Patents by Inventor Emmerich Pastorek

Emmerich Pastorek has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 5169990
    Abstract: In the production of 9,9-bis-(4-hydroxphenyl)-fluorene by condensation by fluorenone and phenol in a molar ratio of 1:4 to 1:8 at 30.degree. to 90.degree. C. in the presence of gaseous hydrogen chloride and .beta.-mercapto-propionic acid as catalyst, the improvement comprising mixing the completed reaction mixture with a polyalkylene glycol, distilling excess phenol from the mixture, and mixing the distillation residue with a solvent miscible with the polyalkylene glycol, recovering the crystallized product, suspending the crystallized product in water and heating the suspension to obtain highly pure 9,9-bis-(4-hydroxyphenyl)-fluorene as white crystals.
    Type: Grant
    Filed: February 11, 1992
    Date of Patent: December 8, 1992
    Assignee: Rutgerswerke Aktiengesellschaft
    Inventors: Winfried Orth, Emmerich Pastorek, Wolfgang Weiss, Hans W. Kleffner
  • Patent number: 5149886
    Abstract: In a process for the preparation of 9,9-bis-(4-hydroxyphenyl)-fluorene by condensing fluorenone and phenol in a molar ratio of 1:4 to 1:8 at 30.degree. to 90.degree. C. in the presence of gaseous hydrogen chloride and .beta.-mercapto-propionic acid catalyst, the improvement comprising distilling water of reaction and dissolved hydrochloric acid from the completed reaction mixture, dissolving the distillation residue in a nitrile, separating the crystallized adduct of nitrile and 9,9-bis-(4-hydroxphenyl)- fluorene from the nitrile and optionally dissociating the adduct to recover high purity 9,9-bis-(4-hydroxphenyl)- fluorene.
    Type: Grant
    Filed: February 11, 1992
    Date of Patent: September 22, 1992
    Assignee: Rutgerswerke AG
    Inventors: Winfried Orth, Emmerich Pastorek, Wolfgang Weiss, Hans W. Kleffner
  • Patent number: 5066806
    Abstract: A process for the recovery of isomeric pure 7-chloro-quinaldine from isomeric mixtures of chloro-quinaldines comprising dissolving the isomeric mixture of chloro-quinaldines in an organic solvent, adding an aqueous tartaric acid solution to the organic solution to form the tartrate of 7-chloro-quinaldine in crystalline form, recovering the crystals and treating the same with a base to obtain 7-chloro-quinaldine.
    Type: Grant
    Filed: August 13, 1990
    Date of Patent: November 19, 1991
    Assignee: Rutgerswerke AG
    Inventors: Emmerich Pastorek, Winfried Orth, Wolfgang Weiss, Hans W. Kleffner
  • Patent number: 4582910
    Abstract: A method for the preparation of 4-halogenonaphthalic acid anhydrides by halogenation of an aqueous solution of an alkali salt of the naphthalic acid with halogen or alkali metal hypohalogenite wherein a solution of the alkali metal salt of the naphthalic acid is treated with a water soluble magnesium salt and at least an equal molar amount of an alkakli metal hydroxide, halogenating this reaction mixture at a temperature in the range of 10.degree. to 25.degree. C. and subsequently acidifying the reaction mixture. In a second embodiment of the invention, an aqueous solution of alkali metal carbonate is used in place of the magnesium salt and alkali metal hydroxide.
    Type: Grant
    Filed: February 19, 1985
    Date of Patent: April 15, 1986
    Assignee: Rutgerswerke Aktiengesellschaft
    Inventors: Winfried Orth, Emmerich Pastorek, Werner Fickert
  • Patent number: 4564700
    Abstract: An improved process for the preparation of fluorene-9-carboxylic acid comprising reacting fluorene and a dialkyl carbonate with alkyls of 1 to 5 carbon atoms in the presence of a member of the group consisting of alkali metal hydrides or potassium alcoholate of an aliphatic alcohol of 1 to 5 carbon atoms, neutralizing the mixture and saponifying the resulting fluorene-9-carboxylic acid ester to obtain fluorene-9-carboxylic acid in good yields.
    Type: Grant
    Filed: November 16, 1983
    Date of Patent: January 14, 1986
    Assignee: Rutgerswerke Aktiengesellschaft
    Inventors: Winfried Orth, Emmerich Pastorek, Werner Fickert
  • Patent number: 4549024
    Abstract: A novel process for the preparation of quinolinic acid comprising reacting quinoline in an aqueous acid with hydrogen peroxide in the presence of at least one cation selected from the group consisting of vanadyl V, cobalt III, titanyl IV and osmium VIII cations at 50.degree. to 100.degree. C. and then oxidizing with chlorite or chlorate ions to form quinolinic acid.
    Type: Grant
    Filed: November 5, 1984
    Date of Patent: October 22, 1985
    Assignee: Rutgerswerke Aktiengesellschaft
    Inventors: Winfried Orth, Emmerich Pastorek, Werner Fickert
  • Patent number: 4510090
    Abstract: Improvement of the yield and purity of phenanthrenequinone during its production by oxidation of phenanthrene by means of chromic acid in a sulfuric acidic medium is achieved by preparing a dispersion made up of phenanthrene, alkali dichromate and water at 95.degree.-100.degree. C., cooling said dispersion down to 80.degree.-85.degree. C. and carrying out the oxidation reaction under cooling and portion-wise addition of concentrated sulfuric acid in a temperature range between 80.degree. and 85.degree. C.
    Type: Grant
    Filed: January 30, 1984
    Date of Patent: April 9, 1985
    Assignee: Rutgerswerke Aktiengesellschaft
    Inventors: Dietrich Tonnius, Wolfgang Weiss, Winfried Orth, Heinrich Miele, Emmerich Pastorek
  • Patent number: 4228083
    Abstract: An improved process for the production of .beta.-(5-nitro-2-furyl)-acrolein by reacting 5-nitro-furfural and acetaldehyde in the presence of a secondary amine, the improvement comprises effecting the reaction in an aliphatic carboxylic acid of 2 to 4 carbon atoms.
    Type: Grant
    Filed: November 8, 1979
    Date of Patent: October 14, 1980
    Assignee: Rutgerswerke Aktiengesellschaft
    Inventors: Emmerich Pastorek, Winfried Orth, Werner Fickert