Abstract: An automatic feedback control system for a water treatment apparatus, such as a recirculating solids contact clarifier, that maintains steady-state operation of the clarifier by accurately measuring the concentration of suspended solids at designated portions of the clarifier and automatically adjusting clarifier variables to maintain optimum conditions despite changes in the inlet flow rate, composition or temperature.

Abstract: The invention provides a method for removing metal oxides and colloidal material from high-resistivity water streams at a relatively high removal efficiency. The method includes hydrating a highly ionized dual morphology ion exchange resin in a macroreticular, desiccated morphology to produce a macroreticular, hydrated morphology. A water stream which is brought into contact with the resin is purified. The water stream may, optionally, also be contacted with both a cation exchange resin and an anion exchange resin.The invention additionally provides a method for selecting ion exchange resins which are particularly suited for use in removing metal oxides from a condensate stream. The method serves to narrow the field of candidates for pilot-scale resin testing with industrial water streams.

Abstract: The invention provides a method for removing metal oxides and colloidal material from high-resistivity water streams at a relatively high removal efficiency. The method includes hydrating a highly ionized dual morphology ion exchange resin in a macroreticular, desiccated morphology to produce a macroreticular, hydrated morphology. A water stream which is brought into contact with the resin is purified. The water stream may, optionally, also be contacted with both a cation exchange resin and an anion exchange resin.The invention additionally provides a method for selecting ion exchange resins which are particularly suited for use in removing metal oxides from a condensate stream. The method serves to narrow the field of candidates for pilot-scale resin testing with industrial water streams.

Abstract: The invention provides a method for separating metallic corrosion products from a water stream. A filter conditioned with a relatively small amount of ion exchange material exhibits comparatively low pressure differential while processing a water stream at commercially desirable flow rates and retention efficiencies. The method permits longer filter runs with a minimal application of material on the filtration surface. The invention additionally provides a filter for separating metallic corrosion products having a relatively broad range of particle sizes from a water stream.

Abstract: A baffle system is described that significantly reduces media loss caused by turbulence encountered during gas and liquid backwashing of a discrete media filter bed. When positioned about a filter collection trough or outlet, the baffle system deflects rising gas bubbles away from the collection trough and disengages filter media from the backwash liquid.

Abstract: The invention provides a method for removing transition metal oxides and soluble cation species from condensate at a relatively high removal efficiency. The method includes hydrating a strongly acidic dual morphology cation exchange resin in a macroeticular, desiccated morphology to produce a macroreticular, hydrated morphology. Condensate which is brought into contact with the resin when it is in a hydrogen form is purified. The condensate may, optionally, also be contacted with an anion exchange resin.The invention additionally provides a method for selecting cation exchange resins which are particularly suited for use in removing metal oxides from a condensate stream. The method serves to narrow the field of condidates for pilot-scale resin testing with industrial condensate.

Abstract: Methods for treating aqueous solutions and for recovering specific chemical products from an aqueous solution by ion exchange or adsorption by passing the aqueous solution through a regenerable filter bed comprising a flocculated mixture of finely divided active particulate material and filter aid materials having a depth of from about 3.0 inches to about 60 inches.

Abstract: A deaerator device for separating non-condensable gases from condensate. The device includes an upper deaerator stage means comprising a spray nozzle assembly which directs liquid particles under high velocity into a hood located thereabove. In the hood, the particles are raised to their saturation temperature by steam introduced into the device wherein the non-condensable gases are liberated from the condensate and vented to the atmosphere. Located below the nozzles is tray for receiving the condensed water. The tray has a plurality of openings which directs condensate into a lower deaerator stage consisting of a packing which removes substantially all of the non-condensable gases left in the condensate.

Abstract: A layer of precoat filter aid material including powdered activated carbon removes oxygen and impurities from a liquid having hydrazine added thereto. Oxygen concentrations may be reduced to parts per billion concentrations. Suspended solids can be removed by the precoat layer, and if the precoat layer includes an active particulate material, either as a component of the precoat layer or as an underlayer, the concentration of impurities and dissolved solids in the liquid can also be reduced.

Abstract: A method and apparatus is provided for holding first material along with less dense material in substantially separate layers and for effecting removal of at least some of the second material to a location displaced from the layer. The materials are arranged in the two layers with the first material at the bottom of a vessel and with the second material disposed above the first material. An elongate withdrawal conduit projects into the vessel to define (1) an exit port at the wall of the vessel, (2) a confined flow passageway communicating with the exit port within the vessel, and (3) at least one withdrawal aperture with the uppermost portion of any withdrawal aperture being lower than the uppermost portion of the exit port. The upper surface of the first material layer is maintained below the conduit while flow of the second material from the second material layer is effected into and through the conduit via the withdrawal aperture.

Abstract: A method for treating a sugar syrup to neutralize, decolorize and decalcify the sugar syrup during the clarification and decolorization process of sugar refining comprises contacting a sugar syrup with a neutralizing precoat filter layer disposed on a porous support means. The precoat filter layer comprises a liquid slurry constituted by an aqueous suspension of fibrous filter aid material and a neutralizing amount of particulate, crystalline alumino-siliate molecular sieve having an average particle size of less than 10 microns.

Abstract: A method for treating aqueous solutions by ion exchange uses a weakly acidic cation exchange resin to remove ammonia and other volatile amines along with corrosion products and metal ion leakage from a solution while substantially reducing the quantity of acid required to regenerate the cation exchange resin. The solution can be passed through a conventional mixed bed comprising a strongly acidic cation exchange resin and a strongly basic anion exchange resin after the pretreatment.

Abstract: The present invention relates to a method for purifying aqueous solutions or condensate in a three component resin system comprising a mixed bed of a strongly basic anion exchange resin, a strongly acidic cation exchange resin and a weakly acidic cation exchange resin. According to the present method, aqueous solutions can be treated to remove metal ions and corrosion products along with ammonia and other volatile amines so that metal ion leakage is substantially reduced and the run length of the resin system is increased. A method for separating and isolating the resins of the three component system is also described.

Abstract: A method for treating aqueous solutions by ion exchange uses a weakly acidic cation exchange resin and a strongly basic anion exchange resin to remove ammonia and other volatile amines along with corrosion products and metal ion leakage from a solution while substantially reducing the quantity of acid required to regenerate the cation exchange resin.

Abstract: A method for treating aqueous solutions by ion exchange uses a weakly acidic cation exchange resin and a strongly basic anion exchange resin to remove corrosion products and metal ion leakage from a solution while substantially reducing the quantity of acid required to regenerate the cation exchange resin. Substantial quantities of ammonia and other volatile amines are not removed from the solution during the treatment process.

Abstract: A method for regenerating the exhausted anion and cation exchange resins in a mixed bed demineralizer which utilizes an inert material of a specific density intermediate to the specific densities of the anion and cation resins. The inert resin remains in the regeneration system and is not returned to the service vessel with the regenerated resin.

Abstract: A process for scrubbing undissolved impurities from the upper portion of an ion exchange resin filtration bed is disclosed wherein air is introduced in the upper portion of the bed and develops a pressure within the vessel. This pressure subsequently forces rinse water down through the upper portion of the bed and out of the vessel. The gas is introduced into the bed and the water is drained therefrom at a level below the bed's upper surface but above a substantial lower portion of the resin bed. In this manner, lesser quantities of scrubbing fluids are required and the majority of the resin material is left undisturbed to maintain maximum ion exchange capacity.

Abstract: The invention relates to a method for converting strong-base anion exchange resins from the monovalent anion form to the hydroxide form. A .?.solution.!. .Iadd.source .Iaddend.of polyvalent anions is first passed through the resin to displace the monovalent anions. A solution of alkali metal hydroxide is then passed through the resin to convert it to the hydroxide form, and to produce an effluent solution of hydroxide ions and polyvalent anions. This effluent solution is then neutralized with an acid containing .Iadd.a source of .Iaddend.polyvalent anions, and the neutralized solution is passed through a second batch of resin in the monovalent anion form. In the preferred embodiment, a portion of the effluent is retained without neutralization and is delivered to the second batch of resin after the neutralized effluent to perform a portion of the hydroxide regeneration.