Abstract: A method of detaching two substrates at the embrittlement zone situated at a given depth of one of the two substrates. The method includes a separation annealing step implemented in a furnace, wherein the annealing includes a first phase during which the temperature changes along an upgrade allowing a high temperature to be reached and annealing at this high temperature to be stabilized, and a second phase during which the temperature changes along a downgrade, at the end of which the furnace is opened to unload the substrates from the furnace. The second phase is regulated so as to minimize temperature inhomogeneities such as cleavage defects at the detached surfaces of the substrates when the furnace is opened.

Abstract: The invention provides a method of producing a heterostructure of the silicon-on-sapphire type, comprising bonding an SOI substrate onto a sapphire substrate and thinning the SOI substrate, thinning being carried out by grinding followed by etching of the SOI substrate. In accordance with the method, grinding is carried out using a wheel with a grinding surface that comprises abrasive particles having a mean dimension of more than 6.7 ?m; further, after grinding and before etching, the method comprises a step of post-grinding annealing of the heterostructure carried out at a temperature in the range of 150° C. to 170° C.

Abstract: A method of detaching two substrates at the embrittlement zone situated at a given depth of one of the two substrates. The method includes a separation annealing step implemented in a furnace, wherein the annealing includes a first phase during which the temperature changes along an upgrade allowing a high temperature to be reached and annealing at this high temperature to be stabilized, and a second phase during which the temperature changes along a downgrade, at the end of which the furnace is opened to unload the substrates from the furnace. The second phase is regulated so as to minimize temperature inhomogeneities such as cleavage defects at the detached surfaces of the substrates when the furnace is opened.