Abstract: An apparatus for preparing samples of granulated material comprises an upper vessel having a floor including a plurality of planks, slots between each plank, and an open ceiling to allow passing of homogenized material, a lower vessel under the upper vessel and having a plurality of division plates that fit in the slots and form a plurality of compartments which hold samples, a feeder which oscillates over the upper surface of the upper vessel to render a homogenised and representative sample. The method comprises positioning the lower vessel under the upper vessel, feeding material to be sampled through the feeder by an oscillating movement, raising the lower vessel such that the division plates partition the heap of material to form a plurality of samples, removing planks from the upper vessel, thus forcing the plurality of samples to fall toward the compartments, and separating both the vessels to remove the samples.

Abstract: A reactor for molybdenum sulphide (MoS2), wherein MoS2 is ionized by an electric field generated by a first set of magnetrons at a frequency in the range of 2500-3500 MHz and heated by a variable magnetic field of 2500 Hz produced by a winding coil, resulting in the exclusive evaporation of molybdenite. MoS2 in gas state is then stimulated by a second set of magnetrons and, with the injection of air, oxidized until trioxide is obtained. Hot gases essentially containing molybdenum trioxide, sulphur dioxide, and nitrogen are conducted from a first body towards a second body though a first duct. Cold air is added to the second body through a second duct to cool the gas, and crystals formed by liquefaction settle and are removed through a lower duct while gases at a temperature of 600° C. are conducted through a higher duct.

Abstract: An apparatus for preparing samples of granulated material comprises an upper vessel having a floor including a plurality of planks, slots between each plank, and an open ceiling to allow passing of homogenized material, a lower vessel under the upper vessel and having a plurality of division plates that fit in the slots and form a plurality of compartments which hold samples, a feeder which oscillates over the upper surface of the upper vessel to render a homogenised and representative sample. The method comprises positioning the lower vessel under the upper vessel, feeding material to be sampled through the feeder by an oscillating movement, raising the lower vessel such that the division plates partition the heap of material to form a plurality of samples, removing planks from the upper vessel, thus forcing the plurality of samples to fall toward the compartments, and separating both the vessels to remove the samples.

Abstract: A reactor for molybdenum sulphide (MoS2), wherein MoS2 is ionized by an electric field generated by a first set of magnetrons at a frequency in the range of 2500-3500 MHz and heated by a variable magnetic field of 2500 Hz produced by a winding coil, resulting in the exclusive evaporation of molybdenite. MoS2 in gas state is then stimulated by a second set of magnetrons and, with the injection of air, oxidized until trioxide is obtained. Hot gases essentially containing molybdenum trioxide, sulphur dioxide, and nitrogen are conducted from a first body towards a second body though a first duct. Cold air is added to the second body through a second duct to cool the gas, and crystals formed by liquefaction settle and are removed through a lower duct while gases at a temperature of 600° C. are conducted through a higher duct.