Patents by Inventor Gunther Windecker
Gunther Windecker has filed for patents to protect the following inventions. This listing includes patent applications that are pending as well as patents that have already been granted by the United States Patent and Trademark Office (USPTO).
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Patent number: 9045382Abstract: The present invention relates to a process for separating off solvents from solvent-comprising hydrogenation outputs from a catalytic hydrogenation process, which comprise at least one water-soluble hydrogenation product having at least one alcohol, lactone, ether, lactam or amino group in a solvent which is immiscible or not completely miscible with water and has a boiling point below 100° C., wherein water is added to the hydrogenation output, the solvent-comprising phase is separated off and recirculated to the hydrogenation.Type: GrantFiled: July 16, 2007Date of Patent: June 2, 2015Assignee: BASF AktiengesellschaftInventors: Rolf Pinkos, Jens Heimann, Hans-Martin Polka, Heiko Urtel, Gunther Windecker
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Patent number: 8476463Abstract: Processes for decreasing fumaric acid deposits in preparing maleic anhydride by heterogeneously catalyzed oxidation of a hydrocarbon with molecular oxygen. Maleic anhydride is absorbed from the crude mixture in an absorbent in an absorption column and desorbed in a desorption column, the entirety or portion of absorbent depleted in maleic anhydride, for controlled precipitation of fumaric acid, being cooled and/or concentrated by evaporating a portion of absorbent such that the difference between the concentration of fumaric acid in the recycle stream at the outlet of the desorption column under existing conditions and the equilibrium concentration of fumaric acid according to the solubility curve after cooling and/or evaporation of a portion of absorbent is ?250 ppm by weight, and the fumaric acid precipitated as a solid is removed completely or partly from the absorbent recycling system and the fumaric acid-depleted absorbent is recycled completely or partly to the absorption column.Type: GrantFiled: March 23, 2009Date of Patent: July 2, 2013Assignee: BASF SEInventors: Gunther Windecker, Jens Weiguny, Alexander Weck, Ellen Dahlhoff, Wolf-Steffen Weiβker, Jörg Heilek, Thomas Krug, Ralf Freyberger
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Patent number: 8461356Abstract: What is described is a process for obtaining maleic anhydride by distillation from a solution of maleic anhydride in a high-boiling absorbent which has been obtained by gas phase oxidation of a hydrocarbon and at least partial absorption of the oxidation products into the absorbent, by i) introducing the solution into the side of a feed column with a rectifying section disposed above the feed point and a stripping section disposed below the feed point, ii) providing an upper combining column which communicates with the upper end of the rectifying section and a lower combining column which communicates with the lower end of the stripping section, iii) providing a draw column which communicates with the upper combining column and the lower combining column, iv) drawing maleic anhydride off as a side draw from the draw column, and drawing off compounds having a lower boiling point than maleic anhydride at the top of the upper combining column and the high-boiling absorbent at the bottom of the lower combining cType: GrantFiled: March 19, 2008Date of Patent: June 11, 2013Assignee: BASF SEInventors: Gunther Windecker, Gerd Kaibel, Michael Steiniger, Thilo Buntrock, Jens Weiguny, Dany Vanden Hautte, Thierry Lurquin
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Patent number: 8071389Abstract: The invention relates to a method of controlling a hydrogenation of a starting material in a hydrogenation reactor, in which the amount of hydrogen reacted in the hydrogenation is firstly determined, the ratio of the amount of hydrogen reacted to the amount of starting material fed in is then derived, this ratio is compared with a prescribed value and, finally, at least one process parameter is altered if the ratio of the amount of hydrogen reacted to the amount of starting material fed in deviates by a prescribed amount from the prescribed value.Type: GrantFiled: January 30, 2006Date of Patent: December 6, 2011Assignee: BASF AktiengesellschaftInventors: Alexander Weck, Markus Rösch, Gunther Windecker, Gunnar Heydrich, Rolf Pinkos, Olga Schubert, Klaus Harth
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Publication number: 20110245517Abstract: The present invention relates to a process for preparing tetrahydrofuran by absorption of C4-dicarboxylic acids and/or derivatives thereof from a crude product mixture into an organic solvent or water as absorption medium, removal of the absorption medium, catalytic hydrogenation of the resulting C4-dicarboxylic acids and/or derivatives thereof and distillation of the water-comprising crude tetrahydrofuran in at least one distillation column, wherein THF-comprising waste streams from the distillation are catalytically hydrogenated with complete or partial recirculation to the process.Type: ApplicationFiled: November 5, 2009Publication date: October 6, 2011Applicant: BASF SEInventors: Gunther Windecker, Jens Weiguny, Alexander Weck, Ellen Dahlhoff, Ralf Freyberger
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Publication number: 20110021789Abstract: A process for decreasing fumaric acid deposits in the preparation of maleic anhydride by heterogeneously catalyzed oxidation of a hydrocarbon with molecular oxygen, in which the maleic anhydride is absorbed from the crude product mixture in an absorbent in an absorption column and desorbed again in a desorption column, the entirety or a portion of the absorbent depleted in maleic anhydride, for controlled precipitation of fumaric acid, being cooled and/or concentrated by evaporating a portion of the absorbent to such an extent that the difference between the concentration of fumaric acid in the recycle stream at the outlet of the desorption column under the conditions existing there and the equilibrium concentration of fumaric acid according to the solubility curve after the cooling and/or evaporation of a portion of the absorbent is greater than or equal to 250 ppm by weight, and the fumaric acid precipitated as a solid is removed completely or partly from the absorbent recycling system and the fumaric acid-Type: ApplicationFiled: March 23, 2009Publication date: January 27, 2011Applicant: BASF SEInventors: Gunther Windecker, Jens Weiguny, Alexander Weck, Ellen Dahlhoff, Wolf-Steffen Weissker, Jörg Heilek, Thomas Krug, Ralf Freyberger
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Patent number: 7807603Abstract: The invention relates to a catalyst provided in the form of an extrudate, which contains 5 to 85% by weight of copper oxide and comprises, in the active material and as binders, the same oxidic carrier material. The invention also relates to the use of the catalyst for hydrogenating carbonyl compounds.Type: GrantFiled: December 4, 2004Date of Patent: October 5, 2010Assignee: BASF AktiengesellschaftInventors: Stephan Schlitter, Olga Schubert, Michael Hesse, Sabine Borchers, Markus Roesch, Rolf Pinkos, Alexander Weck, Gunther Windecker
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Publication number: 20100113805Abstract: What is described is a process for obtaining maleic anhydride by distillation from a solution of maleic anhydride in a high-boiling absorbent which has been obtained by gas phase oxidation of a hydrocarbon and at least partial absorption of the oxidation products into the absorbent, by i) introducing the solution into the side of a feed column with a rectifying section disposed above the feed point and a stripping section disposed below the feed point, ii) providing an upper combining column which communicates with the upper end of the rectifying section and a lower combining column which communicates with the lower end of the stripping section, iii) providing a draw column which communicates with the upper combining column and the lower combining column, iv) drawing maleic anhydride off as a side draw from the draw column, and drawing off compounds having a lower boiling point than maleic anhydride at the top of the upper combining column and the high-boiling absorbent at the bottom of the lower combining cType: ApplicationFiled: March 19, 2008Publication date: May 6, 2010Applicant: BASF SEInventors: Gunther Windecker, Gerd Kaibel, Michael Steiniger, Thilo Buntrock, Jens Weiguny, Dany Vanden Hautte, Thierry Lurquin
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Publication number: 20090314992Abstract: The present invention relates to a process for separating off solvents from solvent-comprising hydrogenation outputs from a catalytic hydrogenation process, which comprise at least one water-soluble hydrogenation product having at least one alcohol, lactone, ether, lactam or amino group in a solvent which is immiscible or not completely miscible with water and has a boiling point below 100° C., wherein water is added to the hydrogenation output, the solvent-comprising phase is separated off and recirculated to the hydrogenation.Type: ApplicationFiled: July 16, 2007Publication date: December 24, 2009Applicant: BASF SEInventors: Rolf Pinkos, Jens Heimann, Hans-Martin Polka, Heiko Urtel, Gunther Windecker
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Patent number: 7598405Abstract: The present invention provides a process for distillatively purifying tetrahydrofuran in the presence of a polar solvent.Type: GrantFiled: September 21, 2005Date of Patent: October 6, 2009Assignee: BASF AktiengesellschaftInventors: Gunther Windecker, Alexander Weck, Markus Roesch, Michael Steiniger, Rolf Pinkos, Dany Vanden Hautte
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Publication number: 20090143601Abstract: The present invention provides a process for preventing fumaric acid deposits in the preparation of maleic anhydride, comprising the following steps: a) absorption of a C4-dicarboxylic acid or of a derivative from a crude product mixture into an organic solvent or water as an absorbent, b) removal of the C4-dicarboxylic acid or of a derivative from the absorbent, the absorbent thus recovered being catalytically hydrogenated fully or partly and recycled fully or partly into the absorption stage (a).Type: ApplicationFiled: May 16, 2007Publication date: June 4, 2009Applicant: BASF SEInventors: Rolf Pinkos, Gerd Kaibel, Ellen Dahlhoff, Gunther Windecker, Jens Heimann
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Patent number: 7459571Abstract: Catalyst in the form of an extrudate which comprises from 5 to 85% by weight of copper oxide and in which the same oxidic support material is present in the active composition and as binder, and the use of the catalyst for the hydrogenation of carbonyl compounds.Type: GrantFiled: November 2, 2007Date of Patent: December 2, 2008Assignee: BASF AktiengesellschaftInventors: Stephan Schlitter, Olga Schubert, Michael Hesse, Sabine Borchers, Markus Roesch, Rolf Pinkos, Alexander Weck, Gunther Windecker
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Patent number: 7442810Abstract: A process for variably preparing mixtures of optionally alkyl-substituted BDO, GBL and THF by two-stage hydrogenation in the gas phase of C4 dicarboxylic acids and/or derivatives thereof, which comprises a) hydrogenating in a gas phase a gas stream of C4 dicarboxylic acids and/or derivatives thereof over a particular catalyst at a particular pressure and temperature to give a stream mainly containing of optionally alkyl-substituted GBL and THF, b) removing any succinct anhydride, c) converting the products remaining predominantly in the gas phase in the partial condensation, THF, water and GBL to give a stream comprising a mixture of BDO, GBL and THF, d) removing the hydrogen from the products and recycling it into the hydrogenation, e) distillatively separating the products, THF, BDO, GBL and water, if appropriate recycling a GBL-rich stream or if appropriate discharging it, and working up BDO, THF and GBL distillatively, and setting the ratio of the products, THF, GBL and BDO, relative to one another wiType: GrantFiled: December 4, 2004Date of Patent: October 28, 2008Assignee: BASF AktiengesellschaftInventors: Markus Roesch, Rolf Pinkos, Michael Hesse, Stephan Schlitter, Henrik Junicke, Olga Schubert, Alexander Weck, Gunther Windecker
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Publication number: 20080182996Abstract: The invention relates to a process for separating off maleic anhydride from a gas stream comprising maleic anhydride, in which a) the gas stream comprising maleic anhydride is brought into contact with a liquid absorbent phase comprising at least one high-boiling inert absorption medium for maleic anhydride and b) maleic anhydride is separated off from the resulting liquid absorbate phase by stripping with a hydrogen-comprising gas as stripping medium in a column, wherein the stripping medium is fed in at two points on the column which are at least one theoretical plate apart.Type: ApplicationFiled: June 30, 2006Publication date: July 31, 2008Applicant: BASF AktiengesellschaftInventors: Gunther Windecker, Alexander Weck, Michael Steiniger, Jan Peter Bredehoft, Bianca Bender, Peter Knappik, Dany Vanden Hautte, Bernard Pierre, Beatrix Haffner
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Publication number: 20080166816Abstract: The invention relates to a method of controlling a hydrogenation of a starting material in a hydrogenation reactor, in which the amount of hydrogen reacted in the hydrogenation is firstly determined, the ratio of the amount of hydrogen reacted to the amount of starting material fed in is then derived, this ratio is compared with a prescribed value and, finally, at least one process parameter is altered if the ratio of the amount of hydrogen reacted to the amount of starting material fed in deviates by a prescribed amount from the prescribed value.Type: ApplicationFiled: January 30, 2006Publication date: July 10, 2008Applicant: BASF AktiengesellschaftInventors: Alexander Weck, Markus Rosch, Gunther Windecker, Gunnar Heydrich, Rolf Pinkos, Olga Schubert, Klaus Harth
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Patent number: 7351311Abstract: Crude water-containing tetrahydrofuran is purified by passing the crude tetrahydrofuran through three distillation columns, withdrawing water from the bottom of the first column, recycling water-containing tetrahydrofuran from the top of the second column into the first column, passing a sidestream of the first column into the second column, recycling the bottom product of the third column into the first column, and withdrawing a distillate at the top of the first column. Additionally, a sidestream of the second column is passed into the third column and the purified tetrahydrofuran is recovered as the top product of the third column.Type: GrantFiled: February 28, 2003Date of Patent: April 1, 2008Assignee: BASF AktiengesellschaftInventors: Gunther Windecker, Alexander Weck, Rolf-Hartmuth Fischer, Markus Rösch, Nils Bottke, Michael Hesse, Stephan Schlitter, Holger Borchert
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Publication number: 20080064883Abstract: Catalyst in the form of an extrudate which comprises from 5 to 85% by weight of copper oxide and in which the same oxidic support material is present in the active composition and as binder, and the use of the catalyst for the hydrogenation of carbonyl compounds.Type: ApplicationFiled: November 2, 2007Publication date: March 13, 2008Applicant: BASF AktiengesellschaftInventors: Stephan SCHLITTER, Olga SCHUBERT, Michael HESSE, Sabine BORCHERS, Markus ROSCH, Rolf PINKOS, Alexander WECK, Gunther WINDECKER
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Publication number: 20080058539Abstract: The present invention provides a process for distillatively purifying tetrahydrofuran in the presence of a polar solvent.Type: ApplicationFiled: September 21, 2005Publication date: March 6, 2008Applicant: BASF AktiengessellschaftInventors: Gunther Windecker, Alexander Weck, Markus Rosch, Michael Steiniger, Rolf Pinkos, Dany Hautte
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Patent number: 7271299Abstract: Optionally alkyl-substituted 1,4-butanediol is prepared from C4-dicarboxylic acids and/or of derivatives thereof by: a) a gas stream of the C4-dicarboxylic acid or the derivative thereof in a first reactor in the gas phase to obtain a product which contains mainly optionally alkyl-substituted ?-butyro-lactone; b) removing succinic anhydride from the product of step a); c) catalytically hydrogenating the product of step b) in a second reactor in the gas phase to obtain optionally alkyl-substituted 1,4-butanediol; d) removing the desired product from intermediates, by-products and any unconverted reactants; and e) optionally recycling unconverted intermediates into one or both hydrogenation stages. The catalysts employed in each of the hydrogenation stages comprise ?95% by weight of CuO, and ?5% by weight of an oxidic support, and the second reactor has a higher pressure than the first reactor.Type: GrantFiled: June 11, 2003Date of Patent: September 18, 2007Assignee: BASF AktiengesellschaftInventors: Michael Hesse, Stephan Schlitter, Holger Borchert, Markus Schubert, Markus Rösch, Nils Bottke, Rolf-Hartmuth Fischer, Alexander Weck, Gunther Windecker, Gunnar Heydrich
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Publication number: 20070135650Abstract: The present invention provides a process for variably preparing mixtures of optionally alkyl-substituted BDO, GBL and THF by two-stage hydrogenation in the gas phase of C4 dicarboxylic acids and/or derivatives thereof, which comprises a) in a first step in the gas phase, hydrogenating a gas stream of C4 dicarboxylic acids and/or derivatives thereof over a catalyst at a pressure of from 2 to 100 bar and a temperature of from 200° C. to 300° C.Type: ApplicationFiled: December 4, 2004Publication date: June 14, 2007Applicant: BASF AKTIENGESELLSCHAFTInventors: Markus Rosch, Rolf Pinkos, Michael Hesse, Stephan Schlitter, Henrik Junicke, Olga Schubert, Alexander Weck, Gunther Windecker