Abstract: In a transmission error logging device, method and computer-readable medium for logging transmission errors that occur on a high speed transmission route of a medical technology diagnostic apparatus, the in-feed port for a signal is provided on the high speed transmission route and an error signal is generated upon detection of an error. The transmission volume is detected by a transmission volume counter and the number of errors is detected by a transmission error counter. The transmission volume counter makes a transmission volume count, representing the transmission volume, available as an output from the transmission volume counter, and the transmission error counter makes a count of the number of errors detected by the error detection device available at an output of the transmission error counter.

Abstract: A magnetic resonance system has components that include a magnetic field generation unit for generation of a basic magnetic field, gradient coils for generation of a field gradient as well as a radio-frequency coil arrangement with a number of radio-frequency coils for transmission and reception of radio-frequency signals. These components can respectively be activated according to a sequence via at least one digital module and at least one analog module. The analog modules are arranged externally to a control computer controlling the digital modules. The digital modules also are arranged externally to the control computer and are associated with the analog module or modules controlled by said digital modules. A data network is provided for communication between the digital modules and the control computer and a synchronous network is provided for synchronization of the digital modules and the control computer.

Abstract: A magnetic resonance system has a first installation unit, in which a control processor device is arranged, as well as a radio-frequency coil arrangement for transmitting and receiving magnetic resonance signals. The radio-frequency coil arrangement is controlled or read out by a transmit device, having a digital transmit unit built into the first installation unit for emitting a digital transmit signal to an analog transmit unit, which outputs an analog transmit signal based on the digital transmit signal, and by a receiving apparatus, having at least one analog reception unit for converting an analog received signal into a digital reception signal and at least one digital reception unit for digital demodulation of the received signal. The digital reception unit is built into a further installation unit external to the first installation unit.

Abstract: The invention provides a process for the preparation of polyamines of the diphenylmethane series. This process comprises a) reacting aniline and formaldehyde in a molar ratio of 1.5:1 to 6:1, in the presence of an acid catalyst at temperatures of 20° C. to 100° C., in which the water content in the acid reaction mixture is <20 wt. % and a degree of protonation of <15% is established, and b) increasing the temperature of the reaction to a temperature of 110° C. to 250° C. when the ratio of the weight contents of p-aminobenzylaniline to 4,4?-MDA in the reaction mixture falls below a value of 1.00.

Abstract: The invention provides a process for the preparation of polyamines of the diphenylmethane series. This process comprises a) reacting aniline and formaldehyde in a molar ratio of 1.5:1 to 6:1, in the presence of an acid catalyst at temperatures of 20° C. to 100° C., in which the water content in the acid reaction mixture is <20 wt. % and a degree of protonation of <15% is established, and b) increasing the temperature of the reaction to a temperature of 110° C. to 250° C. when the ratio of the weight contents of p-aminobenzylaniline to 4,4?-MDA in the reaction mixture falls below a value of 1.00.

Abstract: The invention relates to a process for the production of liquid, storage-stable isocyanate mixtures with a low color index having carbodiimide-(CD) and/or uretone imine (UI) groups, the isocyanate mixtures that can be obtained by this process and their use for the production of blends with other isocyanates or for the production of isocyanate group-containing pre-polymers and also of polyurethane plastics, preferably polyurethane foamed plastics.

Abstract: The invention relates to a method of producing polyisocyanates of the diphenylmethane series including the steps of a) reacting aniline and formaldehyde in the presence of HCl to provide a product mixture containing polyamines of the diphenylmethane series, HCl, aniline and water; b) removing excess aniline and water by distillation to provide a product mixture comprising polyamines of the diphenylmethane series, HCl, no more than 10 wt. % aniline based on the polyamines, and no more than 5 wt. % water based on the polyamines; and c) phosgenating the product mixture in (b).

Abstract: A fraction of diisocyanates of the diphenylmethane series containing at least 95 wt. % binuclear methylenediphenyl diisocyanate is obtained by a) reacting aniline and formaldehyde in the presence of an acid catalyst to produce diamines and polyamines of the diphenylmethane series containing binuclear methylenediphenyl diamine, b) phosgenating the diamines and polyamines produced in a), optionally in the presence of a solvent, to produce a crude diisocyanate and polyisocyanate, and c) separating a fraction containing at least 95 wt. % binuclear methylenediphenyl diisocyanate with a 4,4?-MDI content of over 60 wt. %, a 2,4?-MDI content of 4 to 35 wt. % and a 2,2?-MDI content of 0.01 to 10 wt. %, relative to the mass of the fraction, and a maximum of 20 ppm phenyl isocyanate and optionally a maximum of 50 ppm solvent from the crude diisocyanate and polyisocyanate produced in b) in a single distillation step with optional upstream and/or downstream separation of low-boiling components.

Abstract: The invention relates to a process for the preparation of liquid, storage-stable isocyanate mixtures which are characterized by a low color number and which contain carbodiimide (CD) and/or uretonimine (UI) groups. This invention also relates to the isocyanate mixtures obtained by this process, to their use for the preparation of blends with further isocyanates, and to the preparation of prepolymers containing isocyanate groups and of polyurethane plastics, preferably polyurethane foams from these isocyanate mixtures.

Abstract: The present invention relates to a process for the production of MDI fractions containing 2,4?-MDI, and in which the 2,2?-MDI component from the MDA production is largely removed from the isomer mixture. Highly reactive monomeric MDI products can be produced in this way. These MDI products are characterised in their processing by significantly reduced emissions of MDI monomers.

Abstract: A fraction of diisocyanates of the diphenylmethane series containing at least 95 wt. % binuclear methylenediphenyl diisocyanate is obtained by a) reacting aniline and formaldehyde in the presence of an acid catalyst to produce diamines and polyamines of the diphenylmethane series containing binuclear methylenediphenyl diamine, b) phosgenating the diamines and polyamines produced in a), optionally in the presence of a solvent, to produce a crude diisocyanate and polyisocyanate, and c) separating a fraction containing at least 95 wt. % binuclear methylenediphenyl diisocyanate with a 4,4?-MDI content of over 60 wt. %, a 2,4?-MDI content of 4 to 35 wt. % and a 2,2?-MDI content of 0.01 to 10 wt. %, relative to the mass of the fraction, and a maximum of 20 ppm phenyl isocyanate and optionally a maximum of 50 ppm solvent from the crude diisocyanate and polyisocyanate produced in b) in a single distillation step with optional upstream and/or downstream separation of low-boiling components.

Abstract: The invention relates to a method for determining the isomer composition in an isocyanate isomer mixture, wherein a spectrum of the isomer mixture is recorded and the spectrum is entered into a chemometric calibration model.

Abstract: The invention relates to a method of producing polyisocyanates of the diphenylmethane series including the steps of

Abstract: In a method for sampling a received radio-frequency signal, in particular a radio-frequency signal from a receiving coil in a magnetic resonance apparatus, the received radio-frequency signal is down-mixed to a low-frequency baseband such as for image production. The radio-frequency signal from a receiving coil in a magnetic resonance apparatus is passed directly to a high clock rate analog/digital converter where it is converted, as a function of the clock, to a lower frequency, after which it is down-mixed by digital demodulation to a baseband at an even lower frequency.

Abstract: The present invention concerns a process for the production of methylenedianiline (MDA) having a high monomer content.

Abstract: Dinitrotoluene (DNT) is produced by the adiabatic nitration of toluene with nitric acid at a temperature of from about 60 to about 200° C. and at a molar ratio of toluene to nitric acid of from about 1:1.5 to about 1:3.0. The reaction mixture thus-obtained is concentrated to a water content of up to 30% by weight. The dinitrotoluene which is present in the reaction mixture is at least partially (if not completely) removed from the reaction mixture either before or after concentration of the reaction mixture. The DNT which is still present in the vapor generated during the concentration of the reaction mixture is kept liquid by the addition of a solvent to the vapors generated during concentration of the reaction mixture. The solvent added to vapor, together with any DNT present in the vapor is recovered. This solvent/DNT mixture may be recycled directly to the reaction vessel. The solvent/DNT mixture may also be separated. The separated solvent may be recycled to the solvent addition step.

Abstract: Dinitrotoluene (DNT) is produced by the adiabatic nitration of toluene with nitric acid at a temperature of from about 60 to about 200° C. and at a molar ratio of toluene to nitric acid of from about 1:1.5 to about 1:3.0. The reaction mixture thus-obtained is concentrated to a water content of up to 30% by weight. The dinitrotoluene which is present in the reaction mixture is at least partially (if not completely) removed from the reaction mixture either before or after concentration of the reaction mixture. The DNT which is still present in the vapor generated during the concentration of the reaction mixture is kept liquid by the addition of a solvent to the vapors generated during concentration of the reaction mixture. The solvent added to vapor, together with any DNT present in the vapor is recovered. This solvent/DNT mixture may be recycled directly to the reaction vessel. The solvent/DNT mixture may also be separated. The separated solvent may be recycled to the solvent addition step.

Abstract: The present invention concerns a process for the production of methylenedianiline (MDA) having a high monomer content.

Abstract: In a magnetic resonance transmission method and magnetic resonance transmission operating therewith a high-frequency power amplifier emits an output signal with an actual amplitude and an actual phase to a magnetic resonance transmission antenna. A fraction of the signal is digitilized in a magnetic resonance receiver and is supplied to a pulse controller that is realized in software. An analog magnetic resonance reception signal of an object can be supplied to the magnetic resonance receiver during the pulses. The pulse controller determines correction values for a generator amplitude and a generator phase with which a pulse generator is driven, the pulse generator being connected upstream relative to the high-frequency amplifier.

Abstract: In a method for sampling a received radio-frequency signal, in particular a radio-frequency signal from a receiving coil in a magnetic resonance apparatus, the received radio-frequency signal is down-mixed to a low-frequency baseband such as for image production. The radio-frequency signal from a receiving coil in a magnetic resonance apparatus is passed directly to a high clock rate analog/digital converter where it is converted, as a function of the clock, to a lower frequency, after which it is down-mixed by digital demodulation to a baseband at an even lower frequency.