Abstract: To sample hot liquids containing volatile materials, the liquid is cooled in a refrigerator and pumped through a syringe needle into a container until the container overflows. The needle is removed slowly and the container is automatically closed as the needle is withdrawn, wherein liquid flows upwardly continuously as the needle is withdrawn through an opening. The cap for the container includes a closure having a valve opening extending upwardly and sized to narrowly receive the syringe needle in a perpendicular valve member opening. The valve member includes a flat member on one end adapted to be gripped by a cam follower for opening and closing of the valve opening in coordination with the movement of the syringe needle.

Abstract: To pump fluid into sample containers, a distributor arm of a sample collector is calibrated as to position in a computer memory and is moved from position to position over different containers while a counter in computer memory keeps track of its position. When the distributor arm is over the designated container, samples are pumped into the container. To pump the fluid into the container, the rollers of a peristaltic pump are supported to prevent the rollers from compressing the tube more than the thickness of the walls of the tube. A tube holder rotates along with the roller assembly of the peristaltic pump and keeps the tube in line with the rollers.

Abstract: The rollers of a peristaltic pump are supported to prevent said rollers from compressing said tube more than the thickness of the walls of the tube. A tube holder rotates along with the roller assembly of the peristaltic pump and keeps the tube in line with the rollers.