Abstract: A process for purifying solid crude aluminum chloride, containing iron impurities, includes the steps of mixing iron with the crude aluminum chloride and reactively subliming and desubliming the mixture.

Abstract: A process for continuous production of metal chlorides includes the steps of providing metallic ore, containing iron purities, and a carbon source; drying the metallic ore; drying the carbon source; mixing the dried metallic ore, the dried- carbon source, and a sulfur-containing compound; calcining the mixture in a first fluidized bed reactor in the presence of air; chlorinating the calcined product in a second fluidized bed reactor in the presence of additional carbon source and additional sulfur-containing compound to produce crude metal chlorides and waste gases; and reactively subliming and desubliming the crude metal chlorides, in the presence of additional iron, aluminum, cesium, copper, lead, lithium, magnesium, mercury, potassium, sodium, titanium, uranium, zinc or zirconium, to produce purified aluminum chloride.

Abstract: The invention comprises a process for the manufacture of metal chlorides by the double-decomposition reaction between a metal chlorinating agent and a metal oxide having greater affinity for chlorine than does the oxide of the metal chloride, and in the presence of small amounts of boron chloride or functionally equivalent boron compounds that increase the rate and degree of completion of the reaction.A major application of this invention is for the making by the chlorination of clay of aluminum chloride and alumina intermediates for the manufacture of aluminum metal.SiCl.sub.4 is formed in the carbo-chlorination of clay or other aluminous-siliceous ores. The SiCl.sub.4 by this invention is catalyzed with BCl.sub.3 and reacted with calcined clay to produce AlCl.sub.3 and SiO.sub.2. The practical use of SiCl.sub.4 to make AlCl.sub.3 thus eliminates the previous costly burden of waste SiCl.sub.4 production.

Abstract: Apparatus and method are disclosed for externally testing flanged or hubbed connections used on fluid conducting conduits. A ring gasket fits between the faces of the connecting flanges or hubs to effect a fluid tight seal. A test ring also fits between the faces of the hub or flange connection in a manner so as to form a space between the test ring and the ring gasket. Seal means closes the space between the test ring and the faces of the flanges or hubs. The outside diameter of the test ring is confined within fastening means which secures the hubs or flanges together. Fluid under pressure, used to test the effectiveness of the ring gasket seal, is applied to the space between the ring gasket and the test ring seal means. The pressure in that space falls when the ring gasket is defective but remains constant if the ring gasket is sound. Following the test, fluid pressure is bled off the space between the ring gasket and the test ring seal means.

Abstract: Apparatus and method are disclosed for externally testing flanged or hubbed connections used on fluid conducting conduits. A ring gasket fits between the faces of the connecting flanges or hubs to effect a fluid tight seal. A test ring also fits between the faces of the hub or flange connection in a manner so as to form a space between the test ring and the ring gasket. Seal means closes the space between the test ring and the faces of the flanges or hubs. The outside diameter of the test ring is confined within fastening means which secures the hubs or flanges together. Fluid under pressure, used to test the effectiveness of the ring gasket seal, is applied to the space between the ring gasket and the test ring seal means. The pressure in that space falls when the ring gasket is defective but remains constant if the ring gasket is sound. Following the test, fluid pressure is bled off the space between the ring gasket and the test ring seal means.