Patents by Inventor Eugene E. Spala

Eugene E. Spala has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).

  • Patent number: 9434906
    Abstract: Disclosed herein are marine diesel engine lubricating oil compositions which comprises (a) a major amount of an oil of lubricating viscosity, and (b) about 3 wt. % to about 40 wt. %, based on the total weight of the marine diesel engine lubricating oil composition, of a sulfurized, alkaline earth metal alkylphenate detergent which is substantially free of polyol promoter oxidation products.
    Type: Grant
    Filed: March 25, 2013
    Date of Patent: September 6, 2016
    Assignees: Chevron Oronite Company, LLC, Chevron Oronite Technology B.V.
    Inventors: Ronald Theodorus Fake Jukes, Eugene E. Spala
  • Patent number: 9062271
    Abstract: Disclosed herein is an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition, which is prepared by the process comprising (a) providing an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition having a total base number (TBN) greater than about 250; and (b) sparging the overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition with air at a temperature ranging from about 190° C. to about 250° C.
    Type: Grant
    Filed: October 30, 2013
    Date of Patent: June 23, 2015
    Assignees: Chevron Oronite Technology B.V., Chervon Oronite Company LLC
    Inventors: Ronald T. F. Jukes, Eugene E. Spala
  • Publication number: 20150119304
    Abstract: Disclosed herein is an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition, which is prepared by the process comprising (a) providing an overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition having a total base number (TBN) greater than about 250; and (b) sparging the overbased salt of a sulfurized alkyl-substituted hydroxyaromatic composition with air at a temperature ranging from about 190° C. to about 250° C.
    Type: Application
    Filed: October 30, 2013
    Publication date: April 30, 2015
    Applicants: CHEVRON ORONITE COMPANY LLC, Chevron Oronite Technology B.V.
    Inventors: Ronald T.F. Jukes, Eugene E. Spala
  • Patent number: 8993499
    Abstract: A carboxylate detergent prepared by the process comprising (a) alkylating a hydroxyaromatic compound with at least one normal alpha olefin having from about 12 to about 30 carbon atoms per molecule that has been isomerized to obtain an isomerized alpha olefin having 15-98 wt % branching and a residual alpha olefin content of between from about 0.1 to about 30 wt %, thereby producing an alkylated hydroxyaromatic compound; (b) neutralizing the resulting alkylated hydroxyaromatic compound with an alkali metal base; (c) carbonating the alkali metal salt from step (b) with carbon dioxide; (d) acidifying the salt produced in step (c); and (e) overbasing the resulting alkylated hydroxyaromatic carboxylic acid.
    Type: Grant
    Filed: December 19, 2008
    Date of Patent: March 31, 2015
    Assignees: Chevron Oronite Company LLC, Chevron Oronite S.A.
    Inventors: Curt B. Campbell, Gilles P. Sinquin, Eugene E. Spala, Gilbert R. Chapon
  • Patent number: 8933002
    Abstract: Disclosed herein is a neutral or overbased salt of a sulfurized alkylhydroxyaromatic compound obtained by the process comprising the steps of (a) sulfurizing an alkylhydroxyaromatic compound derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof to provide a sulfurized alkylhydroxyaromatic reaction product; (b) removing any unsulfurized alkylhydroxyaromatic compound from the sulfurized alkylhydroxyaromatic reaction product of step (a) to obtain a sulfurized alkylhydroxyaromatic compound substantially free of the unsulfurized alkylhydroxyaromatic compound; and (c) neutralizing the sulfurized alkylhydroxyaromatic compound of step (b) to provide a salt of the sulfurized alkylhydroxyaromatic compound, wherein the overbased salt of the sulfurized alkylhydroxyaromatic compound contains less than about 2% by combined mass of the unsulfurized alkylhydroxyaromatic compound and its unsulfurized metal
    Type: Grant
    Filed: November 10, 2011
    Date of Patent: January 13, 2015
    Assignees: Chevron Oronite Company LLC, Chevron Oronite SAS
    Inventors: Gilles Sinquin, Curt Campbell, Hélène Lecroq, Eugene E. Spala
  • Publication number: 20140081043
    Abstract: Disclosed is a method for improving filtration in the preparation of an alkaline earth metal alkyltoluene sulfonate concentrate by selectively controlling the meta, ortho, para isomer distribution of the alkyl group of the alkyltoluene produced by the process comprising alkylating toluene with at least one isomerized normal alpha olefin, having from about 18 to about 30 carbon atoms and having from 20% to 100% branching in an alkylation process which includes monitoring % isomer formation and adjusting an alkylation process parameter in order to provide a target specified isomer content of less than 38% meta-isomer content; and thereafter sulfonating and neutralizing to produce a low base number sulfonated alkyltoluene concentrate having a Base Number of about 2 to 60 (ASTM D 2896).
    Type: Application
    Filed: March 30, 2011
    Publication date: March 20, 2014
    Inventors: Pierre Téqui, Curt B. Campbell, Gilles P. Sinquin, Christine Boemare Gandon, Kyle J. Frederic, Eugene E. Spala
  • Patent number: 8603956
    Abstract: The present invention is directed to super overbased polyalkenyl sulfonate and alkylaryl sulfonate composition comprising (a) one or more super overbased polyalkenyl sulfonates and (b) one or more super overbased alkylaryl sulfonates wherein the total base number (TBN) of the sulfonate composition is greater than 400. The present invention is also directed to a process for preparing such super overbased polyalkenyl sulfonate and alkylaryl sulfonate composition.
    Type: Grant
    Filed: April 12, 2006
    Date of Patent: December 10, 2013
    Assignee: Chevron Oronite Company LLC
    Inventor: Eugene E. Spala
  • Publication number: 20130123157
    Abstract: Disclosed herein is a neutral or overbased salt of a sulfurized alkylhydroxyaromatic compound obtained by the process comprising the steps of (a) sulfurizing an alkylhydroxyaromatic compound derived from alkylation of a hydroxyaromatic compound with one or more olefins comprising C9 to C18 oligomers of monomers selected from propylene, butylene or mixtures thereof to provide a sulfurized alkylhydroxyaromatic reaction product; (b) removing any unsulfurized alkylhydroxyaromatic compound from the sulfurized alkylhydroxyaromatic reaction product of step (a) to obtain a sulfurized alkylhydroxyaromatic compound substantially free of the unsulfurized alkylhydroxyaromatic compound; and (c) neutralizing the sulfurized alkylhydroxyaromatic compound of step (b) to provide a salt of the sulfurized alkylhydroxyaromatic compound, wherein the overbased salt of the sulfurized alkylhydroxyaromatic compound contains less than about 2% by combined mass of the unsulfurized alkylhydroxyaromatic compound and its unsulfurized metal
    Type: Application
    Filed: November 10, 2011
    Publication date: May 16, 2013
    Applicant: Chevron Oronite Company LLC
    Inventors: Gilles Sinquin, Curt Campbell, Hélène Lecroq, Eugene E. Spala
  • Patent number: 8188020
    Abstract: The present invention provides overbased detergents as lubricating additives effective for the lubrication of mechanical components in land and marine engines, such as, for example, hydraulic systems, transmissions, two-stroke and four-stroke vehicular engines, and trunk piston and two-stroke crosshead marine engines.
    Type: Grant
    Filed: December 22, 2003
    Date of Patent: May 29, 2012
    Assignee: Chevron Oronite S.A.
    Inventors: Jean-Louis Le Coent, Amedee Guellec, Eugene E. Spala
  • Publication number: 20090170737
    Abstract: A carboxylate detergent prepared by the process comprising (a) alkylating a hydroxyaromatic compound with at least one normal alpha olefin having from about 12 to about 30 carbon atoms per molecule that has been isomerized to obtain an isomerized alpha olefin having 15-98 wt % branching and a residual alpha olefin content of between from about 0.1 to about 30 wt %, thereby producing an alkylated hydroxyaromatic compound; (b) neutralizing the resulting alkylated hydroxyaromatic compound with an alkali metal base; (c) carbonating the alkali metal salt from step (b) with carbon dioxide; (d) acidifying the salt produced in step (c); and (e) overbasing the resulting alkylated hydroxyaromatic carboxylic acid.
    Type: Application
    Filed: December 19, 2008
    Publication date: July 2, 2009
    Inventors: Curt B. Campbell, Gilles P. Sinquin, Eugene E. Spala, Gilbert R. Chapon