1, 1981Assignee: Degussa & Henkel Kommanditgesellschaft auf AktienInventors: Hans Strack, Wolfgang Roebke, Dieter Kneitel, Ehrfried Parr
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Patent number: 4303629Abstract: There are produced crystalline zeolite powders of Type A with the composition 1.0.+-.0.2 M.sub.2/n O:Al.sub.2 O.sub.3 :1.85.+-.0.5 SiO.sub.2 .multidot.y H.sub.2 O where M is a metal cation, n is its valence and y has a value up to 6 with 50 weight % of the particles not over 4.0.mu. and with a particle spectrum______________________________________ Fraction (.mu.) Portion (weight %) ______________________________________ <3 35 to 60 <5 82 to 95 <10 93 to 99 <15 96 to 100 ______________________________________by hydrothermally crystallizing a SiO.sub.2, Al.sub.2 O.sub.3, Na.sub.2 O and water containing alkali aluminate, water, silicate synthesis mixture with optionally a tempering step wherein in a given case during the crystallization or tempering step instead of stirring shearing forces are employed. The process comprises providing an aqueous alkali silicate soluton, heating it to a temperature between 30.degree. and 80.degree. C.Type: GrantFiled: October 27, 1977Date of Patent: December 1, 1981Assignee: Degussa & Henkel Kommanditgesellschaft auf AktienInventors: Hans Strack, Wolfgang Roebke, Dieter Kneitel, Ehrfried Parr
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Patent number: 4303627Abstract: There are produced crystalline zeolite powders of Type A with the composition 1.0.+-.0.2 M.sub.2/n O:Al.sub.2 O.sub.3 :1.85.+-.0.5 SiO.sub.2 .multidot.y H.sub.2 O where M is a metal cation, n is its valence and y has a value up to 6 with 50 weight % of the particles not over 5.9.mu. and with a particle spectrum______________________________________ Fraction (.mu.) Portion (weight %) ______________________________________ <3 15 to 25 <5 35 to 55 <10 80 to 94 <15 96 to 100 ______________________________________by hydrothermally crystallizing a SiO.sub.2, Al.sub.2 O.sub.3, Na.sub.2 O and water containing alkali aluminate, water, silicate synthesis mixture with an optional tempering step wherein in a given case during the crystallization or tempering step instead of stirring shearing forces are employed. The process comprises providing water in a container, simultaneously feeding into the water at a temperature of 30.degree. to 100.degree. C.Type: GrantFiled: October 27, 1977Date of Patent: December 1, 1981Assignee: Degussa & Henkel Kommanditgesellschaft auf AktienInventors: Hans Strack, Wolfgang Roebke, Dieter Kneitel, Ehrfried Parr
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Patent number: 4303628Abstract: There are produced crystalline zeolite powders of Type A with the composition1.0.+-.0.2 M.sub.2/n O:Al.sub.2 O.sub.3 :1.85.+-.0.5 SiO.sub.2 .multidot.y H.sub.2 Owhere M is a metal cation, n is its valence and y has a value up to 6 with 50 weight % of the particles not over 4.9.mu. and with a particle spectrum______________________________________ Fraction (.mu.) Portion (weight %) ______________________________________ <3 10 to 60 <5 55 to 95 <10 93 to 99 <15 96 to 100 ______________________________________by hydrothermally crystallizing a SiO.sub.2, Al.sub.2 O.sub.3, Na.sub.2 O and water containing alkali aluminate, water, silicate synthesis mixture with an optional tempering step wherein in a given case during the crystallization or tempering step instead of stirring shearing forces are employed. The process comprises mixing with stirring (1) an aqueous alkali silicate solution and (2) an aqueous sodium hydroxide with a NaOH content of 0.Type: GrantFiled: October 27, 1977Date of Patent: December 1, 1981Assignee: Degussa & Henkel Kommanditgesellschaft auf AktienInventors: Hans Strack, Wolfgang Roebke, Dieter Kneitel, Ehrfried Parr