Abstract: The present disclosure provides a purification method for 3-amino-5-methylpiperidine with amino protected by Boc. The method includes adding a solvent to the crude product of 3-amino-5-methylpiperidine with amino protected by Boc, heating until it is dissolved to obtain a mixed solution; adding an acid and an amine crystallization auxiliary to the mixed solution, stirring and dispersing to obtain a dispersed solution; cooling the dispersed solution until crystallization, separating and drying same to obtain a salt crystal of 3-amino-5-methylpiperidine with amino protected by Boc. The present disclosure improves the product characters of 3-amino-5-methylpiperidine with amino protected by Boc after salifying and crystallization, thereby improving the yield and purity of the product, at the same time, it simplifies the operation steps of salifying and crystallization of 3-amino-5-methylpiperidine with amino protected by Boc, shortens the operation time, and reduces production costs.

Abstract: Provided in the present disclosure are a nemonoxacin malate active pharmaceutical ingredient with low combination impurities, and a preparation method thereof, specifically, provided in the present disclosure is a method for preparing the nemonoxacin malate active pharmaceutical ingredient, the method includes the following steps: 1) providing a C1-C3 alcohol/water mixed solvent in which nemonoxacin free base (Formula II) and D,L-malic acid are dissolved; and 2) performing cooling crystallization on a mixed solution obtained in the step 1), and then performing solid-liquid separation, washing and drying on a precipitated solid, so as to obtain the nemonoxacin malate active pharmaceutical ingredient.

Abstract: The present disclosure discloses a method for synthesizing quinolones intermediates by a continuous flow reaction. Specifically, according to the method, a microchannel reactor is used, which improves the selectivity and conversion rate of the reaction, and the conversion rate of compound ii is increased to more than 95% and the yield is increased to more than 85%; avoids the use of a solvent such as methanol, and methyl tert-butyl ether, etc., in the intermittent reaction process, which simplifies the post-processing method, shortens the overall operation time from about 24 hours to a few minutes, greatly improving the production efficiency, and realizing the continuity and automation of the whole process; and thus makes the product have high purity and high yield, which is suitable for industrial production.

Abstract: Prokaryotic cells having a metal-phenolic network coating are disclosed, as are compositions including such cells, methods for their use, and methods for producing such cells.

Abstract: Provided in the present disclosure are a nemonoxacin malate active pharmaceutical ingredient with low combination impurities, and a preparation method thereof, specifically, provided in the present disclosure is a method for preparing the nemonoxacin malate active pharmaceutical ingredient, the method includes the following steps: 1) providing a C1-C3 alcohol/water mixed solvent in which nemonoxacin free base (Formula II) and D,L-malic acid are dissolved; and 2) performing cooling crystallization on a mixed solution obtained in the step 1), and then performing solid-liquid separation, washing and drying on a precipitated solid, so as to obtain the nemonoxacin malate active pharmaceutical ingredient.

Abstract: The present invention provides a method for preparing a chiral 4-aryl-?-amino acid derivative. The preparation method comprises hydrogenating an enamine compound having a structure as shown in Formula III in an organic solvent in the presence of a catalyst containing a transition metal and BIBOPs. The preparation method of the present invention uses a small amount of a selected asymmetric catalyst, and has a simple operation, mild reaction conditions, a high yield, a high stereoselectivity, and better industrial application and economic values.

Abstract: Prokaryotic cells having a metal-phenolic network coating are disclosed, as are compositions including such cells, methods for their use, and methods for producing such cells.

Abstract: A method of price text detection by an imaging controller comprises obtaining, by the imaging controller, an image of a shelf supporting labels bearing price text, generating, by the imaging controller, a plurality of text regions containing candidate text elements from the image, assigning, by the imaging controller, a classification to each of the text regions, selected from a price text classification and a non-price text classification. The imaging controller, within each of a subset of the text regions having the price text classification: detects a price text sub-region and generates a price text string by applying character recognition to the price text sub-region. The method further includes presenting, by the imaging controller, the locations of the subset of text regions, in association with the corresponding price text strings.

Abstract: A light emitting structure has a substrate, a divider, a light guide element and a light emitting element. The divider is connected with the substrate and erected from the substrate. The light guide element is connected with the divider. The divider is positioned in between the substrate and the light guide element. A chamber is delineated by the substrate, the divider and the light guide element. The light emitting element is mounted onto the substrate, surrounded by the divider, accommodated within the chamber and transparent. The light guide element has an external surface, an internal surface and a convex section and/or a concave section. The external surface and the internal surface are oppositely positioned to each other. The external surface faces away from the substrate. The internal surface faces towards the substrate. The convex section and/or the concave section is formed on the external surface and/or the internal surface.

Abstract: A method of price text detection by an imaging controller comprises obtaining, by the imaging controller, an image of a shelf supporting labels bearing price text, generating, by the imaging controller, a plurality of text regions containing candidate text elements from the image, assigning, by the imaging controller, a classification to each of the text regions, selected from a price text classification and a non-price text classification. The imaging controller, within each of a subset of the text regions having the price text classification: detects a price text sub-region and generates a price text string by applying character recognition to the price text sub-region. The method further includes presenting, by the imaging controller, the locations of the subset of text regions, in association with the corresponding price text strings.

Abstract: Disclosed herein is a method for effecting atom or group transfer polymerization comprising polymerizing one or more radically-polymerizable monomers in the presence of a system comprising an electrically active micro-organism, a transition metal catalyst, one or more radically-polymerizable monomers, and a radical initiator. Micro-organism respiratory electron flux is harnessed to control the performance of a metal-catalyzed polymerization. The bacterial electron transport pathways of the electroactive micro-organisms can be engineered to tune and adapt various function of the electroactive micro-organism and its role in polymerization. Polymerization may be accomplished under aerobic or anaerobic conditions. Freshly cultured micro-organisms or lyophilized micro-organisms may be used to direct polymerization.

Abstract: A method for detecting defects in computer software code comprises: preprocessing a code to check; generating an SEG for the code to check, wherein the SEG includes nodes, data dependency edges and control dependency edges that connect the nodes, wherein, the nodes include value nodes and operator nodes, the value nodes including terminal value nodes representing unknown values or constants generated outside a function, and non-terminal value node representing values generated within the function, wherein each non-terminal value node is associated with a unique memory location, and wherein the data dependency edge is a directed edge connecting a value node to another value node that has a direct data dependency relationship with the value node, and traversing the SEG in a depth-first way backward from a null pointer node in a lowest level of the SEG and generating a bug report when a defect is found.

Abstract: A surface cleaning apparatus includes a separating and collection assembly defining a collection chamber which receives debris and has a debris outlet, a cover assembly having a pre-motor filter, a debris ejector, and a push rod operably coupleable to the debris ejector to displace the debris ejector relative to the debris outlet. The push rod can be accommodated by an opening of the pre-motor filter.

Abstract: A method for detecting defects in computer software code comprises: preprocessing a code to check; generating an SEG for the code to check, wherein the SEG includes nodes, data dependency edges and control dependency edges that connect the nodes, wherein, the nodes include value nodes and operator nodes, the value nodes including terminal value nodes representing unknown values or constants generated outside a function, and non-terminal value node representing values generated within the function, wherein each non-terminal value node is associated with a unique memory location, and wherein the data dependency edge is a directed edge connecting a value node to another value node that has a direct data dependency relationship with the value node, and traversing the SEG in a depth-first way backward from a null pointer node in a lowest level of the SEG and generating a bug report when a defect is found.

Abstract: A surface cleaning apparatus includes a separating and collection assembly defining a collection chamber which receives debris and has a debris outlet, a cover assembly having a pre-motor filter, a debris ejector, and a push rod operably coupleable to the debris ejector to displace the debris ejector relative to the debris outlet. The push rod can be accommodated by an opening of the pre-motor filter.

Abstract: A surface cleaning apparatus includes a separating and collection assembly defining a collection chamber which receives debris and has a debris outlet, and a debris ejector reciprocally moveable within the collection chamber for vertical displacement relative to an exhaust grill. A push rod can be used to displace the debris ejector relative to the exhaust grill.

Abstract: A surface cleaning apparatus includes a separating and collection assembly defining a collection chamber which receives debris and has a debris outlet, and a debris ejector reciprocally moveable within the collection chamber for vertical displacement relative to an exhaust grill. A push rod can be used to displace the debris ejector relative to the exhaust grill.

Abstract: A surface cleaning apparatus includes a separating and collection assembly defining a collection chamber which receives debris and has a debris outlet, and a debris ejector reciprocally moveable within the collection chamber for ejecting debris through the debris outlet. A retractable push rod can be used to displace the debris ejector relative to the debris outlet.

Abstract: In a method for displaying system information, a request to display system information of the electronic device is made. Then, system information to be displayed is obtained from the electronic device. A display interface for displaying the system information is generated according to the obtained system information. The obtained system information is arranged on the display interface according to a predefined way. And, the display interface containing the obtained system information is displayed.

Abstract: A surface cleaning apparatus, such as a steam mop or fluid delivery mop, comprises an upright housing and a foot coupled to the upright housing. The cleaning apparatus comprises an illumination element for illuminating a fluid supply tank and the contents therein. A cleaning pad can be mounted to a lower surface of the foot and positioned to contact the surface to be cleaned. A movable agitator provided on the foot is configured for movement between a first use position in contact with the surface to be cleaned and a second non-use position out of contact with the surface to be cleaned.